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33750344516
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note
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4: C, 48.68; H, 5.08; S, 8.96. Found: C, 48.50; H, 5.30; S, 8.99.
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23
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33750341814
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note
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3, R1 = 0.0467, wR2 = 0.0890. Data collection: Broker Smart CCD system, T = 100 K, Mo Kα (λ = 0.71073 Å), 31 845 reflections, 10 761 unique reflections. The data were corrected for absorption; the structure was solved by direct methods; all non-H atoms were refined anisotropically by full-matrix least squares (SHELKL-97); all H atoms were placed using a riding model and their positions constrained relative to their parent atom.
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24
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33845551954
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