Manganese(I) poly(mercaptoimidazolyl)borate complexes: Spectroscopic and structural characterization of Mn ⋯ H-B interactions in solution and in the solid state

Dalton Transactions

Volumn , Issue 1, 2005, Pages 171-180

  Graham, Leigh A ^a   Fout, Alison R ^a   Kuehne, Karl R ^a   White, Jennifer L ^a   Mookherji, Bhaskar ^a   Marks, Fred M ^a   Yap, Glenn P A ^b   Zakharov, Lev N ^c   Rheingold, Arnold L ^c   Rabinovich, Daniel ^a  

^a UNIVERSITY OF NORTH CAROLINA AT CHARLOTTE   (United States)

^b UNIVERSITY OF DELAWARE   (United States)

^c UNIVERSITY OF CALIFORNIA   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CHEMICAL BONDS; CHLORINATION; COMPLEXATION; DIAMAGNETISM; INFRARED SPECTROSCOPY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

COORDINATION CHEMISTRY; LIGANDS; PERIODIC TABLE;

MANGANESE;

EID: 19944426800     PISSN: 14779226     EISSN: None     Source Type: Journal    
DOI: 10.1039/b412280a     Document Type: Article

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42. 2-B,H) fashion, while displaying Mn ⋯ H distances in an even broader range (ca. 1.50-1.83 Å), usually exhibit Mn ⋯ H-B bond angles that are clearly more acute, typically between 88 and 105°. See refs. 11b-d and the following: (a) J. W. Lott and D. F. Gaines, Inorg. Chem., 1974, 13, 2261; (b) D. F. Gaines, J. W. Lott and J. C. Calabrese, Inorg. Chem., 1974, 13, 2419; (c) J. C. Calabrese, M. B. Fischer, D. F. Gaines and J. W. Lott, J. Am. Chem. Soc., 1974, 96, 6318; (d) M. W. Chen, J. C. Calabrese, D. F. Gaines and D. F. Hillenbrand, J. Am. Chem. Soc., 1980, 102, 4928; (e) A. R. Kennedy and J. H. Morris, Acta Crystallogr., Sect. C, 2001, 57, 269; (f) M. A. Beckett, D. S. Brassington, S. J. Coles, T. Gelbrich and M. B. Hursthouse, Polyhedron, 2003, 22, 1627.
43. 2-B,H) fashion, while displaying Mn ⋯ H distances in an even broader range (ca. 1.50-1.83 Å), usually exhibit Mn ⋯ H-B bond angles that are clearly more acute, typically between 88 and 105°. See refs. 11b-d and the following: (a) J. W. Lott and D. F. Gaines, Inorg. Chem., 1974, 13, 2261; (b) D. F. Gaines, J. W. Lott and J. C. Calabrese, Inorg. Chem., 1974, 13, 2419; (c) J. C. Calabrese, M. B. Fischer, D. F. Gaines and J. W. Lott, J. Am. Chem. Soc., 1974, 96, 6318; (d) M. W. Chen, J. C. Calabrese, D. F. Gaines and D. F. Hillenbrand, J. Am. Chem. Soc., 1980, 102, 4928; (e) A. R. Kennedy and J. H. Morris, Acta Crystallogr., Sect. C, 2001, 57, 269; (f) M. A. Beckett, D. S. Brassington, S. J. Coles, T. Gelbrich and M. B. Hursthouse, Polyhedron, 2003, 22, 1627.
44. 2-B,H) fashion, while displaying Mn ⋯ H distances in an even broader range (ca. 1.50-1.83 Å), usually exhibit Mn ⋯ H-B bond angles that are clearly more acute, typically between 88 and 105°. See refs. 11b-d and the following: (a) J. W. Lott and D. F. Gaines, Inorg. Chem., 1974, 13, 2261; (b) D. F. Gaines, J. W. Lott and J. C. Calabrese, Inorg. Chem., 1974, 13, 2419; (c) J. C. Calabrese, M. B. Fischer, D. F. Gaines and J. W. Lott, J. Am. Chem. Soc., 1974, 96, 6318; (d) M. W. Chen, J. C. Calabrese, D. F. Gaines and D. F. Hillenbrand, J. Am. Chem. Soc., 1980, 102, 4928; (e) A. R. Kennedy and J. H. Morris, Acta Crystallogr., Sect. C, 2001, 57, 269; (f) M. A. Beckett, D. S. Brassington, S. J. Coles, T. Gelbrich and M. B. Hursthouse, Polyhedron, 2003, 22, 1627.
