Determination of chlorpyrifos metabolites in human urine by reversed-phase/weak anion exchange liquid chromatography-electrospray ionisation-tandem mass spectrometry

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 822, Issue 1-2, 2005, Pages 160-169

  Bicker, Wolfgang ^a,b   Lämmerhofer, Michael ^a   Lindner, Wolfgang ^a  

^a UNIVERSITY OF VIENNA   (Austria)

^b UNIVERSITY OF VIENNA   (Austria)

Author keywords

Chlorpyrifos; Human poisoning; Liquid chromatography tandem mass spectrometry; Metabolites; Reversed phase weak anion exchange stationary phase; Urine

Indexed keywords

ACETONITRILE; BODY FLUIDS; ION EXCHANGE; IONIZATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PESTICIDES; PHOSPHATES;

CHLORPYRIFOS METABOLITES; DIETHYL THIOPHOSPHATE (DETP); HUMAN URINE; MASS SPECTROMETRIC SCREENING;

METABOLITES;

ACETIC ACID ETHYL ESTER; ACETONITRILE; CHLORPYRIFOS; PESTICIDE; PHOSPHATE; PYRIDINOL;

ANALYTIC METHOD; ANALYTICAL PARAMETERS; ANION EXCHANGE CHROMATOGRAPHY; ARTICLE; BIOTRANSFORMATION; DIAGNOSTIC ACCURACY; DIAGNOSTIC VALUE; ELECTROSPRAY; ELECTROSPRAY MASS SPECTROMETRY; ELUTION; HUMAN; INTOXICATION; LINEAR SYSTEM; LIQUID LIQUID EXTRACTION; METABOLITE; PRIORITY JOURNAL; PRODUCT RECOVERY; QUANTITATIVE ANALYSIS; REVERSED PHASE LIQUID CHROMATOGRAPHY; SEPARATION TECHNIQUE; SIGNAL NOISE RATIO; STANDARD; TANDEM MASS SPECTROMETRY; TOXICOKINETICS; URINALYSIS; URINARY EXCRETION; VALIDATION PROCESS;

CHLORPYRIFOS; CHROMATOGRAPHY, ION EXCHANGE; HUMANS; PHOSPHATES; PHOSPHORIC ACID ESTERS; POISONING; PYRIDONES; REPRODUCIBILITY OF RESULTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION;

EID: 22244468685     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2005.06.003     Document Type: Article

References (44)

