-
2
-
-
33845585240
-
-
(a) Schaub, T.; Backes, M.; Radius, U. J. Am. Chem. Soc. 2006, 128, 15964.
-
(2006)
J. Am. Chem. Soc
, vol.128
, pp. 15964
-
-
Schaub, T.1
Backes, M.2
Radius, U.3
-
3
-
-
33646354884
-
-
(b) Guo, H.; Kong, F.; Kanno, K.; He, J.; Nakajima, K.; Takahashi, T. Organometallics 2006, 25, 2045.
-
(2006)
Organometallics
, vol.25
, pp. 2045
-
-
Guo, H.1
Kong, F.2
Kanno, K.3
He, J.4
Nakajima, K.5
Takahashi, T.6
-
4
-
-
23844554544
-
-
(c) Steffen, A.; Sladek, M. I.; Braun, T.; Neumann, B.; Stammler, H.-G. Organometallics 2005, 24, 4057.
-
(2005)
Organometallics
, vol.24
, pp. 4057
-
-
Steffen, A.1
Sladek, M.I.2
Braun, T.3
Neumann, B.4
Stammler, H.-G.5
-
6
-
-
29844439845
-
-
(e) Yoshikai, N.; Mashima, H.; Nakamura, E. J. Am. Chem. Soc. 2005, 127, 17978.
-
(2005)
J. Am. Chem. Soc
, vol.127
, pp. 17978
-
-
Yoshikai, N.1
Mashima, H.2
Nakamura, E.3
-
7
-
-
0037620634
-
-
(f) Terao, J.; Ikumi, A.; Kuniyasu, H.; Kambe, N. J. Am. Chem. Soc. 2003, 125, 5646.
-
(2003)
J. Am. Chem. Soc
, vol.125
, pp. 5646
-
-
Terao, J.1
Ikumi, A.2
Kuniyasu, H.3
Kambe, N.4
-
11
-
-
0037505267
-
-
(c) Yus, M.; Herrera, R. P.; Guijarro, A. Tetrahedron Lett. 2003, 44, 5025.
-
(2003)
Tetrahedron Lett
, vol.44
, pp. 5025
-
-
Yus, M.1
Herrera, R.P.2
Guijarro, A.3
-
12
-
-
0025144229
-
-
(d) Namavari, M.; Satyamurthy, N.; Phelps, M. E.; Barrio, J. R. Tetrahedron Lett. 1990, 31, 4973.
-
(1990)
Tetrahedron Lett
, vol.31
, pp. 4973
-
-
Namavari, M.1
Satyamurthy, N.2
Phelps, M.E.3
Barrio, J.R.4
-
13
-
-
37049069368
-
-
(e) Landini, D.; Albanese, D.; Mottadelli, S.; Penso, M. J. Chem. Soc., Perkin Trans. 1 1992, 2309.
-
(1992)
J. Chem. Soc., Perkin Trans. 1
, pp. 2309
-
-
Landini, D.1
Albanese, D.2
Mottadelli, S.3
Penso, M.4
-
14
-
-
34247279249
-
-
(f) Begum, S. A.; Terao, J.; Kambe, N. Chem. Lett. 2007, 36, 196.
-
(2007)
Chem. Lett
, vol.36
, pp. 196
-
-
Begum, S.A.1
Terao, J.2
Kambe, N.3
-
15
-
-
0002968439
-
In Organo-Fluorine Compounds; Baasner, B
-
Hagemann, H, Tatlow, J. C, Eds, /; Houben-Weyl: Stuttgart, Germany
-
Paleta, O. In Organo-Fluorine Compounds; Baasner, B., Hagemann, H., Tatlow, J. C., Eds.; Methods of Organic Chemistry, Vol. E 10b/Part 2; Houben-Weyl: Stuttgart, Germany, 2000: p 306.
-
(2000)
Methods of Organic Chemistry
, vol.E 10b
, Issue.PART 2
, pp. 306
-
-
Paleta, O.1
-
16
-
-
34247490216
-
-
Richmond, T. G. In Activation of Unreactive Bonds and Organic Synthesis; Murai, S., Ed.; Topics in Organometallic Chemistry, 3; Springer: Berlin, Germany, 1999; p 243.
-
(a) Richmond, T. G. In Activation of Unreactive Bonds and Organic Synthesis; Murai, S., Ed.; Topics in Organometallic Chemistry, Vol. 3; Springer: Berlin, Germany, 1999; p 243.
-
-
-
-
17
-
-
0010820910
-
-
(b) Kiplinger, J. L.; Richmond, T. G.; Osterberg, C. E. Chem. Rev. 1994, 94, 373.
