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22
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2542511376
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note
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-3, λ(Mo Kα) = 0.710 73 Å, 6445 reflections (2.5 < θ < 25°) were collected at 293 K, 4567 unique reflections and 3491reflections with I > 3σ(I) used in refinements, 253 parameters, R = 0.033, Rw = 0.042, GOF = 0.97.
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23
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0026588471
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Spectroscopic analyses were in agreement with reported data for compound 16, previously synthesized from tetraformylTTF and the corre-sponding phosphonium salt in a Wittig reaction: Sallé, M.; Gorgues, A.; Jubault, M.; Boubekeur, K.; Batail, P. Tetrahedron 1992, 48, 3081.
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Sallé, M.1
Gorgues, A.2
Jubault, M.3
Boubekeur, K.4
Batail, P.5
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24
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0028302223
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Garín, J.; Orduna, J.; Uriel, S.; Moore, A. J.; Bryce, M. R.; Wegener, S.; Yufit, D. S.; Howard, J. A. K. Synthesis 1994, 489.
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Howard, J.A.K.8
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25
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2542631766
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note
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Studies of the pentameric TTF resulting from the HWE reaction between tetraphosphonate 11 and aldehyde 17 will be reported later.
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26
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2542544863
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note
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The number of electrons was determined by thin-layer cyclic voltammetry (TLCV) using 2,3-dichloro-1,4-naphthoquinone as the one-electron standard reference.
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27
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0002593586
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Farges, J.-P., Ed.; Marcel Dekker: New York, Chapter 3
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Becker, J.Y.2
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Takimiya, K.1
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Otsubo, T.5
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31
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0034836364
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Krief, P.9
Khodorkovsky, V.10
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32
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34
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2542615045
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note
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All the results obtained by chemical oxidation were also confirmed by time-resolved spectroelectrochemistry coupled to cyclic voltammetry.
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