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Volumn 46, Issue 19, 2007, Pages 3541-3543

High-yield synthesis of medium and large platinacycloalkanes from bis(alkenyl) precursors

Author keywords

Metallacycles; Metathesis; Platinum; Structure elucidation; Thermal decomposition

Indexed keywords

HYDROGENATION; ORGANOMETALLICS; PYROLYSIS; SYNTHESIS (CHEMICAL);

METATHESIS; PLATINACYCLOALKANES;

PARAFFINS;

EID: 34250889418 PISSN: 14337851 EISSN: None Source Type: Journal
DOI: 10.1002/anie.200604979 Document Type: Article

Times cited : (23)

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- Structure determination and crystallographic data for 2c: crystals were obtained by slow diffusion of n-hexane into a solution of 2c in dichoromethane. C41H52P2Pt 1, Mr, 801.86 g mol-1, triclinic, space group P1, a, 12.1550(1, b, 12.3649(1, c, 14.4431(2) Å, α, 108.061(1, β, 95.214(1, γ, 114.631(1)°, V, 1814.14(3) Å3, Z, 2, ρcalcd, 1.468 g cm-3, T, 113(2) K, μ, 3.982 mm-1, F(000, 812, 3.37° < 2θ < 26.37°, λ(MoKα, 0.71073 Å, crystal size 0.15 x 0.17 x 0.21 mm3. Intensity data were collected with a Nonius KappaCCD diffractometer. 34 532 reflections, 7379 independent (R int, 0.0309, empirical absorption correction SADABS, structure solution using direct metho
- -3. CCDC-629152 (2c) and CCDC-629153 (3d) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via http://www.ccdc.cam.ac.uk/data_request/cif.

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