메뉴 건너뛰기




Volumn 63, Issue 26, 2007, Pages 5918-5929

Synthesis of migrastatin and its macrolide core

Author keywords

[No Author keywords available]

Indexed keywords

LACTONE DERIVATIVE; MACROLIDE; MIGRASTATIN; UNCLASSIFIED DRUG;

EID: 34248633349     PISSN: 00404020     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tet.2007.02.107     Document Type: Article
Times cited : (37)

References (35)
  • 14
    • 33749026617 scopus 로고    scopus 로고
    • For a recent review on macrocyclization of unsaturated lactones by ring-closing metathesis, see:
    • For a recent review on macrocyclization of unsaturated lactones by ring-closing metathesis, see:. Gradillas A., and Pérez-Castells J. Angew. Chem., Int. Ed. 45 (2006) 6086-6101
    • (2006) Angew. Chem., Int. Ed. , vol.45 , pp. 6086-6101
    • Gradillas, A.1    Pérez-Castells, J.2
  • 16
    • 34248633898 scopus 로고    scopus 로고
    • note
    • 1H NMR spectra of the crude reaction mixture.
  • 18
    • 0026325277 scopus 로고
    • Phosphonoacetate III can be easily prepared from inexpensive starting materials:
    • Phosphonoacetate III can be easily prepared from inexpensive starting materials:. Patois C., Savignac P., About-Jaudet E., and Collignon N. Synth. Commun. 21 (1991) 2391-2396
    • (1991) Synth. Commun. , vol.21 , pp. 2391-2396
    • Patois, C.1    Savignac, P.2    About-Jaudet, E.3    Collignon, N.4
  • 19
    • 34248642727 scopus 로고    scopus 로고
    • note
    • Catalyst [Ru]-II was added in six portions over 144 h.
  • 20
    • 34248658677 scopus 로고    scopus 로고
    • note
    • 2,6-Heptadienoic acid I and mixed anhydride IV were prepared according to Ref. 6c.
  • 24
    • 0038215596 scopus 로고    scopus 로고
    • For a review on olefin cross-metathesis, see:
    • For a review on olefin cross-metathesis, see:. Connon S.J., and Blechert S. Angew. Chem., Int. Ed. 42 (2003) 1900-1923
    • (2003) Angew. Chem., Int. Ed. , vol.42 , pp. 1900-1923
    • Connon, S.J.1    Blechert, S.2
  • 26
    • 34248679763 scopus 로고    scopus 로고
    • note
    • Crotyltitanium complex Ti(S,S)-I allows the delivery of the nucleophile on the Re face of aldehyde 16.
  • 28
    • 34248632399 scopus 로고    scopus 로고
    • note
    • Enone 20 was recovered in 40% yield. The catalyst [Ru]-III and 15 were added three times over 72 h. The yields for this reaction range from 27% to 50%.
  • 32
    • 34248683787 scopus 로고    scopus 로고
    • note
    • Catalyst [Cu]-I was prepared following the procedure described in Ref. 24.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.