-
(1994)
Chem. Rev
, vol.94
, pp. 373
-
-
Kiplinger, J.L.1
Richmond, T.G.2
Osterberg, C.E.3
-
18
-
-
0001677496
-
-
(c) Burdeniuc, J.; Jedlicka, B.; Crabtree, R. H. Chem. Ber. 1997, 130, 145.
-
(1997)
Chem. Ber
, vol.130
, pp. 145
-
-
Burdeniuc, J.1
Jedlicka, B.2
Crabtree, R.H.3
-
19
-
-
0036860845
-
-
Alonso, F.; Beletskaya, I. P.; Yus, M. Chem. Rev. 2002, 102, 4009.
-
(2002)
Chem. Rev
, vol.102
, pp. 4009
-
-
Alonso, F.1
Beletskaya, I.P.2
Yus, M.3
-
22
-
-
0028869192
-
-
(b) Roehl, C. M.; Boglu, D.; Bruehl, C.; Moortgat, G. K. Geophys. Res. Lett. 1995, 22, 815.
-
(1995)
Geophys. Res. Lett
, vol.22
, pp. 815
-
-
Roehl, C.M.1
Boglu, D.2
Bruehl, C.3
Moortgat, G.K.4
-
27
-
-
19744376115
-
-
Vela, J.; Smith, J. M.; Yu, Y.; Ketterer, N. A.; Flaschenriem, C. J.; Lachicotte, R. J.; Holland, P. L. J. Am. Chem. Soc. 2005, 127, 7857. See also:
-
(d) Vela, J.; Smith, J. M.; Yu, Y.; Ketterer, N. A.; Flaschenriem, C. J.; Lachicotte, R. J.; Holland, P. L. J. Am. Chem. Soc. 2005, 127, 7857. See also:
-
-
-
-
29
-
-
0033829402
-
-
(a) Kraft, B. M.; Lachicotte, R. J.; Jones, W. D. J. Am. Chem. Soc. 2000, 122, 8559.
-
(2000)
J. Am. Chem. Soc
, vol.122
, pp. 8559
-
-
Kraft, B.M.1
Lachicotte, R.J.2
Jones, W.D.3
-
30
-
-
0000723874
-
-
(b) Yang, H.; Gao, H.; Angelica, R. J. Organometallics 1999, 18, 2285.
-
(1999)
Organometallics
, vol.18
, pp. 2285
-
-
Yang, H.1
Gao, H.2
Angelica, R.J.3
-
32
-
-
0041508445
-
-
(d) Cellier, P. P.; Spindler, J.-F.; Taillefer, M.; Cristau, H.-J. Tetrahedron Lett. 2003, 44, 7191.
-
(2003)
Tetrahedron Lett
, vol.44
, pp. 7191
-
-
Cellier, P.P.1
Spindler, J.-F.2
Taillefer, M.3
Cristau, H.-J.4
-
33
-
-
0141773672
-
-
Kuhl, S.; Schneider, R.; Fort, Y. Adv. Synth. Catal. 2003, 345, 341. See also:
-
(e) Kuhl, S.; Schneider, R.; Fort, Y. Adv. Synth. Catal. 2003, 345, 341. See also:
-
-
-
-
35
-
-
0034904455
-
-
(g) Yus, M. Synlett 2001, 1197.
-
(2001)
Synlett
, pp. 1197
-
-
Yus, M.1
-
38
-
-
0242611465
-
-
(c) Noveski, D.; Braun, T.; Schulte, M.; Neumann, B.; Stammler, H.-G. Dalton Trans. 2003, 4075.
-
(2003)
Dalton Trans
, pp. 4075
-
-
Noveski, D.1
Braun, T.2
Schulte, M.3
Neumann, B.4
Stammler, H.-G.5
-
39
-
-
0035913924
-
-
(a) Amii, H.; Hatamoto, Y.; Seo, M.; Uneyama, K. J. Org. Chem. 2001, 66, 7216.
-
(2001)
J. Org. Chem
, vol.66
, pp. 7216
-
-
Amii, H.1
Hatamoto, Y.2
Seo, M.3
Uneyama, K.4
-
40
-
-
37049078673
-
-
(b) Saboureau, C.; Troupel, M.; Sibille, S.; Périchon, J. J. Chem. Soc., Chem. Commun. 1989, 1138.
-
(1989)
J. Chem. Soc., Chem. Commun
, pp. 1138
-
-
Saboureau, C.1
Troupel, M.2
Sibille, S.3
Périchon, J.4
-
41
-
-
0344848561
-
-
(c) Clavel, P.; Léger-Lambert, M.-P.; Biran, C.; Serein-Spirau, F.; Bordeau, M.; Roques, N.; Marzouk, H. Synthesis 1999, 829.
