Determination of 2-alkylcyclobutanones with electronic impact and chemical ionization gas chromatography/mass spectrometry (GC/MS) in irradiated foods

Journal of Agricultural and Food Chemistry

Volumn 54, Issue 6, 2006, Pages 1990-1996

  Horvatovich, Peter ^a   Werner, Dalal ^b   Jung, Stephanie ^a   Miesch, Michel ^c   Delincee, Henry ^d   Hasselmann, Claude ^a   Marchioni, Eric ^a  

^a INSTITUT DE RECHERCHES SUBATOMIQUES   (France)

^b Aérial ^*  (France)

^c UNIVERSITÉ LOUIS PASTEUR   (France)

^d FEDERAL RESEARCH INSTITUTE OF NUTRITION AND FOOD   (Germany)

Author keywords

2 alkylcyclobutanone; Chemical ionization; Electronic impact ionization; Irradiated food; Mass spectrometry

Indexed keywords

PERSEA AMERICANA;

ALKANE; CYCLOBUTANE DERIVATIVE; TRIACYLGLYCEROL;

ANIMAL; ARTICLE; AVOCADO; CHEMISTRY; FAT INTAKE; FOOD ANALYSIS; FOOD IRRADIATION; MASS FRAGMENTOGRAPHY; METHODOLOGY; POULTRY; SALMON;

ALKANES; ANIMALS; CYCLOBUTANES; DIETARY FATS; FOOD ANALYSIS; FOOD IRRADIATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; PERSEA; POULTRY; SALMON; TRIGLYCERIDES;

EID: 33645785887     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf0524426     Document Type: Article

References (26)

