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Volumn 8, Issue 17, 2006, Pages 3685-3688

G-quartet formation from an N2-modified guanosine derivative

Author keywords

[No Author keywords available]

Indexed keywords

DRUG DERIVATIVE; GUANOSINE; N2 (4 N BUTYLPHENYL) 2',3',5' O TRIACETYLGUANOSINE; N2-(4-N-BUTYLPHENYL)-2',3',5'-O-TRIACETYLGUANOSINE;

EID: 33748589997     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol061236w     Document Type: Article
Times cited : (39)

References (32)
  • 17
    • 0021378844 scopus 로고
    • G1 was synthesized by following the literature procedure: Wright, G. E.; Dudycz, Z. W. J. Med. Chem. 1984, 27, 175-181.
    • (1984) J. Med. Chem. , vol.27 , pp. 175-181
    • Wright, G.E.1    Dudycz, Z.W.2
  • 19
    • 33748620766 scopus 로고    scopus 로고
    • note
    • 2 = 0.126 (I > 2σ(I)), GOF = 0.942 was achieved by using 4735 reflections and 353 parameters. All non-hydrogen atoms were refined anisotropically. Details of the crystal structure can be found in the supporting materials.
  • 20
    • 33748596959 scopus 로고    scopus 로고
    • note
    • 1H diffusion NMR spectra were recorded on a Bruker Avance-600 spectrometer using a pulse sequence of longitudinal-eddy-current delay (LED) with bipolar-gradient pulses. The pulse field gradient duration was varied from 4 to 15 ms, and the variable gradient strength (G) was changed from 6 to 350 mT/m. The diffusion period was varied from 50 to 90 ms. A total of 16 transients were collected for each of the 16 or 32 increment steps with a recycle delay of 20 s. The eddy-current delay was set to 5 μs.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.