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3 (2.0 mmol for 1a) or NaOAc (2.0 mmol for 1b-d) in water (3 mL). The mixture was then heated with vigorous stirring at the temperature and for the time shown in Table 2. It was then cooled, diluted with water and extracted with ethyl acetate. The products 2a-g were purified by column chromatography over silica gel
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Walet, M.A.M.6
De Vries, J.G.7
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