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int = 0.0797). Structure solution and refinement based on 1534 observed reflections with I ≥ 2σ(I) and 142 parameters gave R1 = 0.0554, wR2 = 0.1254 and S = 1.003. CCDC-253101. Data collection for 1 was performed on a Rigaku Mercury CCD diffractometer equipped with a graphite-monochromated MoKa radiation (λ = 0.71073 Å) at 293(2) K. The intensity data set was collected with an ω scan technique and corrected by CrystalClear software. The structure was solved by the direct methods and refined by full-matrix least-squares techniques. Non-hydrogen atoms were located by difference Fourier map and subjected to anisotropic refinement. Hydrogen atoms were added according to the theoretical models. All of the calculations were performed by the Siemens SHELXTL version 5 package of crystallographic software.
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