Wide compositional and structural diversity in the system Tl/Bi/P/Q (Q = S, Se) and observation of vicinal P-Tl J coupling in the solid state

Inorganic Chemistry

Volumn 46, Issue 9, 2007, Pages 3632-3644

  Gave, Matthew A ^a   Malliakas, Christos D ^a   Weliky, David P ^a   Kanatzidis, Mercouri G ^a,b  

^a MICHIGAN STATE UNIVERSITY   (United States)

^b NORTHWESTERN UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 34248329223     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic062465h     Document Type: Article

References (60)

1. (a) Kanatzidis, M. G. Chem. Mater. 1990, 2, 353-363.
2. (b) Kanatzidis, M. G.; Park, Y. J. Am. Chem. Soc. 1989, 111, 3767-3769.
3. (c) Kanatzidis, M. G.; Park, Y. Chem. Mater. 1990, 2, 99-101.
4. (d) Park, Y.; Kanatzidis, M. G. Angew. Chem., Int. Ed. Engl. 1990, 29, 914-915.
5. (e) McCarthy, T. J.; Kanatzidis, M. G. Inorg. Chem. 1995, 34, 1257-1267.
6. (f) Chondroudis, K.; Kanatzidis, M. G. J. Solid State Chem. 1998, 138, 321-328.
7. (g) Iordanidis, L.; Bile, D.; Mahanti, S. D.; Kanatzidis, M. G. J. Am. Chem. Soc. 2003, 125, 13741-13752.
8. McCarthy, T. J.; Ngeyi, S.-P.; Liao, J.-H.; DeGroot, D. C.; Hogan, T.; Kannewurf, C. R.; Kanatzidis, M. G. Chem. Mater. 1993, 5, 331-340.
9. Iordanidis, L.; Brazis, P. W.; Kyratsi, T.; Ireland, J.; Lane, M.; Kannewurf, C. R.; Chen, W.; Dyck, J. S.; Uher, C.; Ghelani, N. A.; Hogan, T.; Kanatzidis, M. G. Chem. Mater. 2001, 13, 622-633.
10. Iordanidis, L.; Schindler, J. L.; Kannewurf, C. R.; Kanatzidis, M. G. J. Solid State Chem. 1999, 143, 151-162.
11. (a) Kohatsu, I.; Wuensch, B. J. Acta Crystallogr. 1976, B32, 2401-2409.
12. (b) Cook, R.; Schafer, H. Rev. Chim. Miner. 1982, 19, 19-27.
13. (c) Wiegers, G. A.; Meetsma, A.; Vansmaalen, S.; Haange, R. J.; Wulff, J.; Zeinstra, T.; Deboer, J. L.; Kuypers, S.; Vantendeloo, G.; Vanlanduyt, J.; Amelinckx, S.; Meerschaut, A.; Rabu, P.; Rouxel, J. Solid State Commun. 1989, 70, 409-413.
14. (a) Mrotzek, A.; Kanatzidis, M. G. Acc. Chem. Res. 2003, 36, 111-119.
15. (b) Kanatzidis, M. G. Acc. Chem. Res. 2005, 38, 359-368.
16. (a) Makovicky, E. Fortschr. Mineral. 1981, 59, 137-190.
17. (b) Makovicky, E. Fortschr. Mineral. 1985, 63, 45-89.
18. (c) Makovicky, E. Z. Kristallogr. 1985, 173, 1-23.
19. (d) Makovicky, E. Neues Jahrb. Mineral, Abh. 1989, 160, 269-297.
20. Chung, I.; Do, J.; Canlas, C. G.; Weliky, D. P.; Kanatzidis, M. G. Inorg. Chem. 2004, 43, 2762-2764.
21. Knaust, J. M.; Dorhout, P. K. J. Chem. Crystallogr. 2006, 36, 217-223.
22. (a) Kanatzidis, M. G. Curr. Opin. Solid State Mater. Sci. 1997, 2, 139-149.
23. (b) Coste, S.; Hanko, J.; Bujoli-Doeuff, M.; Louarn, G.; Evain, M.; Brec, R.; Alonso, B.; Jobic, S.; Kanatzidis, M. G. J. Solid State Chem. 2003, 175, 133-145.
24. (a) Manriquez, V.; Galdamez, A.; Ruiz-Leon, D. Mater. Res. Bull. 2006, 41, 1337-1344.
25. (b) Belkyal, I.; El Azhari, M.; Wu, Y. D.; Bensch, W.; Hesse, K. F.; Depmeier, W. Solid State Sci. 2006, 8 (1), 59-63.
26. (c) Gieck, C.; Tremel, W. Chem. - Eur. J. 2002, 8, 2980-2987.
27. (d) Coste, S.; Kopnin, E.; Evain, M.; Jobic, S.; Brec, R.; Chondroudis, K.; Kanatzidis, M. G. Solid State Sci. 2002, 4, 709-716.
28. (e) Hess, R. F.; Gordon, P. L.; Tait, C. D.; Abney, K. D.; Dorhout, P. K. J. Am. Chem. Soc. 2002, 124, 1327-1333.
29. (f) Coste, S.; Kopnin, E.; Evain, M.; Jobic, S.; Payen, C.; Brec, R. J. Solid State Chem. 2001, 162, 195-203.
30. McCarthy, T. J.; Kanatzidis, M. G. Chem. Mater. 1993, 5, 1061-1063.
31. Manriquez, V.; Galdamez, A.; Leon, D. R.; Garland, M. T.; Jimenez, M. Z. Kristallogr. Krist. 2003, 218, 151-152.