1. C.M. Thompson, and R.J. Richardson C. Timothy Marrs Bryan Ballantyne Pesticide Toxicology and International Regulation 2004 John Wiley & Sons Chichester 89
2. C.K. Aaron, and M.A. Howland M.J. Ellenhorn S. Schonwald G. Ordog J. Wasserberger Ellenhorn's Medical Toxicology second ed. 1997 Williams & Wilkins Baltimore 1429
3. D. Aygun, Z. Doganay, L. Altintop, H. Guven, M. Onar, T. Deniz, and T. Sunter J. Toxicol. Clin. Toxicol. 40 2002 903
4. W.L. Chen, J.J. Sheets, R.J. Nolan, and J.L. Mattsson Regul. Toxicol. Pharmacol. 29 1999 15
5. S. Padilla Toxicology 102 1995 215
6. J. Cocker, H.J. Mason, S.J. Garfitt, and K. Jones Toxicol. Lett. 134 2002 97
7. V. Drevenkar, Z. Radić, Ž. Vasilić, and E. Reiner Arch. Environ. Contam. Toxicol. 20 1991 417
8. P. Griffin, H. Mason, K. Heywood, and J. Cocker Occup. Environ. Med. 56 1999 10
9. R.J. Nolan, D.L. Rick, N.L. Freshour, and J.H. Saunders Toxicol. Appl. Pharmacol. 73 1984 8
10. W. Bicker, M. Lämmerhofer, D. Genser, H. Kiss, W. Lindner, Toxicol. Lett. (2005) in press.
11. D.B. Barr, and L.L. Needham J. Chromatogr. B 778 2002 5
12. N. Kupfermann, A. Schmoldt, and H. Steinhart J. Anal. Toxicol. 28 2004 242
13. R. Bravo, L.M. Caltabiano, G. Weerasekera, R.D. Whitehead, C. Fernandez, L.L. Needham, A. Bradman, and D.B. Barr J. Expo. Anal. Environ. Epidem. 14 2004 249
14. R. Bravo, W.J. Driskell, R.D. Whitehead Jr., L.L. Needham, and D.B. Barr J. Anal. Toxicol. 26 2002 245
15. A.N. Oglobline, H. Elimelakh, B. Tattam, G. Holder, R. Geyer, and G.E. O'Donnell Analyst 126 2001 1037
16. J. Hardt, and J. Angerer J. Anal. Toxicol. 24 2000 678
17. W.C. Lin, C.H. Kuei, H.C. Wu, C.C. Yang, and H.Y. Chang J. Anal. Toxicol. 26 2002 176
18. A.N. Oglobline, G.E. O'Donnell, R. Geyer, G.M. Holder, and B. Tattam J. Anal. Toxicol. 25 2001 153
19. T.F. Moate, C. Lu, R.A. Fenske, R.M.A. Hahne, and D.A. Kalman J. Anal. Toxicol. 23 1999 230
20. C. Aprea, G. Sciarra, and L. Lunghini J. Anal. Toxicol. 20 1996 559
21. B.P. Nutley, and J. Cocker Pestic. Sci. 38 1993 315
22. S.J. Reid, and R.R. Watts J. Anal. Toxicol. 5 1981 126
23. F. Hernández, J.V. Sancho, and O.J. Pozo Rapid Commun. Mass Spectrom. 16 2002 1766
24. H.M. Koch, and J. Angerer J. Chromatogr. B. 759 2001 43
25. C. Aprea, A. Betta, G. Catenacci, A. Lotti, S. Magnaghi, A. Barisano, V. Passini, I. Pavan, G. Sciarra, V. Vitalone, and C. Minoia J. AOAC Int. 82 1999 305
26. J.R. Ormand, D.A. McNett, and M.J. Bartels J. Anal. Toxicol. 23 1999 35
27. D.B. Shealy, M.A. Bonin, J.V. Wooten, D.L. Ashley, L.L. Needham, and A.E. Bond Environ. Int. 22 1996 661
28. R.H. Hill Jr., D.B. Shealy, S.L. Head, C.C. Williams, S.L. Bailey, M. Gregg, S.E. Baker, and L.L. Needham J. Anal. Toxicol. 19 1995 323
29. M.J. Bartels, and P.E. Kastl J. Chromatogr. 575 1992 69
30. A.O. Olsson, J.V. Nguyen, M.A. Sadowski, and D.B. Barr Anal. Bioanal. Chem. 376 2003 808
31. J.V. Sancho, O.J. Pozo, and F. Hernández Rapid Commun. Mass Spectrom. 14 2000 1485
32. M.J.W. Chang, C.Y. Lin, L.W. Lo, and R.S. Lin Bull. Environ. Contam. Toxicol. 56 1996 367
33. B.A. MacKenzie, C.A.F. Striley, R.E. Biagini, L.E. Stettler, and C.J. Hines Bull. Environ. Contam. Toxicol. 65 2000 1
34. D.D. Shackelford, D.L. Young, C.A. Mihaliak, B.A. Shurdut, and J.A. Itak J. Agric. Food Chem. 47 1999 177
35. E. Watanabe, R. Hoshino, Y. Kanzaki, H. Tokumoto, H. Kubo, and H. Nakazawa J. Agric. Food Chem. 50 2002 3637
36. R. Nogueira, M. Lämmerhofer, W. Lindner, J. Chromatogr. A (in review).
37. F. Hernández, J.V. Sancho, and O.J. Pozo J. Chromatogr. B 808 2004 229
38. V. Drevenkar, Ž. Vasilić, B. Štengl, Z. Fröbe, and V. Rumenjak Chem. Biol. Interact. 87 1993 315
39. Ž. Vasilić, V. Drevenkar, V. Rumenjak, B. Štengl, and Z. Fröbe Arch. Environ. Contam. Toxicol. 22 1992 351
40. T. Shafik, D.E. Bradway, H.F. Enos, and A.R. Yobs J. Agric. Food Chem. 21 1973 625
41. B.K. Matuszewski, M.L. Constanzer, and C.M. Chavez-Eng Anal. Chem. 75 2003 3019
42. M.T. Shafik, and H.F. Enos J. Agric. Food Chem. 17 1969 1186
43. H. Mei W.A. Korfmacher Using Mass Spectrometry for Drug Metabolism Studies 2005 CRC Press Boca Raton 103
44. Ph. Hubert, P. Chiap, J. Crommen, B. Boulanger, E. Chapuzet, N. Mercier, S. Bervoas-Martin, P. Chevalier, D. Grandjean, P. Lagorce, M. Lallier, M.C. Laparra, M. Laurentie, and J.C. Nivet Anal. Chim. Acta 391 1999 135