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note
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Even if nine lines only were detectable in this multiplet, the experimental intensity ratio between these components corresponded well to the theoretical 0.015:0.18:1:3.3:7.5:12:14:12:7.5:3.3:1:0.18:0.015 ratio (Figure S3). The observed averaged JHF corresponded well to the expected value, i.e., (17 x 2)/12.
-
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19
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22544485822
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note
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The nature of the exchange processes has been deduced mainly on the basis of the correlations in the meta region, since the cross-peaks in the ortho region were affected also by dipolar and scalar contributions, and the para region is intrinsically less informative.
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20
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22544481588
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Wiley-Interscience Publishers: New York, Chapter VI
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22544470124
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29 salt of 1 showed a short N-O contact of ca. 273 pm.
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+ cation of the anions 2 and/or 3 does occur (as revealed by a cross-peak in the 2D EXSY map of Figure S4), but it is too slow to lead to averaged signals.
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