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3CN) at room temperature when oxidizing a relatively concentrated solution of TTF (ca. 5 mM). This absorption disappeared at low concentration (ca. 0.5 mM) but increased on a thin film of TTF-derivatized polythiophenes, confirming its assignment to a dimer.
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3CN) at room temperature when oxidizing a relatively concentrated solution of TTF (ca. 5 mM). This absorption disappeared at low concentration (ca. 0.5 mM) but increased on a thin film of TTF-derivatized polythiophenes, confirming its assignment to a dimer
-
3CN) at room temperature when oxidizing a relatively concentrated solution of TTF (ca. 5 mM). This absorption disappeared at low concentration (ca. 0.5 mM) but increased on a thin film of TTF-derivatized polythiophenes, confirming its assignment to a dimer.
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Review on bis-TTFs: Otsubo, T.; Aso, Y.; Takimiya, K. Adv. Mater. 1996, 8, 203.
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0001393574
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The ability of very short bridges to facilitate the formation of an intramolecular MV complex has also been observed in the crystal structure of the radical cation salt of a TTF twin donor containing one methylenedithio bridging unit: Izuoka, A.; Kumai, R.; Sugawara, T. Chem. Lett. 1992, 285. Oxidation of mono-bridged bis-TTF derivatives has also been studied by Cava and co-workers: Sudmale, I. V.; Tormos, G. V.; Khodorkovsky, V. Y.; Edzina, A. S.; Neilands, O. J.; Cava, M. P. J. Org. Chem. 1993, 58, 1355.
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Izuoka, A.1
Kumai, R.2
Sugawara, T.3
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12
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0001393574
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The ability of very short bridges to facilitate the formation of an intramolecular MV complex has also been observed in the crystal structure of the radical cation salt of a TTF twin donor containing one methylenedithio bridging unit: Izuoka, A.; Kumai, R.; Sugawara, T. Chem. Lett. 1992, 285. Oxidation of mono-bridged bis-TTF derivatives has also been studied by Cava and co-workers: Sudmale, I. V.; Tormos, G. V.; Khodorkovsky, V. Y.; Edzina, A. S.; Neilands, O. J.; Cava, M. P. J. Org. Chem. 1993, 58, 1355.
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Sudmale, I.V.1
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Cava, M.P.6
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14
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37049077707
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(a) Becher, J.; Lau, J.; Leriche, P.; Mørk, P.; Svenstrup, N. J. Chem. Soc., Chem. Commun. 1994, 2715.
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16
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0029874149
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(c) Simonsen, K. B.; Svenstrup, N.; Lau, J.; Simonsen, O.; Mørk, P.; Kristensen, G. J.; Becher, J. Synthesis 1996, 3, 407.
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0001523842
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Becher, J.1
Li, Z.-T.2
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Svenstrup, N.4
Lau, J.5
Nielsen, M.B.6
Leriche, P.7
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18
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0342663322
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note
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2 (1101.79); C, 43.61; H, 4.39; N, 2.54; S, 46.56. Found: C, 43.64; H, 4.36; N, 2.49; S, 46.71.
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-
-
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19
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0342663323
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note
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2/cyclohexane 1:3], yielding 4a (1.01 g, 72%) as an orange glass.
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20
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0033577823
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Simonsen, K. B.; Svenstrup, N.; Lau, J.; Thorup, N.; Becher, J. Angew. Chem., Int. Ed. Engl. 1999, 38, 1417.
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Simonsen, K.B.1
Svenstrup, N.2
Lau, J.3
Thorup, N.4
Becher, J.5
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21
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0343533564
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note
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2 (1468.68): C, 49.48; H, 5.01; N, 3.81. Found: C, 49.51; H, 4.94; N, 3.83.
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-
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22
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33748212323
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Alternative procedures for preparing TTF-belts: (a) Adam, M.; Enkelmann, V.; Räder, H.-J.; Röhrich, J.; Müllen, K. Angew. Chem., Int. Ed. Engl. 1992, 31, 309. (b) Matsuo, K.; Takimiya, K.; Aso, Y.; Otsubo, T.; Ogura, F. Chem. Lett. 1995, 523.
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Adam, M.1
Enkelmann, V.2
Räder, H.-J.3
Röhrich, J.4
Müllen, K.5
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23
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33748212323
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Alternative procedures for preparing TTF-belts: (a) Adam, M.; Enkelmann, V.; Räder, H.-J.; Röhrich, J.; Müllen, K. Angew. Chem., Int. Ed. Engl. 1992, 31, 309. (b) Matsuo, K.; Takimiya, K.; Aso, Y.; Otsubo, T.; Ogura, F. Chem. Lett. 1995, 523.
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Chem. Lett.
, pp. 523
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Matsuo, K.1
Takimiya, K.2
Aso, Y.3
Otsubo, T.4
Ogura, F.5
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24
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0343969370
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note
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+).
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-
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25
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33750542705
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(a) Li, Z.-T.; Stein, P. C.; Svenstrup, N.; Lund, K. H.; Becher, J. Angew. Chem., Int. Ed. Engl. 1995, 34, 2524.
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Angew. Chem., Int. Ed. Engl.
