An accurate methodology to identify the level of aggregation in solution by PGSE NMR measurements: The case of half-sandwich diamino ruthenium(II) salts

Organometallics

Volumn 24, Issue 14, 2005, Pages 3476-3486

  Zuccaccia, Daniele ^a   Macchioni, Alceo ^a  

^a UNIVERSITY OF PERUGIA   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

COMPLEXATION; CONFORMATIONS; NEGATIVE IONS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; RUTHENIUM; SALTS; SOLUTIONS; SOLVENTS; TEMPERATURE DISTRIBUTION;

CRITICAL FACTORS; DENATURED SOLVENTS; NMR MEASUREMENTS; RELATIVE ANIONS;

AGGLOMERATION;

EID: 22444448700     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om050145k     Document Type: Article

References (59)

1. Hahn, E. L. Phys. Rev. 1950, 80, 580-594.
2. Stejskal, E. O.; Tanner, J. E. J. Chem Phys. 1965, 42, 288.
3. Stilbs, P. Prog. Nucl. Magn. Reson. Spectrosc. 1987, 19, 1.
4. Price, W. S. Concepts Magn. Res. 1997, 9, 299.
5. Price, W. S. Concepts Magn. Res. 1998, 10, 197.
6. Johnson, C. S., Jr. Prog. Nucl. Magn. Reson. Spectrosc. 1999, 34, 203.
7. For reviews on applications to organometallic chemistry, see: Valentini, M.; Rüegger, H.; Pregosin, P. S. Helv. Chim. Acta 2001, 84, 2833.
8. Binotti, B.; Macchioni, A.; Zuccaccia, C.; Zuccaccia, D. Comments Inorg. Chem. 2002, 23, 417.
9. Pregosin, P. S.; Martinez-Viviente, E.; Kumar, P. G. A. Dalton Trans. 2003, 4007.
10. For a recent review on the application in supramolecular chemistry, see: Cohen, Y.; Avram, L.; Frish, L. Angew. Chem., Int. Ed. 2005, 44, 520.
11. Mo, H.; Pochapsky, T. C. J. Phys. Chem. B 1997, 101, 4485.
12. Zuccaccia, C.; Bellachioma, G.; Cardaci, G.; Macchioni, A. Organometallics 2000, 19, 4663.
13. (a) Bondi, A. J. Phys. Chem. 1964, 68, 441.
14. (b) Rowland R. S.; Taylor, R. J. Phys. Chem. 1996, 100, 7384.
15. Edward, J. T. J. Chem. Educ. 1970, 47, 261.
16. Chen, H.-C.; Chen, S.-H. J. Phys. Chem. 1984, 88, 5118.
17. Espinosa, P. J.; de la Torre, J. G. J. Phys. Chem. 1987, 91, 3612.
18. Gierer, A.; Wirtz, K. Z. Naturforsch. A 1953, 8, 522.
19. Spernol, A.; Wirtz, K. Z. Naturforsch. A 1953, 8, 532.
20. Macchioni, A. Eur. J. Inorg. Chem. 2003, 195.
21. Macchioni, A. In Perspectives in Organometallic Chemistry; Screttas, C. G., Steele, B. R., Eds.; The Royal Society of Chemistry: Cambridge, 2003; pp 196-207.
22. Zuccaccia, C.; Stahl, N. G.; Macchioni, A.; Chen, M.-C.; Roberts, J. A.; Marks, T. J. J. Am. Chem. Soc. 2004, 126, 1448.
23. Zuccaccia, D.; Sabatini, S.; Bellachioma, G.; Cardaci, G.; Clot, E.; Macchioni, A.; Inorg. Chem. 2003, 42, 5465.
24. Zuccaccia, D.; Clot, E.; Macchioni, A. New J. Chem. 2005, 29, 430.
25. For a recent review on ion pairing effect in transition-metal organometallic chemistry, see: Macchioni, A. Chem. Rev. 2005, in press.
26. Crabtree, R. H.; Pearman, A. J. J. Organomet. Chem. 1977, 141, 325.
27. (a) Novakova, O.; Chen, H.; Vrana, O.; Rodger, A.; Sadler, P. J.; Brabek, V. Biochemistry 2003, 42, 11544.
28. (b) Chen, H.; Morris, R. E.; Sadler, P. J. J. Am. Chem Soc. 2003, 125, 173.
