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Volumn 7, Issue 6, 2005, Pages 893-897

Plate-to-plate fluorous solid-phase extraction for solution-phase parallel synthesis

Author keywords

[No Author keywords available]

Indexed keywords

FLUOROCARBON;

EID: 28244474559     PISSN: 15204766     EISSN: None     Source Type: Journal    
DOI: 10.1021/cc050061z     Document Type: Article
Times cited : (34)

References (56)
  • 1
    • 0034840718 scopus 로고    scopus 로고
    • For general reviews on fluorous silica gel-based separations, see: (a) Curran, D. P. Synlett 2001, 1488.
    • (2001) Synlett , pp. 1488
    • Curran, D.P.1
  • 2
    • 84958612634 scopus 로고    scopus 로고
    • Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim
    • (b) Curran, D. P. In Handbook of Fluorous Chemistry; Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim, 2004, pp 101-127.
    • (2004) Handbook of Fluorous Chemistry , pp. 101-127
    • Curran, D.P.1
  • 3
    • 84958681225 scopus 로고    scopus 로고
    • Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim
    • For recent reviews on fluorous synthesis, see: (a) Curran, D. P. In Handbook of Fluorous Chemistry; Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim, 2004, pp 128-155.
    • (2004) Handbook of Fluorous Chemistry , pp. 128-155
    • Curran, D.P.1
  • 4
    • 2942545969 scopus 로고    scopus 로고
    • (b) Zhang, W. Chem. Rev. 2004, 104, 2531.
    • (2004) Chem. Rev. , vol.104 , pp. 2531
    • Zhang, W.1
  • 14
    • 13244253108 scopus 로고    scopus 로고
    • Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim
    • (a) Gladysz, J. A.; Emnet, C. In Handbook of Fluorous Chemistry; Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim, 2004, pp 11-23.
    • (2004) Handbook of Fluorous Chemistry , pp. 11-23
    • Gladysz, J.A.1    Emnet, C.2
  • 15
    • 10044238972 scopus 로고    scopus 로고
    • Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim
    • (b) Gladysz, J. A. In Handbook of Fluorous Chemistry; Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim, 2004, pp 41-55.
    • (2004) Handbook of Fluorous Chemistry , pp. 41-55
    • Gladysz, J.A.1
  • 28
    • 12344269144 scopus 로고    scopus 로고
    • Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim
    • For a review on fluorous protecting groups and tags, see: (a) Zhang, W. In Handbook of Fluorous Chemistry; Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim, 2004, pp 222-236.
    • (2004) Handbook of Fluorous Chemistry , pp. 222-236
    • Zhang, W.1
  • 46
    • 28244438401 scopus 로고    scopus 로고
    • note
    • A 2 x 12 SPE manifold is available from Supelco, Fisher, and Waters.
  • 47
  • 48
    • 28244484706 scopus 로고    scopus 로고
    • Argonaut VacMaster-96 SPE manifold, Product no. 121-9600. Cartridges are placed on Isolute array-24 base plate, Product no. 121-9650 (www.argotech.com).
  • 49
    • 28244492760 scopus 로고    scopus 로고
    • Wob-L piston pump, model 2545
    • Wob-L piston pump, model 2545 (www.welchvacuum.com).
  • 50
    • 28244439083 scopus 로고    scopus 로고
    • Whatman 24-well (10 mL) receiving plate, Product no. 7701-51022
    • Whatman 24-well (10 mL) receiving plate, Product no. 7701-51022 (www.whatman.com).
  • 51
    • 28244455827 scopus 로고    scopus 로고
    • FluoroFlash silica gel cartridges, 3 g, 6 mL
    • FluoroFlash silica gel cartridges, 3 g, 6 mL (www.fluorous.com).
  • 52
    • 28244444854 scopus 로고    scopus 로고
    • note
    • Sudan blue II (17354-14-2) from Aldrich.
  • 54
    • 28244447667 scopus 로고    scopus 로고
    • From Argonaut Technologies, Inc.
    • From Argonaut Technologies, Inc.
  • 56
    • 0033575461 scopus 로고    scopus 로고
    • After conducting coupling reactions with F-CDMT, we found literature which indicated that in DCM, the complex of CDMT with NMM could cause NMM demethylation. The relatively low yields and purities listed in Table 3 may relate in part to using DCM as the reaction solvent. For NMM demethylation, see: Kunishima, M.; Kawachi, C.; Iwasaki, F.; Terao, K.; Tani, S. Tetrahedron Lett. 1999, 40, 5327.
    • (1999) Tetrahedron Lett. , vol.40 , pp. 5327
    • Kunishima, M.1    Kawachi, C.2    Iwasaki, F.3    Terao, K.4    Tani, S.5


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.