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11B NMR spectra (3: δ = 47.7 ppm, 4: δ = 62.5 ppm).
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2 = 0.0505, 6339 independent reflections [2θ ≤ 52.12°] and 325 parameters. Details of the X-ray crystal structure determination can be found in the Supporting Information. CCDC-263858 (3) and CCDC-263859 (4) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from the Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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