Ecofriendly fast batch synthesis of dioxolanes, dithiolanes, and oxathiolanes without solvent under microwave irradiation

Organic Process Research and Development

Volumn 2, Issue 6, 1998, Pages 428-430

  Perio, Bertrand ^a   Dozias, Marie Joelle ^b   Hamelin, Jack ^a  

^a CNRS   (France)

^b Prolabo   (France)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0032355224     PISSN: 10836160     EISSN: None     Source Type: Journal    
DOI: 10.1021/op980043o     Document Type: Article

References (6)

1. Perio, B.; Dozias, M. J.; Jacquault, P.; Hamelin, J. Tetrahedron Lett. 1997, 38, 7867 and references therein.
2. Commarnot, R.; Didenot, R.; Gardais, J. F. Fr. Demande, 2560529 (Cl. B01J19/12), 06 Sept 1985, Appl. 84/3,496, 02 Mar 1984; Chem. Abstr. 1986, 105, 17442e. Temperature measured by an IR captor: Prolabo, Fr. Patent 62241D, 14669Fr, 23 Dec 1991.
3. Commarnot, R.; Didenot, R.; Gardais, J. F. Fr. Demande, 2560529 (Cl. B01J19/12), 06 Sept 1985, Appl. 84/3,496, 02 Mar 1984; Chem. Abstr. 1986, 105, 17442e. Temperature measured by an IR captor: Prolabo, Fr. Patent 62241D, 14669Fr, 23 Dec 1991.
4. Dauben, J.; Löken, B.; Ringold, H. J. J. Am. Chem. Soc. 1954, 76, 1359.
5. Jolivet-Fouchet, S.; Hamelin, J.; Texier-Boullet, F.; Toupet, L.; Jacquault, P. Tetrahedron 1998, 54, 4561.
6. This apparatus operates with a power between 0 and 300 W, having quartz reactors (8 cm high; 4,2.5, or 1.5 cm diameter) fitted with a stirring device and monitored either in power or in temperature.