1. Anonymous. Safety and Nutritional Adequacy of Irradiated Food. World Health Organization: Geneva, Switzerland, 1994.
2. Anonymous. Wholesomeness of Irradiated Food. Report of a joint FAO/IAEA/WHO Expert Committee; World Health Organization: Geneva, Switzerland, Technical Report Series 659, 1981.
3. Anonymous. High-Dose Irradiation: Wholesomeness of Food Irradiated with Doses above 10 kGy. Report of a Joint FAO/ IAEA/WHO Study Group; World Health Organisation: Geneva, Switzerland, Technical Report Series 890, 1999.
4. Anonymous. Foodstuffs. Detection of irradiated food containing bone. Method by ESR spectroscopy. European Committee for Standardization: Brussels, Belgium, EN 1786, 1996.
5. Anonymous. Foodstuffs. Detection of irradiated food containing cellulose. Method by ESR spectroscopy. European Committee for Standardization: Brussels, Belgium, EN 1787, 1996, revised 2000.
6. Anonymous. Foodstuffs. Detection of irradiated food from which silicate minerals can be isolated. Method by thermoluminescence. European Committee for Standardization: Brussels, Belgium, EN 1788, 1996, revised 2001.
7. Anonymous. Foodstuffs. Detection of irradiated food containing fat. Gas chromatographic analysis of hydrocarbons. European Committee for Standardization: Brussels, Belgium, EN 1784, 1996, revised 2003.
8. Anonymous. Foodstuffs. Detection of irradiated food containing fat. Gas chromatographic/mass spectrometric analysis of 2-alkylcyclobutanones. European Committee for Standardization: Brussels, Belgium, EN 1785, 1996, revised 2003.
9. Anonymous. Foodstuffs. Detection of irradiated food containing crystalline sugar by ESR spectroscopy. European Committee for Standardization: Brussels, Belgium, EN 13708, 2001.
10. Anonymous. Foodstuffs. Detection of irradiated food using photostimulated luminescence. European Committee for Standardization: Brussels, Belgium, EN 13751, 2002.
11. Anonymous. Foodstuffs. DNA comet assay for the detection of irradiated foodstuffs - Screening method. European Committee for Standardization: Brussels, Belgium, EN 13784, 2001.
12. Anonymous. Foodstuffs. Detection of irradiated food using direct epifluorescence filter technique/aerobic plate count (DEFT/ APC) - Screening method. European Committee for Standardization: Brussels, Belgium, EN 13783, 2001.
13. Anonymous. Foodstuffs. Microbiological screening method for irradiated food using LAL/GNB procedures. European Committee for Standardization: Brussels, Belgium, EN 14569, 2004.
14. Ndiaye, B.; Jamet, G.; Miesch, M.; Hasselmann, C.; Marchioni, E. 2-Alkylcyclobutanones as markers for irradiated foodstuffs. II. The CEN (European Committee for Standardization) method: Field of application and limit of utilization. Radiat. Phys. Chem. 1999, 55, 437-445.
15. Crone, A. V. J.; Hamilton, J. T. G.; Stevenson, M. H. Effect of storage and cooking on the dose response of 2-dodecylcyclobutanone, a potential marker for irradiated chicken. J. Sci. Food Agr. 1992, 58, 249-252.
16. Crone, A. V. J.; Hand, M. V.; Hamilton, J. T. G.; Sharma, N. D.; Boyd, D. R.; Stevenson, M. H. Synthesis, characterization and use of 2-tetradecylcyclobutanone together with other cyclobutanones as markers of irradiated liquid whole egg. J. Sci. Food Agr. 1993, 62, 361-367.
17. Horvatovich, P.; Miesch, M.; Hasselmann, C.; Marchioni, E. Supercritical fluid extraction of hydrocarbons and 2-alkylcyclobutanones for the detection of irradiated foodstuffs. J. Chromatogr., A 2000, 897, 259-268.
18. Ndiaye, B.; Horvatovich, P.; Miesch, M.; Hasselmann, C.; Marchioni, E. 2-Alkylcyclobutanones as markers for irradiated foodstuffs III. Improvement of the field of application on the EN 1785 method by using silver ion chromatography. J. Chromatogr., A 1999, 858, 109-115.
19. Horvatovich, P.; Miesch, M.; Hasselmann, C.; Marchioni, E. Supercritical fluid extraction for the detection of 2-dodecylcyclobutanone in low dose irradiated plant foods, J. Chromatogr., A 2002, 968, 251-255.
20. Marchioni, E.; Horvatovich, P.; Ndiaye, B.; Miesch, M.; Hasselmann, C. Detection of low amount of irradiated ingredients in non-irradiated precooked meals. Radiat. Phys. Chem. 2002, 63, 447-450.
21. Horvatovich, P.; Miesch, M.; Delincée, H.; Hasselmann, C.; Marchioni, E. Determination of mono-unsaturated alkyl side-chain 2-alkylcyclobutanones in irradiated foods. J. Agric Food Chem. 2005, 53, 5836-5841.
22. Girod, C.; Staub, C. Analysis of drugs of abuse in hair by automated solid-phase extraction, GC/EI/MS and GC ion trap/ CI/MS. Forensic Sci. Int. 2000, 107, 261-271.
23. Miesch, M.; Ndiaye, B.; Hasselmann, C.; Marchioni E. 2- Alkylcyclobutanones as markers for irradiated foodstuffs. I. Synthesis of saturated and unsaturated standards. Radiat. Phys. Chem. 1999, 55, 337-344.
24. Kuntz, F.; Marchioni, E.; Strasser, A. Homogénéisation de la dose déposée dans un produit ionisé aux électrons accélérés. In Proceedings of an International Symposium on High Dose Dosimetry for Radiation Processing, 5-9 November 1990; The International Atomic Energy Agency: Vienna, Austria, 1991; IAEA Report SM 314/30, pp 479-488.
25. Meier, W.; Artho, A.; Nägeli, P. Detection of irradiation of fat-containing foods by on-line LC-GC-MS of alkylcyclobutanones. Mitt. Geb. Lebensm. Unters. Hyg. 1996, 87, 118-122.
26. Souci, S. W.; Fachmann, W.; Kraut, H. Avocado. In Food Composition and Nutrition Tables, 6th ed.; Medpharm Scientific Publishers: Stuttgart, Germany, 2000; pp 949-950.