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Volumn 48, Issue 5, 2007, Pages 831-833

Microwave-assisted synthesis of N,N-bis-(2-pyridylmethyl)amine derivatives. Useful ligands in coordination chemistry

Author keywords

[No Author keywords available]

Indexed keywords

ALKENE; COORDINATION COMPOUND; LIGAND; LITHIUM N (PROPONOATE) N,N BIS(2 PYRIDYLMETHYL)AMINE; METHANOL; N (3 AMINOPROPYL) N,N BIS(2 PYRIDYLMETHYL)AMINE; N (3 PROPIONITRILE) N,N BIS(2 PYRIDYLMETHYL)AMINE; N (METHYLPROPANOATE) N,N BIS(2 PYRIDYLMETHYL)AMINE; N (PROPANAMIDE) N,N BIS(2 PYRIDYLMETHYL)AMINE; N,N BIS(2 PYRIDYLMETHYL)AMINE; N,N BIS(2 PYRIDYLMETHYL)AMINE DERIVATIVE; PYRIDINE DERIVATIVE; REAGENT; SOLVENT; UNCLASSIFIED DRUG;

EID: 33845952395     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2006.11.154     Document Type: Article
Times cited : (13)

References (42)
  • 33
    • 0011932271 scopus 로고    scopus 로고
    • Loupy A. (Ed), Wiley-VCH, Weinheim
    • In: Loupy A. (Ed). Microwaves in Organic Synthesis (2003), Wiley-VCH, Weinheim
    • (2003) Microwaves in Organic Synthesis
  • 35
    • 33845925037 scopus 로고    scopus 로고
    • note
    • We have used a monomode microwave CEM Discover, see more details in www.cem.com.
  • 36
    • 33845956584 scopus 로고    scopus 로고
    • note
    • 4 (5 mmol) was added and the mixture was irradiated at 150 W for 30 min. After the usual work-up, the product was obtained in 80% yield as a brown oil.
  • 37
    • 33845950303 scopus 로고    scopus 로고
    • note
    • Microwave-assisted synthesis of PABMPA, MPBMPA, and PNBMPA: In a 10 mL pyrex-ballon, BMPA (5 mmol) and olefin (15 mmol) in MeOH (5 mL) were irradiated at 260 W (time see Table 1). After the mixture was washed with hexane (4 times) and the solvent was eliminated to furnish (yields see Table 1) the compounds as orange oils.
  • 39
    • 33845933412 scopus 로고    scopus 로고
    • note
    • 3OD) δ 36.5, 53.0, 60.7, 123.7, 124.6, 138.7, 146.9, 160.7, 180.9.
  • 41
    • 33845940935 scopus 로고    scopus 로고
    • Carvalho, N. M. F.; Horn, A., Jr.; Antunes, O. A. C. Dalton Trans., submitted for publication.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.