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Volumn 47, Issue 34, 2006, Pages 6121-6123

Synthesis of the C1-C16 fragment of spirastrellolide A

Author keywords

[No Author keywords available]

Indexed keywords

MACROLIDE; SPIRASTRELLOLIDE A; UNCLASSIFIED DRUG;

EID: 33746289835     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2006.06.067     Document Type: Article
Times cited : (58)

References (33)
  • 8
    • 33746319498 scopus 로고    scopus 로고
    • Wang, C.; Forsyth, C. J., Abstract No. ORGN-414, 229th ACS National Meeting, San Diego, CA, Spring, 2005.
  • 13
    • 0037307278 scopus 로고    scopus 로고
    • For a review on chemistry of spiroketals, see:
    • For a review on chemistry of spiroketals, see:. Mead K.T., and Brewer B.N. Curr. Org. Chem. 7 (2003) 227
    • (2003) Curr. Org. Chem. , vol.7 , pp. 227
    • Mead, K.T.1    Brewer, B.N.2
  • 17
    • 33746282850 scopus 로고    scopus 로고
    • note
    • 3): δ 1.06 (d, J = 7.5 Hz, 3H), 2.45 (ddd, J = 3.5, 4.5, and 16.5 Hz, 1H), 2.50-2.54 (m, 2H), 3.80 (s, 3H), 3.95 (dt, J = 4.5 and 6.5 Hz, 1H), 4.45 ...
  • 22
    • 84941216140 scopus 로고
    • For a review on Sharpless asymmetric epoxidation:. Morrison J.D. (Ed), Academic Press, New York
    • For a review on Sharpless asymmetric epoxidation:. Finn M.G., and Sharpless K.B. In: Morrison J.D. (Ed). Asymmetric Synthesis Vol. 5 (1985), Academic Press, New York 247
    • (1985) Asymmetric Synthesis , vol.5 , pp. 247
    • Finn, M.G.1    Sharpless, K.B.2
  • 23
    • 33746313524 scopus 로고    scopus 로고
    • note
    • The enantiomeric excess was determined by chiral HPLC: the retention times of the two enantiomers were 25.789 (S) min and 27.861 (R) min, respectively. The formation of R-(+)-Mosher's ester gave ≥ 95% de by NMR.
  • 27
    • 0034596069 scopus 로고    scopus 로고
    • For the synthesis of key precursor to 12b, see:
    • For the synthesis of key precursor to 12b, see:. Drouet K.E., and Theodorakis E.A. Chem. Eur. J. 6 (2000) 1987
    • (2000) Chem. Eur. J. , vol.6 , pp. 1987
    • Drouet, K.E.1    Theodorakis, E.A.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.