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25
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32644484286
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note
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2 (748.48); calcd: C, 44.93; H, 4.04; N, 3.74; enc: C, 45.06; H, 4.12; N, 4.01.
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26
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32644487388
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note
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0 0 0 = 1528, R and wR2 are 0.0376 [I > 2σ(I)] and 0.0966 (all data). Crystallographic data (excluding structure factors) for 3a-c have been deposited with the Cambridge Crystallographic Data Center as supplementary publication numbers 3a : CCDC 291340, 3b : CCDC 291341, 3c : CCDC 291342. Copies of the data may be obtained, free of charge, on application to CCDC, 12 Union Road, Cambridge, CB2 1EZ, UK (fax: +44 (0) 1223 33603 or e-mail: deposit@ccdc.cam.ac. uk ).
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