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In our attempts to find a catalyst that was compatible with 6, we tried both unsupported amines (diethylenetriamine and tris(2-aminoethyl)-amine) and supported amines (diethylenetriamine, polystyrene bound; tris(2-aminoethyl)- amine, polystyrene bound; PEI on silica gel; PEI on Amberzyme; and MCM-41 functionalized with W-(2-aminoethyl)-3-aminopropyl groups).
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