45. 2-B,H) fashion, while displaying Mn ⋯ H distances in an even broader range (ca. 1.50-1.83 Å), usually exhibit Mn ⋯ H-B bond angles that are clearly more acute, typically between 88 and 105°. See refs. 11b-d and the following: (a) J. W. Lott and D. F. Gaines, Inorg. Chem., 1974, 13, 2261; (b) D. F. Gaines, J. W. Lott and J. C. Calabrese, Inorg. Chem., 1974, 13, 2419; (c) J. C. Calabrese, M. B. Fischer, D. F. Gaines and J. W. Lott, J. Am. Chem. Soc., 1974, 96, 6318; (d) M. W. Chen, J. C. Calabrese, D. F. Gaines and D. F. Hillenbrand, J. Am. Chem. Soc., 1980, 102, 4928; (e) A. R. Kennedy and J. H. Morris, Acta Crystallogr., Sect. C, 2001, 57, 269; (f) M. A. Beckett, D. S. Brassington, S. J. Coles, T. Gelbrich and M. B. Hursthouse, Polyhedron, 2003, 22, 1627.
46. 2-B,H) fashion, while displaying Mn ⋯ H distances in an even broader range (ca. 1.50-1.83 Å), usually exhibit Mn ⋯ H-B bond angles that are clearly more acute, typically between 88 and 105°. See refs. 11b-d and the following: (a) J. W. Lott and D. F. Gaines, Inorg. Chem., 1974, 13, 2261; (b) D. F. Gaines, J. W. Lott and J. C. Calabrese, Inorg. Chem., 1974, 13, 2419; (c) J. C. Calabrese, M. B. Fischer, D. F. Gaines and J. W. Lott, J. Am. Chem. Soc., 1974, 96, 6318; (d) M. W. Chen, J. C. Calabrese, D. F. Gaines and D. F. Hillenbrand, J. Am. Chem. Soc., 1980, 102, 4928; (e) A. R. Kennedy and J. H. Morris, Acta Crystallogr., Sect. C, 2001, 57, 269; (f) M. A. Beckett, D. S. Brassington, S. J. Coles, T. Gelbrich and M. B. Hursthouse, Polyhedron, 2003, 22, 1627.
47. 2-B,H) fashion, while displaying Mn ⋯ H distances in an even broader range (ca. 1.50-1.83 Å), usually exhibit Mn ⋯ H-B bond angles that are clearly more acute, typically between 88 and 105°. See refs. 11b-d and the following: (a) J. W. Lott and D. F. Gaines, Inorg. Chem., 1974, 13, 2261; (b) D. F. Gaines, J. W. Lott and J. C. Calabrese, Inorg. Chem., 1974, 13, 2419; (c) J. C. Calabrese, M. B. Fischer, D. F. Gaines and J. W. Lott, J. Am. Chem. Soc., 1974, 96, 6318; (d) M. W. Chen, J. C. Calabrese, D. F. Gaines and D. F. Hillenbrand, J. Am. Chem. Soc., 1980, 102, 4928; (e) A. R. Kennedy and J. H. Morris, Acta Crystallogr., Sect. C, 2001, 57, 269; (f) M. A. Beckett, D. S. Brassington, S. J. Coles, T. Gelbrich and M. B. Hursthouse, Polyhedron, 2003, 22, 1627.
48. See refs. 10, 13 and the following: (a) S. Trofimenko, J. Am. Chem. Soc., 1969, 91, 588; (b) J. H. MacNeil, A. W. Roszak, M. C. Baird, K. F. Preston and A. L. Rheingold, Organometallics, 1993, 12, 4402; (c) J. E. Joachim, C. Apostolidis, B. Kanellakopulos, R. Maier, N. Marques, D. Meyer, J. Müller, A. Pires de Matos, B. Nuber, J. Rebizant and M. L. Ziegler, J. Organomet. Chem., 1993, 448, 119; (d) H. V. R. Dias, H.-J. Kim, H.-L. Lu, K. Rajeshwar, N. R. de Tacconi, A. Derecskei-Kovacs and D. S. Marynick, Organometallics, 1996, 15, 2994; (e) P. J. Bailey, M. Lanfranchi, L. Marchio and S. Parsons, Inorg. Chem., 2001, 40, 5030; (f) P. J. Bailey, P. Pinho and S. Parsons, Inorg. Chem., 2003, 42, 8872.
