-
1
-
-
0034840718
-
-
For general reviews on fluorous silica gel-based separations, see: (a) Curran, D. P. Synlett 2001, 1488.
-
(2001)
Synlett
, pp. 1488
-
-
Curran, D.P.1
-
2
-
-
84958612634
-
-
Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim
-
(b) Curran, D. P. In Handbook of Fluorous Chemistry; Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim, 2004, pp 101-127.
-
(2004)
Handbook of Fluorous Chemistry
, pp. 101-127
-
-
Curran, D.P.1
-
3
-
-
84958681225
-
-
Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim
-
For recent reviews on fluorous synthesis, see: (a) Curran, D. P. In Handbook of Fluorous Chemistry; Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim, 2004, pp 128-155.
-
(2004)
Handbook of Fluorous Chemistry
, pp. 128-155
-
-
Curran, D.P.1
-
4
-
-
2942545969
-
-
(b) Zhang, W. Chem. Rev. 2004, 104, 2531.
-
(2004)
Chem. Rev.
, vol.104
, pp. 2531
-
-
Zhang, W.1
-
9
-
-
0037021091
-
-
(g) Tzschucke, C. C.; Markert, C.; Bannwarth, W.; Roller, S.; Hebel, A. Angew. Chem., Int. Ed. 2002, 41, 3964.
-
(2002)
Angew. Chem., Int. Ed.
, vol.41
, pp. 3964
-
-
Tzschucke, C.C.1
Markert, C.2
Bannwarth, W.3
Roller, S.4
Hebel, A.5
-
12
-
-
0035793878
-
-
(c) Luo, Z.; Zhang, Q.; Oderaotoshi, Y.; Curran, D. P. Science 2001, 291, 1766.
-
(2001)
Science
, vol.291
, pp. 1766
-
-
Luo, Z.1
Zhang, Q.2
Oderaotoshi, Y.3
Curran, D.P.4
-
13
-
-
0037019535
-
-
(d) Zhang, W.; Luo, Z.; Chen, C. H.-T.; Curran, D. P. J. Am. Chem. Soc. 2002, 124, 10443.
-
(2002)
J. Am. Chem. Soc.
, vol.124
, pp. 10443
-
-
Zhang, W.1
Luo, Z.2
Chen, C.H.-T.3
Curran, D.P.4
-
14
-
-
13244253108
-
-
Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim
-
(a) Gladysz, J. A.; Emnet, C. In Handbook of Fluorous Chemistry; Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim, 2004, pp 11-23.
-
(2004)
Handbook of Fluorous Chemistry
, pp. 11-23
-
-
Gladysz, J.A.1
Emnet, C.2
-
15
-
-
10044238972
-
-
Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim
-
(b) Gladysz, J. A. In Handbook of Fluorous Chemistry; Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim, 2004, pp 41-55.
-
(2004)
Handbook of Fluorous Chemistry
, pp. 41-55
-
-
Gladysz, J.A.1
-
16
-
-
0000035623
-
-
Curran, D. P.; Hadida, S.; He, M. J. Org. Chem. 1997, 62, 6714.
-
(1997)
J. Org. Chem.
, vol.62
, pp. 6714
-
-
Curran, D.P.1
Hadida, S.2
He, M.3
-
19
-
-
0037071183
-
-
(a) Zhang, W.; Curran, D. P.; Chen, C. H.-T. Tetrahedron 2002, 58, 3871.
-
(2002)
Tetrahedron
, vol.58
, pp. 3871
-
-
Zhang, W.1
Curran, D.P.2
Chen, C.H.-T.3
-
20
-
-
0037013910
-
-
(b) Lindsley, C. W.; Zhao, Z.; Leister, W. H. Tetrahedron Lett. 2002, 43, 4225.
-
(2002)
Tetrahedron Lett.
, vol.43
, pp. 4225
-
-
Lindsley, C.W.1
Zhao, Z.2
Leister, W.H.3
-
21
-
-
0037009729
-
-
(c) Lindsley, C. W.; Zhao, Z.; Leister, W. H.; Strauss, K. A. Tetrahedron Lett. 2002, 43, 6319.
-
(2002)
Tetrahedron Lett.
, vol.43
, pp. 6319
-
-
Lindsley, C.W.1
Zhao, Z.2
Leister, W.H.3
Strauss, K.A.4
-
22
-
-
0037416843
-
-
(d) Zhang, W.; Chen, C. H.-T.; Nagashima, T. Tetrahedron Lett. 2003, 44, 2065.
-
(2003)
Tetrahedron Lett.
, vol.44
, pp. 2065
-
-
Zhang, W.1
Chen, C.H.-T.2
Nagashima, T.3
-
26
-
-
0037124435
-
-
(c) Lindsley, C. W.; Zhao, Z.; Newton, R. C.; Leister, W. H.; Strauss, K. A. Tetrahedron Lett. 2002, 43, 4467-4470.
-
(2002)
Tetrahedron Lett.
, vol.43
, pp. 4467-4470
-
-
Lindsley, C.W.1
Zhao, Z.2
Newton, R.C.3
Leister, W.H.4
Strauss, K.A.5
-
27
-
-
2442445175
-
-
(d) Zhang, W.; Chen, C. H.-T.; Lu, Y.; Nagashima, T. Org. Lett. 2004, 6, 1473-1476.
-
(2004)
Org. Lett.
, vol.6
, pp. 1473-1476
-
-
Zhang, W.1
Chen, C.H.-T.2
Lu, Y.3
Nagashima, T.4
-
28
-
-
12344269144
-
-
Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim
-
For a review on fluorous protecting groups and tags, see: (a) Zhang, W. In Handbook of Fluorous Chemistry; Gladysz, J. A., Curran, D. P., Horvath, I. T., Eds.; Wiley-VCH: Weinheim, 2004, pp 222-236.
