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47
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32644477752
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note
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The apparatus is commercially available from CEM Microwave Technology and is called 'Voyager'.
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52
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32644469664
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note
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4, the ethyl acetate was removed in vacuo leaving the crude product. That product was then isolated and characterized by comparison of NMR data with that in the literature.
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53
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32644481743
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note
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2/amine catalyst systems used in conjunction with mineral bases.
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