32. McCarthy, T. J.; Kanatzidis, M. G. J. Alloys Compd. 1996, 236, 70-85.
33. Chung, I.; Karst, A. L.; Weliky, D. P.; Kanatzidis, M. G. Inorg. Chem. 2006, 45, 2785-2787.
34. (a) Odoulov, S. G.; Shumelyuk, A. N.; Brost, G. A.; Magde, K. M. Appl. Phys. Lett. 1996, 69, 3665-3667.
35. (b) Shumelyuk, A.; Hryhorashchuk, A.; Odoulov, S. Phys. Rev. A 2005, 72, 023819.
36. Kroupa, J.; Tyagur, Y. I.; Grabar, A. A.; Vysochanskii, Y. M. Ferroelectrics 1999, 223, 421-428.
37. McGuire, M. A.; Reynolds, T. K.; DiSalvo, F. J. Chem. Mater. 2005, 17, 2875-2884.
38. Iyer, R. G.; Aitken, J. A.; Kanatzidis, M. G. Solid State Sci. 2004, 6, 451-459.
39. Wachter, J. B.; Chrissafis, K.; Petkov, V.; Malliakas, C. D.; Bilc, D.; Kyratsi, Th.; Paraskevopoulos, K. M.; Mahanti, S. D.; Torbrügge, T.; Eckert, H.; Kanatzidis, M. G. J. Solid State Chem. 2007, 180, 420-431.
40. Canlas, C. G.; Kanatzidis, M. G.; Weliky, D. P. Inorg. Chem. 2003, 42, 3399-3405.
41. Schmedt auf der Günne, J.; Eckert, H. Chem. - Eur. J. 1998, 9, 1762-1767.
42. 4 can be found in the Supporting Information.
43. SHELXTL version 5; Bruker Analytical X-ray Instruments Inc.: Madison, WI, 1998.
44. Petricek, V.; Dusek, M.; Palatinus, L. 2000. Jana2000. The crystallography computing system; Institute of Physics: Praha, Czech Republic, 2000.
45. (a) Wendlandt, W. W.; Hecht, H. G. Reflectance Spectroscopy; Interscience Publishers: New York, 1966.
46. (b) Kotum, G. Reflectance Spectroscopy; Springer-Verlag: New York, 1969.
47. (c) Tandon, S. P.; Gupta, J. P. Phys. Status Solidi 1970, 38, 363-367.
48. Canlas, C. G.; Mathukumaran, R. B.; Kanatzidis, M. G.; Weliky, D. P. Solid State Nucl. Magn. Reson. 2003, 24, 110-122.
49. Breshears, J. D.; Kanatzidis, M. G. J. Am. Chem. Soc. 2000, 122, 7839-7840.
50. Kanatzidis, M. G.; Sutorik, A. C. Prog. Inorg. Chem. 1995, 43, 151-265.
51. A reaction with the stoichiometric ratio of Tl/Bi/6P/14S was subsequently found to produce compound III as the sole crystalline product. Attempts to remove the glassy impurities by washing with ethylene-diamine, methanol, and ether resulted in a product that was amorphous by powder X-ray diffraction, suggesting that compound III decomposes under such conditions.
52. Gave, M. A.; Bilc, D.; Mahanti, S. D.; Breshears, J. D.; Kanatzidis, M. G. Inorg. Chem. 2005, 44, 5293-5303.
53. McCarthy, T. J.; Kanatzidis, M. G. J. Chem. Soc., Chem. Commun. 1994, 1089-1090.
54. Chen, J. H.; Dorhout, P. K.; Ostenson, J. E. Inorg. Chem. 1996, 35, 5627-5633.
55. Crystal twinning in a merohedral fashion was a major difficulty in solving and refining the structure. Data sets on several crystals were collected but could not be successfully refined, as large residual electron densities remained. Careful examination of the reciprocal lattice revealed a second twin domain rotated 180° along the a axis. When the corresponding twin law of (Formula Presented) was applied, the R value dropped from 28% to 5%. This led to small residuals in the electron density map and with a twin fraction of 43.2-(1)%.
56. Greenwood, N. N.; Earnshaw, A. Chemistry of the Elements; Butterworth Heinemann: Oxford, U.K., 1998; pp 75 and 222.
57. Regelsky, G. Ph.D. Thesis, University of Munster, Minister, Germany, 2000.
58. Bryce, D. L.; Wasylishen, R. E. J. Mol. Struct. 2002, 602-603, 463-472.
59. Walther, B.; Bauer, S. Organomet. Chem. 1977, 142, 177-184.
60. A mathematical deconvolution of the spectrum was only successful when the feature furthest downfield was modeled by two closely spaced peaks.