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Volumn 43, Issue 25, 2002, Pages 4467-4470

A general Staudinger protocol for solution-phase parallel synthesis

Author keywords

Azides; Combinatorial chemistry; Reduction

Indexed keywords

AMINE; TRIPHENYLPHOSPHINE;

EID: 0037124435     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(02)00827-4     Document Type: Article
Times cited : (47)

References (20)
  • 6
    • 84991420133 scopus 로고    scopus 로고
    • a and steric hindrance of the amine, 6, being generated and failed to be general. With SCX SPE, we were limited to unhindered basic amines. For example, anilines, pyridines and many tertiary amines failed to be retained; therefore, pure compounds were not obtained
  • 7
    • 84991430675 scopus 로고    scopus 로고
    • 3 (cat#: 01-64-0347) had a loading of 0.48 mmol/g
  • 9
    • 84991420135 scopus 로고    scopus 로고
    • Conversion and purity were determined by analytical LCMS and NMR analysis
  • 11
    • 84991411747 scopus 로고    scopus 로고
  • 16
    • 84991415518 scopus 로고    scopus 로고
    • note
  • 17
    • 84991419096 scopus 로고    scopus 로고
    • 2O/0.1%TFA, 4 min gradient) >98% pure by UV (214 nm) and 100% pure by ELSD, 744.2 (M+1)
  • 18
    • 84991427378 scopus 로고    scopus 로고
    • 31P NMR recorded at 122.7 MHz on a Varian VXR-300 spectrometer
  • 19
    • 84991430017 scopus 로고    scopus 로고
    • note
  • 20
    • 84991430679 scopus 로고    scopus 로고
    • note


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.