-
(2004)
Handbook of Fluorous Chemistry
, pp. 222-236
-
-
Zhang, W.1
-
30
-
-
0035874698
-
-
(a) Luo, Z. Y.; Williams, J.; Read, R. W.; Curran, D. P J. Org. Chem. 2001, 66, 4261.
-
(2001)
J. Org. Chem.
, vol.66
, pp. 4261
-
-
Luo, Z.Y.1
Williams, J.2
Read, R.W.3
Curran, D.P.4
-
31
-
-
0037603321
-
-
(b) Curran, D. P.; Amatore, M.; Campbell, M.; Go, E.; Guthrie, D.; Luo, Z. J. Org. Chem. 2003, 68, 4643.
-
(2003)
J. Org. Chem.
, vol.68
, pp. 4643
-
-
Curran, D.P.1
Amatore, M.2
Campbell, M.3
Go, E.4
Guthrie, D.5
Luo, Z.6
-
38
-
-
2442445175
-
-
(i) Zhang, W.; Chen, C. H-T.; Lu, Y.; Nagashima, T. Org. Lett. 2004, 6, 1473.
-
(2004)
Org. Lett.
, vol.6
, pp. 1473
-
-
Zhang, W.1
Chen, C.H.-T.2
Lu, Y.3
Nagashima, T.4
-
41
-
-
4143081635
-
-
(l) Villard, A.-L.; Warrington, B. H.; Ladlow, M. J. Comb. Chem. 2004, 6, 611.
-
(2004)
J. Comb. Chem.
, vol.6
, pp. 611
-
-
Villard, A.-L.1
Warrington, B.H.2
Ladlow, M.3
-
42
-
-
12344302489
-
-
(m) McAllister, L. A.; McCormick, R. A.; Brand, S.; Procter, D. J. Angew. Chem., Int. Ed. 2005, 44, 452.
-
(2005)
Angew. Chem., Int. Ed.
, vol.44
, pp. 452
-
-
McAllister, L.A.1
McCormick, R.A.2
Brand, S.3
Procter, D.J.4
-
43
-
-
0242710897
-
-
(a) de Visser, P. C.; van Helden, M.; Filtppov, D. V.; van der Marel, G. A.; Drijfhout, J. W.; van Boom, J. H.; Noort, D.; Overkleeft, H. S. Tetrahedron Lett. 2003, 44, 9013.
-
(2003)
Tetrahedron Lett.
, vol.44
, pp. 9013
-
-
De Visser, P.C.1
Van Helden, M.2
Filtppov, D.V.3
Van Der Marel, G.A.4
Drijfhout, J.W.5
Van Boom, J.H.6
Noort, D.7
Overkleeft, H.S.8
-
45
-
-
21444443047
-
-
(c) Brittain, S. M.; Ficarro, S. B.; Brock, A.; Peters, E. C. Nat. Biotech. 2005, 23, 463.
-
(2005)
Nat. Biotech.
, vol.23
, pp. 463
-
-
Brittain, S.M.1
Ficarro, S.B.2
Brock, A.3
Peters, E.C.4
-
46
-
-
28244438401
-
-
note
-
A 2 x 12 SPE manifold is available from Supelco, Fisher, and Waters.
-
-
-
-
47
-
-
0034648035
-
-
For a special issue of SPE for sample preparations, see: Poole, C. F.; Wilson, I. D. J. Chromatogr., A 2000, 885, 1-471.
-
(2000)
J. Chromatogr., A
, vol.885
, pp. 1-471
-
-
Poole, C.F.1
Wilson, I.D.2
-
48
-
-
28244484706
-
-
Argonaut VacMaster-96 SPE manifold, Product no. 121-9600. Cartridges are placed on Isolute array-24 base plate, Product no. 121-9650 (www.argotech.com).
-
-
-
-
49
-
-
28244492760
-
-
Wob-L piston pump, model 2545
-
Wob-L piston pump, model 2545 (www.welchvacuum.com).
-
-
-
-
50
-
-
28244439083
-
-
Whatman 24-well (10 mL) receiving plate, Product no. 7701-51022
-
Whatman 24-well (10 mL) receiving plate, Product no. 7701-51022 (www.whatman.com).
-
-
-
-
51
-
-
28244455827
-
-
FluoroFlash silica gel cartridges, 3 g, 6 mL
-
FluoroFlash silica gel cartridges, 3 g, 6 mL (www.fluorous.com).
-
-
-
-
52
-
-
28244444854
-
-
note
-
Sudan blue II (17354-14-2) from Aldrich.
-
-
-
-
54
-
-
28244447667
-
-
From Argonaut Technologies, Inc.
-
From Argonaut Technologies, Inc.
-
-
-
-
55
-
-
23844483282
-
-
Nagashima, T.; Petro, M.; Lu, Y.; Zhang, W. Tetrahedron Lett. 2005, 46, 6585.
-
(2005)
Tetrahedron Lett.
, vol.46
, pp. 6585
-
-
Nagashima, T.1
Petro, M.2
Lu, Y.3
Zhang, W.4
-
56
-
-
0033575461
-
-
After conducting coupling reactions with F-CDMT, we found literature which indicated that in DCM, the complex of CDMT with NMM could cause NMM demethylation. The relatively low yields and purities listed in Table 3 may relate in part to using DCM as the reaction solvent. For NMM demethylation, see: Kunishima, M.; Kawachi, C.; Iwasaki, F.; Terao, K.; Tani, S. Tetrahedron Lett. 1999, 40, 5327.
-
(1999)
Tetrahedron Lett.
, vol.40
, pp. 5327
-
-
Kunishima, M.1
Kawachi, C.2
Iwasaki, F.3
Terao, K.4
Tani, S.5
|