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6
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0000128133
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For some selected recent references on crystal engineering and its applications, see: a
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For some selected recent references on crystal engineering and its applications, see: a) C. B. Aakeröy, A. M. Beatty, Aust. J. Chem. 2001, 54, 409-421;
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16244392094
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0035213446
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25
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0034700565
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The term polycyclitol is derived from polycyclic cyclitols, and as the name suggests, refers to any polyhydroxylated molecule consisting of one or more cyclitol units embedded in a polycyclic carbon framework; see: a
-
The term "polycyclitol" is derived from "polycyclic cyclitols", and as the name suggests, refers to any polyhydroxylated molecule consisting of one or more cyclitol units embedded in a polycyclic carbon framework; see: a) G. Mehta, S. S. Ramesh, Chem. Commun. 2000, 2429-2430;
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25844462855
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25844474648
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a) G. Mehta, S. S. Ramesh, M. K. Bera, Chem. Eur. J. 2003, 9, 2264-2272;
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33
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33846464743
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The details of the synthetic procedures followed in the preparation of the polycyclitols 1-3 have been included in the Exp. Sect.
-
The details of the synthetic procedures followed in the preparation of the polycyclitols 1-3 have been included in the Exp. Sect.
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35
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33846458739
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2 = 0.103, GOF = 1.118 for 724 reflections with I>2σ(I). An OR-TEP plot of 12, with displacement ellipsoids for non-hydrogen atoms drawn at the 50% probability level, is shown below.
-
2 = 0.103, GOF = 1.118 for 724 reflections with I>2σ(I). An OR-TEP plot of 12, with displacement ellipsoids for non-hydrogen atoms drawn at the 50% probability level, is shown below.
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-
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36
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0003147584
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a) A. J. Birch, P. Fitton, D. C. C. Smith, D. E. Steere, A. R. Stelfox, J. Chem. Soc. 1963, 2209-2216;
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39
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33846457630
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0000582084
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0001095772
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30344485672
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0000602940
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a) C. P. Brock, B. Schweizer, J. D. Dunitz, J. Am. Chem. Soc. 1991, 113, 9811-9820;
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1642538255
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d) M. S. Hendi, P. Hooter, R. E. Davis, V. M. Lynch, K. A. Wheeler, Cryst. Growth Des. 2004, 4, 95-101.
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49
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33846446184
-
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int corresponds to subsequent merging of equivalent reflections in this space group.
-
int corresponds to subsequent merging of equivalent reflections in this space group.
-
-
-
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52
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33846463528
-
-
[8a]). The melting point reported corresponds to that of the major polymorph of the te-trol.
-
[8a]). The melting point reported corresponds to that of the major polymorph of the te-trol.
-
-
-
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53
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33846458382
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V6.028, Bruker AXS Inc, Madison, Wisconsin, USA
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a) SMART (V6.028), Bruker AXS Inc., Madison, Wisconsin, USA, 1998;
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(1998)
SMART
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54
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33846406663
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V6.02, Bruker AXS Inc, Madison, Wisconsin, USA
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b) SAINT (V6.02), Bruker AXS Inc., Madison, Wisconsin, USA, 1998.
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SAINT
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55
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0004283942
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University of Göttingen, Germany
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G. M. Sheldrick, SADABS, University of Göttingen, Germany, 1996.
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SADABS
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Sheldrick, G.M.1
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56
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0004150157
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University of Göttingen, Germany
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G. M. Sheldrick, SHELXL97, University of Göttingen, Germany, 1997.
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SHELXL97
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Sheldrick, G.M.1
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