-
(1999)
Synthesis
, pp. 829
-
-
Clavel, P.1
Léger-Lambert, M.-P.2
Biran, C.3
Serein-Spirau, F.4
Bordeau, M.5
Roques, N.6
Marzouk, H.7
-
42
-
-
0030975660
-
-
(d) Ferraris, D.; Cox, C.; Anand, R.; Lectka, T. J. Am. Chem. Soc. 1997, 119, 4319.
-
(1997)
J. Am. Chem. Soc
, vol.119
, pp. 4319
-
-
Ferraris, D.1
Cox, C.2
Anand, R.3
Lectka, T.4
-
43
-
-
14844331718
-
-
Scott, V. J.; Celenligil-Cetin, R.; Ozerov, O. V. J. Am. Chem. Soc. 2005, 127, 2852.
-
(2005)
J. Am. Chem. Soc
, vol.127
, pp. 2852
-
-
Scott, V.J.1
Celenligil-Cetin, R.2
Ozerov, O.V.3
-
44
-
-
2942737372
-
-
3 group, also:
-
3 group, also:
-
-
-
-
46
-
-
34247229206
-
-
(c) Fuchibe, K.; Mitomi, K.; Akiyama, T. Chem. Lett. 2007, 36, 24.
-
(2007)
Chem. Lett
, vol.36
, pp. 24
-
-
Fuchibe, K.1
Mitomi, K.2
Akiyama, T.3
-
48
-
-
3042825520
-
-
Typical Procedure. To a DME solution of 1a (308 mg, 1.39 mmol) and NbCl5 (18 mg, 0.068 mmol) was added solid lithium aluminum hydride (208 mg. 5.47 mmol) carefully. The mixture was magnetically stirred and allowed to reflux for 4 h. The reaction was quenched with water at 0°C and a small amount of sodium tartrate (ca. 200 mg) was added for ease of extraction. Products were extracted with ethyl acetate three times and the combined organic layers were dried over anhydrous sodium sulfate. The organic solvents were removed under reduced pressure and purification by column chromatography (SiO2, hexane) gave 2a (218 mg, 1.33 mmol, 96% yield) as a colorless crystal. The 1H and 13C NMR spectra were in complete agreement with those in the literature Tao, B, Boykin, D. W. J. Org. Chem. 2004, 69, 4330
-
13C NMR spectra were in complete agreement with those in the literature (Tao, B.; Boykin, D. W. J. Org. Chem. 2004, 69, 4330).
-
-
-
-
51
-
-
0032913705
-
-
Other methods to access α,α,α-trifluorotoluenes - oxidative substitutions of dithioacid derivatives: (a) Furuta, S.; Kuroboshi, M.; Hiyama, T. Bull. Chem. Soc. Jpn. 1999, 72, 805.
-
Other methods to access α,α,α-trifluorotoluenes - oxidative substitutions of dithioacid derivatives: (a) Furuta, S.; Kuroboshi, M.; Hiyama, T. Bull. Chem. Soc. Jpn. 1999, 72, 805.
-
-
-
-
54
-
-
34247539068
-
-
Kitazume, T.; Ishikawa, N. Chem. Lett. 1982, 11, 137. See also:
-
(d) Kitazume, T.; Ishikawa, N. Chem. Lett. 1982, 11, 137. See also:
-
-
-
-
55
-
-
0026337764
-
-
(e) Su, D.-B.; Duan, J.-X.; Chen, Q.-Y. Tetrahedron Lett. 1991, 32, 7689.
-
(1991)
Tetrahedron Lett
, vol.32
, pp. 7689
-
-
Su, D.-B.1
Duan, J.-X.2
Chen, Q.-Y.3
-
56
-
-
0040523913
-
-
(a) Harvey, P. G.; Smith, F.; Stacey, M.; Tatlow, J. C. J. Appl. Chem. 1954, 4, 319.
-
(1954)
J. Appl. Chem
, vol.4
, pp. 319
-
-
Harvey, P.G.1
Smith, F.2
Stacey, M.3
Tatlow, J.C.4
-
57
-
-
0008495409
-
-
(b) Marsh, F. D.; Farnham, W. B.; Sam, D. J.; Smart, B. E. J. Am. Chem. Soc. 1982, 104, 4680.
-
(1982)
J. Am. Chem. Soc
, vol.104
, pp. 4680
-
-
Marsh, F.D.1
Farnham, W.B.2
Sam, D.J.3
Smart, B.E.4
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