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xO (x ranging from 0.01 to 0.1) powder (see ref 16). The CNTs were annealed at 600°C in a graphitization furnace under an argon flow of 3 L/min; a heating rate of 13°C/min was used before 15 min of resident time at the determined temperature. Batch II: The CNTs were produced by catalytic decomposition of acetylene on an Fe-Mo/NaY zeolite catalyst at 700°C (see ref 17).
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The TEM images in Figure 1 were made with a Philips CM300 FEG microscope operating at 300 kV. For the TEM sample preparation, CNTs were dispersed in isopropanol and sonicated for 5 min. A droplet of CNT suspension was then put on a Cu TEM grid with a holey C-film.
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-1 were used. The force constant was calibrated directly prior to the measurement.
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In the case of an individual nanotube, neglecting the inner diameter leads to the underestimation of the bending modulus by 10%.
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B = Y is readily established.
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