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Volumn 46, Issue 10, 2007, Pages 3792-3794

Oxidation of the tris(carbene)borate complex PhB(Melm)3Mn I(CO)3 to MnIV[PhB(Melm)3] 2(OTf)2

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EID: 34249680656     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic070187w     Document Type: Article
Times cited : (69)

References (35)
  • 6
    • 33947298577 scopus 로고
    • For selected examples, see
    • For selected examples, see: Trofimenko, S. J. Am. Chem. Soc. 1969, 91, 588;
    • (1969) J. Am. Chem. Soc , vol.91 , pp. 588
    • Trofimenko, S.1
  • 11
    • 34249734030 scopus 로고    scopus 로고
    • int = 0.0418), R1 = 0.0310, and wR2 = 0.0616. See the Supporting Information for full synthetic and characterization details.
    • int = 0.0418), R1 = 0.0310, and wR2 = 0.0616. See the Supporting Information for full synthetic and characterization details.
  • 14
    • 34249741891 scopus 로고    scopus 로고
    • 3 is insensitive to light, water, or heat.
    • 3 is insensitive to light, water, or heat.
  • 15
    • 34249752467 scopus 로고    scopus 로고
    • 2. There is no evidence in the IR spectrum of this material for CO ligands or a carbonate anion.
    • 2. There is no evidence in the IR spectrum of this material for CO ligands or a carbonate anion.
  • 16
    • 34249710592 scopus 로고    scopus 로고
    • Crystallographic data for C38H40B2F 6MnN12O6S2: M, 1003.55, P21/ c, a, 12.8947(5) Å, b, 13.9914(5) Å, c, 13.5128(5) Å, β, 64.280(2)°, V, 2196.38(14) A3, T, 293(2) K, Z, 4, F(000, 1042, μ(Mo Kα, 0.482 mm-1, 27 746 reflections, 3247 unique Rint, 0.0211, R1, 0.0404, and wR2, 0.1132
    • int = 0.0211), R1 = 0.0404, and wR2 = 0.1132.
  • 35
    • 0000890792 scopus 로고    scopus 로고
    • 1/2 = 0.54 V, see: Morris, R. H.; Earl, K. A.; Luck, R. L.; Lazarowych, N. J.; Sella, A. Inorg. Chem. 1987, 26, 2674.
    • 1/2 = 0.54 V, see: Morris, R. H.; Earl, K. A.; Luck, R. L.; Lazarowych, N. J.; Sella, A. Inorg. Chem. 1987, 26, 2674.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.