Convection-compensating diffusion experiments with phase-sensitive double-quantum filtering

Journal of Magnetic Resonance

Volumn 174, Issue 2, 2005, Pages 229-236

  Momot, Konstantin I ^a   Kuchel, Philip W ^a  

^a UNIVERSITY OF SYDNEY   (Australia)

Author keywords

Convection compensating NMR diffusion measurements; DOSY; Drug binding; Drug delivery; Gradient coherence transfer pathway selection; Solvent suppression

Indexed keywords

DIFFUSION; DRUG PRODUCTS; INTEGRAL EQUATIONS; LIQUID CRYSTALS; MATHEMATICAL MODELS; NUCLEAR MAGNETIC RESONANCE; SOLVENTS;

CONVECTION-COMPENSATING NMR DIFFUSION MEASUREMENT; DOSY; DRUG BINDING; DRUG DELIVERY; GRADIENT COHERENCE TRANSFER PATHHWAY SELECTION; SOLVENT SUPPRESSION;

QUANTUM THEORY;

CARBON TETRACHLORIDE; CHLOROFORM; LYSOZYME; MACROGOL DERIVATIVE; SOLUTOL HS 15; STEARIC ACID DERIVATIVE;

ARTICLE; CHEMISTRY; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SIGNAL PROCESSING;

CARBON TETRACHLORIDE; CHLOROFORM; MAGNETIC RESONANCE SPECTROSCOPY; MURAMIDASE; POLYETHYLENE GLYCOLS; SIGNAL PROCESSING, COMPUTER-ASSISTED; STEARIC ACIDS;

EID: 17644377261     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jmr.2005.02.003     Document Type: Article

References (32)

1. C.S. Johnson Diffusion ordered nuclear magnetic resonance spectroscopy: principles and applications Prog. Nucl. Magn. Reson. Spectrosc. 34 1999 203 256
2. G.H. Sørland, J.G. Seland, J. Krane, and H.W. Anthonsen Improved convection compensating pulsed field gradient spin-echo and stimulated-echo methods J. Magn. Reson. 142 2000 323 325
3. A. Jerschow, and N. Müller Suppression of convection artifacts in stimulated-echo diffusion experiments. Double-stimulated-echo experiments J. Magn. Reson. 125 1997 372 375
4. K.I. Momot, and P.W. Kuchel Convection-compensating PGSE experiment incorporating excitation-sculpting water suppression (CONVEX) J. Magn. Reson. 169 2004 92 101
5. W.S. Price Water signal suppression in NMR spectroscopy Annu. Rep. NMR Spectrosc. 38 1999 289 354
6. W.S. Price, F. Elwinger, C. Vigouroux, and P. Stilbs PGSE-WATERGATE, a new tool for NMR diffusion-based studies of ligand-macromolecule binding Magn. Reson. Chem. 40 2002 391 395
7. 1H diffusion-weighted PFG phase-sensitive double-quantum NMR spectroscopy NMR Biomed. 10 1997 285 291
8. J.F. Martin, L.S. Selwyn, R.R. Vold, and R.L. Vold The determination of translational diffusion constants in liquid crystals from pulsed field gradient double quantum spin echo decays J. Chem. Phys. 76 1982 2632 2634
9. D. Zax, and A. Pines Study of anisotropic diffusion of oriented molecules by multiple quantum spin echoes J. Chem. Phys. 78 1983 6333 6334
10. L.D. Field, S.A. Ramadan, and G.K. Pierens Multiple-quantum NMR spectra of partially oriented indene: a new approach to estimating order in a nematic phase J. Magn. Reson. 156 2002 64 71
11. S.A. Ramadan, L.D. Field, and G.K. Pierens Multiple quantum nuclear magnetic resonance spectra of partially oriented styrene in a nematic phase Mol. Phys. 101 2003 1813 1818
12. L.D. Field, and S.A. Ramadan Multiple quantum NMR spectra of toluene and p-bromotoluene partially aligned in a nematic phase Magn. Reson. Chem. 41 2003 933 938
13. P.W. Kuchel, and B.E. Chapman Heteronuclear double-quantum-coherence selection with magnetic-field gradients in diffusion experiments J. Magn. Reson. A 101 1993 53 59
14. B.E. Chapman, and P.W. Kuchel Sensitivity in heteronuclear multiple-quantum diffusion experiments J. Magn. Reson. A 102 1993 105 109
15. M. Liu, X.-A. Mao, C. Ye, J.K. Nicholson, and J.C. Lindon Enhanced effect of magnetic field gradients using multiple quantum NMR spectroscopy applied to self-diffusion coefficient measurement Mol. Phys. 93 1998 913 920
16. M.H. Levitt Spin dynamics: Basics of nuclear magnetic resonance 2001 Wiley Chichester
17. R.R. Ernst, G. Bodenhausen, and A. Wokaun Principles of nuclear magnetic resonance in one and two dimensions 1987 Clarendon Press Oxford
18. T.J. Norwood Multiple-quantum NMR methods Prog. Nucl. Magn. Reson. Spectrosc. 24 1992 295 375
19. C.E. Hughes, M. Carravetta, and M.H. Levitt Some conjectures for cogwheel phase cycling J. Magn. Reson. 167 2004 259 265
20. 1 noise in high-field NMR spectrometers J. Magn. Reson. 100 1992 316 328
21. P.J. Bowyer, A.G. Swanson, and G.A. Morris Analyzing and correcting spectrometer temperature sensitivity J. Magn. Reson. 152 2001 234 246
22. L.J. Mueller, D.W. Elliott, G.M. Leskowitz, J. Struppe, R.A. Olsen, K.-C. Kim, and C.A. Reed Uniform-sign cross-peak double-quantum-filtered correlation spectroscopy J. Magn. Reson. 168 2004 327 335
23. A.A. Shaw, C. Salaun, J.F. Dauphin, and B. Ancian Artifact-free PFG-enhanced double-quantum-filtered COSY experiments J. Magn. Reson. A 120 1996 110 115
24. B. Ancian, I. Bourgeois, J.F. Dauphin, and A.A. Shaw Artifact-free pure absorption PFG-enhanced DQF-COSY spectra including a gradient pulse in the evolution period J. Magn. Reson. 125 1997 348 354
25. A. Jerschow, and N. Müller Convection compensation in gradient enhanced nuclear magnetic resonance spectroscopy J. Magn. Reson. 132 1998 13 18
26. K.I. Momot, P.W. Kuchel, B.E. Chapman, P. Deo, and D. Whittaker NMR study of the association of propofol with nonionic surfactants Langmuir 19 2003 2088 2095
27. + diffusion in a bicontinuous cubic phase by the ionophore monensin Langmuir 20 2004 2660 2666
28. K.I. Momot, and P.W. Kuchel Pulsed field gradient nuclear magnetic resonance as a tool for studying drug delivery systems Concepts Magn. Reson. A 19 2003 51 64
29. W.S. Price, F. Tsuchiya, and Y. Arata Lysozyme aggregation and solution properties studied using PGSE NMR diffusion measurements J. Am. Chem. Soc. 121 1999 11503 11512
30. C. Dalvit, and J.M. Bohlen Proton phase-sensitive pulsed field gradient double-quantum spectroscopy Annu. Rep. NMR Spectrosc. 37 1999 203 271
31. A.D. Bain, I.W. Burton, and W.F. Reynolds Artifacts in 2-dimensional NMR Prog. Nucl. Magn. Reson. Spectrosc. 26 1994 59 89
32. 1 artifacts in two-dimensional NMR spectroscopy J. Magn. Reson. 140 1999 513 515