, vol.34
, pp. 2524
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Li, Z.-T.1
Stein, P.C.2
Svenstrup, N.3
Lund, K.H.4
Becher, J.5
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26
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0000647283
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(b) Li, Z.-T.; Stein, P. C.; Becher, J.; Jensen, D.; Mørk, P.; Svenstrup, N. Chem. Eur. J. 1996, 2, 624.
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Chem. Eur. J.
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Li, Z.-T.1
Stein, P.C.2
Becher, J.3
Jensen, D.4
Mørk, P.5
Svenstrup, N.6
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28
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0347397243
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(d) Nielsen, M. B.; Li, Z.-T.; Becher, J. J. Mater. Chem. 1997, 7, 1175.
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(1997)
J. Mater. Chem.
, vol.7
, pp. 1175
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-
Nielsen, M.B.1
Li, Z.-T.2
Becher, J.3
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29
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33845282499
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For studies on acid-catalyzed isomerization of TTF, see: Souizi, A.; Robert, A. J. Org. Chem. 1987, 52, 1610.
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J. Org. Chem.
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Souizi, A.1
Robert, A.2
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30
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0343969368
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note
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5Cl at 276 K. A yellow single crystal of 4b was selected by optical examination. X-ray data were collected at 294 K on an Enraf Nonius Mach 3 four circles diffractometer equipped with a graphite monochromator utilizing Mo Kα radiation (λ = 0.71073 Å). The structure was solved by direct methods (SIR) using MoIEN package programs [Crystal Structure Analysis: Molecular Enraf-Nonius (MoIEN), 1990. Delft Instruments X-ray Diffraction. B. V. Rontnenweg 1, 2624 BD Delft, The Netherlands] and was refined on F by the full-matrix least-squares method using anisotropic thermal parameters for S and isotropic ones for C. No absorption corrections were made. The H atoms were included in the calculation without refinement.
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-
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32
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0343533562
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-1 was used
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-1 was used.
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-
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33
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0342663320
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6 (0.4 M) was used as the supporting electrolyte in all of the experiments. For more details, see: Gaillard, F.; Levillain, E. J. Electroanal. Chem. 1995, 398, 11.
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J. Electroanal. Chem.
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, pp. 11
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Gaillard, F.1
Levillain, E.2
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34
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0000980709
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3CN. This enhanced ability of TMT-TTF relative to TTF to form dimers is probably a result of the four extra sulfur atoms which can facilitate dimer formation by favorable S-S interactions.
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(1974)
J. Am. Chem. Soc.
, vol.96
, pp. 945
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Moses, P.R.1
Chambers, J.Q.2
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35
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0001241330
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3CN. This enhanced ability of TMT-TTF relative to TTF to form dimers is probably a result of the four extra sulfur atoms which can facilitate dimer formation by favorable S-S interactions.
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(1985)
Zh. Org. Khim.
, vol.21
, pp. 2009
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Kreicberga, J.1
Neilands, O.2
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36
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0033615314
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ESR experiments were run on a Bruker ESP 300 spectrometer driven by the Bruker ESP 1600 computer program. Using this same equipment, similar experiments probing dimer formation of tetrathienylenevinylenes were carried out earlier: Levillain, E.; Roncali, J. J. Am. Chem. Soc. 1999, 121, 8760.
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J. Am. Chem. Soc.
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Levillain, E.1
Roncali, J.2
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37
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0343097619
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23 measured an ESR signal in their studies of the TMT-TTF radical cation. However, in light of their deviating spectral data, we question if their solution did, in fact, contain the pure and fully mono-oxidized TMT-TTF
-
23 measured an ESR signal in their studies of the TMT-TTF radical cation. However, in light of their deviating spectral data, we question if their solution did, in fact, contain the pure and fully mono-oxidized TMT-TTF.
-
-
-
-
38
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0343533561
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-
max = 706 nm), which is in good agreement with the spectroelectrochemical result, whereas neither of our experiments substantiate the two high-energy absorptions
-
max = 706 nm), which is in good agreement with the spectroelectrochemical result, whereas neither of our experiments substantiate the two high-energy absorptions.
-
-
-
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39
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0347076407
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Phillips, T. E.; Kistenmacher, T. J.; Ferraris, J. P.; Cowan, D. O. J. Chem. Soc., Chem. Commun. 1973, 471.
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40
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0000028804
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(a) Akutagawa, T.; Abe, Y.; Nezu, Y.; Nakamura, T.; Kataoka, M.; Yamanaka, A.; Inoue, K.; Inabe, T.; Christensen, C. A.; Becher, J. Inorganic Chem. 1998, 37, 2330.
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41
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0034367548
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(b) Akutagawa, T.; Abe, Y.; Hasegawa, T.; Nakamura, T.; Inabe, T.; Christensen, C. A.; Becher, J. Chem. Lett. 2000, 132.
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Christensen, C.A.1
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43
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0342663319
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6 as the supporting electrolyte. Counter and working electrodes were made of Pt, and the reference electrode was Ag/AgCl
-
6 as the supporting electrolyte. Counter and working electrodes were made of Pt, and the reference electrode was Ag/AgCl.
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44
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