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24644448066
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note
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It should be mentioned that the available mechanistic information does not allow us to rule alternative mechanisms out. Notably, the formation of allyliron species (by allylic C-H activation) instead of the putative metallacyclic intermediates could also explain the observed results.
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25
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0000200235
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For ene-type reactions of ene/diene substrates using iron catalysts formed in situ, see: (a) Takacs, J. M.; Newsome, P. W.; Kuehn, C.; Takusagawa, F. Tetrahedron 1990, 46, 5507.
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and literature cited therein
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(d) [Rh]: Lei, A.; He, M.; Zhang, X. J. Am. Chem. Soc. 2002, 124, 8198 and literature cited therein.
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Lei, A.1
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39
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24644499263
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note
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For the assignment of the stereochemistry, cf. Supporting Information.
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40
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0001760155
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Precedence for the stereochemical switch from cis to trans on going to larger ring sizes is found in organopalladium chemistry, cf: Trost, B. M.; Grese, T. A. J. Am. Chem. Soc. 1991, 113, 7363.
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Trost, B.M.1
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41
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24644496955
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note
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GC investigations show that the E-isomer does not result from equilibration but is the primary product of the reaction.
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