SCOPUS 정보 검색 플랫폼

Synlett

Volumn , Issue 4, 2007, Pages 628-632

Synthesis and spectral properties of a deoxyribose-phthalocyanine conjugate using a Sonogashira coupling reaction

(5) Reddy, Mamidi Ramesh a Shibata, Norio a Yoshiyama, Hideyuki a Nakamura, Shuichi a Toru, Takeshi a

a NAGOYA INSTITUTE OF TECHNOLOGY (Japan)

Author keywords

Nucleosides; Palladium coupling; Photodynamic therapy; Phthalocyanines; Porphyrins

Indexed keywords

DEOXYRIBOSE; PHTHALOCYANINE;

ABSORPTION; ARTICLE; CONJUGATION; FLUORESCENCE ANALYSIS; HYDROPHOBICITY; LIPOPHILICITY; PHOTODYNAMIC THERAPY; PHOTOSENSITIVITY; SONOGASHIRA REACTION; SPECTROSCOPY; SYNTHESIS;

EID: 33947286937 PISSN: 09365214 EISSN: None Source Type: Journal
DOI: 10.1055/s-2007-967977 Document Type: Article

Times cited : (19)

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- Zinc(II) tetrakis({2-Deoxy-3,5-bis[O-(p-toluoyl, α,β- D-ribofuranosyl}ethynyl) phthalocyaninate (4, A mixture of 2 17 (250.0 mg, 0.231 mmol, 316 (524.8 mg, 1.39 mmol, Pd(PPh3)2Cl2 (20 mg) and CuI (10 mg) were dried under vacuum for 1 h. To this mixture, anhyd DMF (2.5 mL) was added followed by Et3N (1 mL) and allowed to stir at r.t. for 72 h. The solvent was removed by evaporation and the crude green solid was purified by silica gel chromatography (EtOAc-hexane, 40:60) to furnish 4 as a blue solid (360.0 mg, 75, IR (KBr, 2954, 2229, 1720, 1611, 1488, 1386, 1271, 1178, 1100, 1020, 837, 752 cm-1; 1H NMR (600MHz, acetone-d6, δ, 8.64 (br s, 8 H, Ar-H, 8.23-8.06 (m, 20 H, Ar-H, 7.42-7.37 (m, 16 H, Ar-H, 5.87-5.56 (m, 8 H, 1′,3′-H, 4.95-4.71 (m, 12 H, 4′,5′-H, 3.11-2.98 m, 8 H, 2′-H, 2.46-2
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61
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