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As discussed, the use of Rh complexes incorporating chiral phosphines such as BINAP has not been investigated with cinnamaldehyde derivatives that are the subject of our work; BINAP has been examined in only two cases involving the enantioselective addition to β-alkyl-α,β-unsaturated aldehydes. See Itooka, R.; Iguchi, Y.; Miyaura, N. J. Org. Chem. 2003, 68, 6000.
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33645185292
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note
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For the preparation of ligand 9; see ref 7a and S1 for details.
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33
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33645169641
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note
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This solvent effect was first observed by Miyaura: see ref 9 for details.
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34
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