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note
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See the Supporting Information for procedures and characterization data for all new compounds.
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39
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20444472903
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note
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This excessive manipulation occurred because we had to abandon earlier plans on the synthesis of lactone 13 in which the bis-TBS ether 21 would have been feasible.
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40
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0037955598
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2, see: Thomazeau, C.; Olivier-Bourbigou, H.; Magna, L.; Luts, S.; Gilbert, B. J. Am. Chem. Soc. 2003, 125, 5264.
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41
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20444469030
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note
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On occasion, we also found diene 26, presumably because alcohol 10 is more sterically demanding than the model system.
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