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25
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29144458640
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note
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In this work, we investigated the direct tosylation of the primary hydroxyl group of methyl arabinoside to avoid using a dithioacetal derivative reported in Ref. 8.
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27
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29144522041
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note
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3S: C, 50.50; H, 7.42. Found: C, 50.20; H, 7.20.
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28
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0037416876
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N. Minakawa, Y. Kato, K. Uetake, D. Kaga, and A. Matsuda Tetrahedron 59 2003 1699 1702
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Minakawa, N.1
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Uetake, K.3
Kaga, D.4
Matsuda, A.5
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29
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29144504267
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note
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5SSi•EtOH: C, 52.72; H, 7.30; N, 9.22. Found: C, 52.50; H, 6.98; N, 9.42.
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30
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29144450151
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note
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5SSi 414.1645, found 414.1595.
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31
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29144518845
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note
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The stereochemistry of the anomeric position of the thioglycosylated products was determined by NOE experiments.
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