49. See refs. 10, 13 and the following: (a) S. Trofimenko, J. Am. Chem. Soc., 1969, 91, 588; (b) J. H. MacNeil, A. W. Roszak, M. C. Baird, K. F. Preston and A. L. Rheingold, Organometallics, 1993, 12, 4402; (c) J. E. Joachim, C. Apostolidis, B. Kanellakopulos, R. Maier, N. Marques, D. Meyer, J. Müller, A. Pires de Matos, B. Nuber, J. Rebizant and M. L. Ziegler, J. Organomet. Chem., 1993, 448, 119; (d) H. V. R. Dias, H.-J. Kim, H.-L. Lu, K. Rajeshwar, N. R. de Tacconi, A. Derecskei-Kovacs and D. S. Marynick, Organometallics, 1996, 15, 2994; (e) P. J. Bailey, M. Lanfranchi, L. Marchio and S. Parsons, Inorg. Chem., 2001, 40, 5030; (f) P. J. Bailey, P. Pinho and S. Parsons, Inorg. Chem., 2003, 42, 8872.
50. See refs. 10, 13 and the following: (a) S. Trofimenko, J. Am. Chem. Soc., 1969, 91, 588; (b) J. H. MacNeil, A. W. Roszak, M. C. Baird, K. F. Preston and A. L. Rheingold, Organometallics, 1993, 12, 4402; (c) J. E. Joachim, C. Apostolidis, B. Kanellakopulos, R. Maier, N. Marques, D. Meyer, J. Müller, A. Pires de Matos, B. Nuber, J. Rebizant and M. L. Ziegler, J. Organomet. Chem., 1993, 448, 119; (d) H. V. R. Dias, H.-J. Kim, H.-L. Lu, K. Rajeshwar, N. R. de Tacconi, A. Derecskei-Kovacs and D. S. Marynick, Organometallics, 1996, 15, 2994; (e) P. J. Bailey, M. Lanfranchi, L. Marchio and S. Parsons, Inorg. Chem., 2001, 40, 5030; (f) P. J. Bailey, P. Pinho and S. Parsons, Inorg. Chem., 2003, 42, 8872.
51. See refs. 10, 13 and the following: (a) S. Trofimenko, J. Am. Chem. Soc., 1969, 91, 588; (b) J. H. MacNeil, A. W. Roszak, M. C. Baird, K. F. Preston and A. L. Rheingold, Organometallics, 1993, 12, 4402; (c) J. E. Joachim, C. Apostolidis, B. Kanellakopulos, R. Maier, N. Marques, D. Meyer, J. Müller, A. Pires de Matos, B. Nuber, J. Rebizant and M. L. Ziegler, J. Organomet. Chem., 1993, 448, 119; (d) H. V. R. Dias, H.-J. Kim, H.-L. Lu, K. Rajeshwar, N. R. de Tacconi, A. Derecskei-Kovacs and D. S. Marynick, Organometallics, 1996, 15, 2994; (e) P. J. Bailey, M. Lanfranchi, L. Marchio and S. Parsons, Inorg. Chem., 2001, 40, 5030; (f) P. J. Bailey, P. Pinho and S. Parsons, Inorg. Chem., 2003, 42, 8872.
52. See refs. 10, 13 and the following: (a) S. Trofimenko, J. Am. Chem. Soc., 1969, 91, 588; (b) J. H. MacNeil, A. W. Roszak, M. C. Baird, K. F. Preston and A. L. Rheingold, Organometallics, 1993, 12, 4402; (c) J. E. Joachim, C. Apostolidis, B. Kanellakopulos, R. Maier, N. Marques, D. Meyer, J. Müller, A. Pires de Matos, B. Nuber, J. Rebizant and M. L. Ziegler, J. Organomet. Chem., 1993, 448, 119; (d) H. V. R. Dias, H.-J. Kim, H.-L. Lu, K. Rajeshwar, N. R. de Tacconi, A. Derecskei-Kovacs and D. S. Marynick, Organometallics, 1996, 15, 2994; (e) P. J. Bailey, M. Lanfranchi, L. Marchio and S. Parsons, Inorg. Chem., 2001, 40, 5030; (f) P. J. Bailey, P. Pinho and S. Parsons, Inorg. Chem., 2003, 42, 8872.
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