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Synthesis of the cyanide derivative has also been recently reported by a different group. Lancaster, S. J.; Walker, D. A.; Thornton-Pett, M.; Bochman, M. Chem. Commun., 1999, 1533-1534.
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0342662936
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note
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3: C, 45.30; H, 1.60; N, 3.52. Found: C, 45.23; H, 1.48; N, 3.47.
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17
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0343097235
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note
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See Supporting Information for synthetic details.
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18
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0342662937
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note
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-1, F(000) = 1292, number of reflections collected = 18837, number of independent reflections = 6122, GOF = 1.028, R1 = 0.0444 (I > 2σ(I)), wR2 = 0.1292 (all data).
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19
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0000112781
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