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The clipping synthesis of rotaxane was employed under ultra-high-pressure, but the effect of pressure was not discussed. For example; J.O. Jeppesen, K.A. Nielsen, J. Perkins, S.A. Vignon, A.D. Fabio, R. Ballardini, M.T. Gandolfi, M. Venturi, V. Balzani, J. Becher, and J.F. Stoddart Chem. Eur. J. 9 2003 2982 3007
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33644987860
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note
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0.
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32
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0037567552
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-2. Even though high-pressure condition accelerates the dissociation of ion pairing, the promotion of the slipping is less than 1.4 times; see: J.W. Jones, and H.W. Gibson J. Am. Chem. Soc. 125 2003 7001 7004
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33644988257
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See Supplementary data.
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See Supplementary data.
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34
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33644988650
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Since TB24C8 has a delicately smaller cavity size, the association rate of 1b and 2b is favorable to monitor; see: Y. Tokunaga, T. Goda, N. Wakamatsu, R. Nakata, and Y. Shimomura Heterocycles 68 2006 5 10
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35
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33644983410
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note
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The thermal reaction of both reactants (50°C, 1 atm, 28 days) afforded 3b in 58% conversion yield. In contrast, the high-pressure conditions (50°C, 2500 atm, 17 days) gave 3b in 66% conversion yield.
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