29. (c) Aird, R. E.; Gumming, J.; Ritchie, A. A.; Muir, M.; Morris, R. E.; Chen, H.; Sadler, P. J.; Jodrell, D. L. Br. J. Cancer 2002, 86, 1652.
30. (d) Chen, H.; Parkinson, J.; Morris, R. E.; Parson, S.; Coxall, R. A.; Gould, R. O.; Sadler, P. J. J. Am. Chem Soc. 2002, 124, 3064.
31. (e) Morris, R. E.; Aird, R. E.; Murdoch, Piedad del Socorro; Chen, H.; Gumming, J.; Hughes, N.; Parson, S.; Parkin, A.; Boyd, G.; Jodrell, D. L.; Sadler, P. J. J. Med. Chem. 2001, 44, 1652.
32. Handbook of Chemistry and Physics, 67th ed; CRC Press: Boca Raton, FL, 1987.
33. Holz, M.; Xi-an, Mao; Seiferling, D.; Sacco, A. J. Chem. Phys. 1996, 104, 669.
34. Mills, R. J. Phys. Chem. 1973, 77, 685.
35. Dinnebier, R. E.; Dollase, W. A.; Helluy, X.; Kümmerlen, J.; Sebald, A.; Schmidt, M. U.; Pagola, S.; Stephens, P. W.; van Smaalen, S. Acta Crystallogr. 1999, B55, 1014.
36. Macura, S.; Ernst, R. R. Mol. Phys. 1980, 41, 95.
37. Reichardt, C. Solvents and Solvent Effect in Organic Chemistry; Wiley-VCH: Weinheim, 2003.
38. (a) Bhambri, S.; Bishop, A.; Kaltsoyannis, N.; Tocher, D. A. J. Chem. Soc., Dalton Trans. 1998, 3379.
39. (b) Albrigth, T. A. Acc. Chem. Res. 1982, 15, 149.
40. Bailey, M. F.; Dahl, L. F. Inorg. Chem. 1965, 4, 1298.
41. Koshland, D. E.; Myers, S. E.; Chesick, J. P. Acta Crystallogr., Sect. B 1977, B33, 2013.
42. Bennet, M. A.; Robertson, G. B.; Smith, A. K. J. Organomet. Chem. 1972, 43, C41.
43. Restivo, R. J.; Ferguson, G.; O'Sullivan, D. J.; Lalor, F. J. Inorg. Chem. 1975, 12, 3046.
44. (a) Iverson, D. J.; Hunter, G.; Blount, J. F.; Damewood, J. R., Jr.; Mislow, K. J. Am. Chem. Soc. 1981, 103, 6073.
45. (b) Hunter, G.; Blount, J. F.; Damewood, J. R.; Iverson, D. J.; Mislow, K. Organometallics 1982, 1, 448.
46. Siedle, A. R.; Newmark, R. A.; Pignolet, L. H.; Wang, D. X.; Albright, T. A. Organometallics 1986, 5, 38.
47. Albrigth, T. A.; Hoffmann R.; Tse J. C.; D'Ottavio T. J. Am. Chem. Soc. 1979, 101, 3812.
48. Braga, D. Chem. Rev. 1992, 92, 633.
49. Wright, J. M.; Landis, C. B.; Ros, M. A. M. P.; Horton, A. D. Organometallics 1998, 17, 5031.
50. Landis, C. R.; Luck, L. L.; Wright, J. M. J. Magn. Reson., Ser. B 1995, 109, 44-59.
51. Beringhelli, T.; D'Alfonso, G.; Maggioni, D.; Mercandelli, P.; Sironi, A. Chem. Eur. J. 2005, 11, 650.
52. Benneth, M. A.; Smith, A. K. J. Chem. Soc., Dalton Trans. 1974, 233.
53. Jeener, J.; Meier, B. H.; Bachmann, P.; Ernst, R. R. J. Chem. Phys. 1979, 71, 4546.
54. Wagner, R.; Berger, S. J. Magn. Reson. A 1996, 123, 119.
55. Lix, B.; Sönnichsen, F. D.; Sykes, B. D. J. Magn. Reson. A 1996, 121, 83.
56. Neuhaus, D.; Williamson, M. The Nuclear Overhauser Effect in Structural and Conformational Analysis, Wiley-VCH: Weinheim, 2000; Chapter 4.
57. Tanner, J. J. Chem. Phys. 1970, 52, 2523.
58. Tyrrell, H. J. W.; Harris, K. R. Diffusion in Liquids; Butterworth: London, 1984.
59. Dinnebier, R. E.; Dollase, W. A.; Helluy, X.; Kümmerlen, J.; Sebald, A.; Schmidt, M. U.; Pagola, S.; Stephens, P. W.; Van Smaalen, S. Acta Crystallogr. 1999, B55, 1014.