Multiple quantum NMR spectra of toluene and p-bromotoluene partially aligned in a nematic phase

Magnetic Resonance in Chemistry

Volumn 41, Issue 11, 2003, Pages 933-938

  Field, Leslie D ^a   Ramadan, Saadallah A ^a  

^a UNIVERSITY OF SYDNEY   (Australia)

Author keywords

1H NMR; Dipolar coupling; Liquid crystal; Multiple quantum spectroscopy; NMR; p bromotoluene; Partially aligned molecules; Toluene

Indexed keywords

LIQUID CRYSTALS; MOLECULAR ORIENTATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; ORGANIC SOLVENTS;

1H NMR; ALIGNED MOLECULES; DIPOLAR COUPLINGS; LIQUID-CRYSTALS; MULTIPLE QUANTUM NMR; MULTIPLE QUANTUM SPECTROSCOPIES; NEMATIC PHASIS; NMR SPECTRUM; P-BROMOTOLUENE; PARTIALLY ALIGNED MOLECULE;

TOLUENE;

4 BROMOTOLUENE; SOLVENT; TOLUENE; TOLUENE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CRYSTAL STRUCTURE; LIQUID CRYSTAL; MOLECULAR BIOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; QUANTUM CHEMISTRY; SPIN LABELING;

EID: 0242522144     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/mrc.1281     Document Type: Article

References (47)

1. (a) Emsley JW (ed). Nuclear Magnetic Resonance of Liquid Crystals. Riedel: Dordrecht, 1985;
2. (b) Emsley JW, Lindon JC. NMR Spectroscopy Using Liquid Crystal Solvents. Pergamon, Press: Oxford, 1975.
3. Drobney G, Pines A, Sinton S, Weitekamp D, Wemmer D. Faraday Symp. Chem. Soc. 1979; 13: 49.
4. Sinton S, Pines A. Chem. Phys. Lett. 1980; 76: 263.
5. Warren WS, Pines A. J. Am. Chem. Soc. 1981; 103: 1613.
6. Weitekamp D, Garbow JR, Pines A. J. Chem. Phys. 1982; 77: 2870.
7. Slichter CP. Principles of Magnetic Resonance (3rd edn). Springer: Berlin, 1990.
8. Ernst RR, Bodenhausen G, Wokaun A. Principles of Magnetic Resonance in One and Two Dimensions. Oxford University Press: Oxford, 1988.
9. Bodenhausen G. Prog. Nucl. Magn. Reson. Spectrosc. 1981; 14: 137.
10. Drobney GP. Annu Rev. Phys. Chem. 1985; 36: 451.
11. Weitekamp D. Adv. Magn. Reson. 1983; 11: 111.
12. (a) Field LD. In Encyclopaedia of NMR, Grant DM, Harris RK (eds). Wiley: Chichester, 1996; 3172;
13. (b) Field LD. In NMR of Orientationally Ordered Liquids, Burnell EE, de Lange CA (eds). Kluwer Academic Press: Dordrecht, 2003; Chapter 4.
14. (a) Sinton S, Zax D, Murdoch JB, Pines A. Mol. Phys. 1984; 53: 333;
15. (b) Sinton S. PhD Thesis, University of California, Berkeley, CA, 1982.
16. Polson JM, Burnell EE. J. Chem. Phys. 1995; 103: 6891.
17. Celebre G, Castiglione F, Longerie M, Emsley JW. J. Magn. Reson. A 1996; 121: 139.
18. Syvitsky RT, Burnell EE. Can. J. Chem. 1999; 77: 1761.
19. Castiglione F, Celebre G, De Luca G, Longerie M. J. Magn. Reson. 2000; 142: 216.
20. Syvitsky RT, Burnell EE. J. Magn. Reson. 2000; 144: 58.
21. Chandrakumar T, Polson JM, Burnell EE. J. Magn. Reson. A 1996; 118: 264.
22. Field LD, Pierens GK, Cross KJ, Terry ML. J. Magn. Reson. 1992; 97: 451.
23. Field LD, Ramadan SA, Pierens GK. J. Magn. Reson. 2002; 156: 64.
24. Ramadan SA, Field LD, Pierens GK. Mol. Phys. in press.
25. Diehl P, Khetrapal CL. NMR - Basic Principles and Progress, Vol 1. Springer: Berlin, 1969.
26. Diehl P, Kellerhals HP, Niederberger W. J. Magn. Reson. 1971; 4: 352.
27. Pierens GK. PhD Thesis, University of Sydney, 1992.
28. Ramadan SA. PhD Thesis, University of Sydney, 2000.
29. Ferretti JA, Harris RK, Johannesen RB. J. Magn. Reson. 1970; 3: 84.
30. (a) Keeler J, Clowes RT, Davies AL, Laue E. Methods Enzymol. 1994; 239: 145;
31. (b) Bax A, DeJong PG, Mehlkopf AF, Schmidt J. Chem. Phys. Lett. 1980; 69: 568;
32. (c) Pierens GK, Carpenter TA, Colebrook LD, Field LD, Hall LD. J. Magn. Reson. 1992; 99: 398;
33. (d) Vold RL, Waugh JS, Klein MP, Phelps DE. J. Chem. Phys. 1982; 48: 3831;
34. (e) Martin JF, Selwyn LS, Vold RR, Vold RL. J. Chem. Phys. 1982; 76: 2632;
35. (f) Zax D, Pines A. J. Chem. Phys. 1983; 78: 6333;
36. (g) Maudsley A, Wokaun A, Ernst RR. Chem. Phys. Lett. 1978; 55: 9.
37. Brugel W. Handbook of NMR Spectral Parameters. Heyden: London, 1979.
38. HyperChem™ Release 4.5 for SGI. Molecular Modeling System. Hypercube.
39. Bunker PR. Molecular Symmetry and Spectroscopy. Academic Press: New York, 1979.
40. Saupe A, Englert G. Phys. Rev. Lett. 1963; 11: 462.
41. Diehl P, Heinrichs PM, Niederberger W. Mol. Phys. 1971; 20: 139.
42. (a) Langseth A, Stoicheff BP. Can. J. Phys. 1956; 34: 350;
43. (b) Cox EG, Cruickshank DWJ, Smith JAS. Proc. R. Soc. London, Ser. A 1958; 1: 247.
44. Lister DG, Macdonald JN, Owen NL. Internal Rotation and Inversion: an Introduction to Large Amplitude Motion in Molecules. Academic Press: New York, 1978.
45. SPARTAN SGI Version 5.0.2 OpenGl. Wavefunction: Irvine, CA.
46. (a) Iijima T. Z. Naturforsch., Teil A 1977; 32: 1063;
47. (b) Seip R, Shultz G, Hargittai I, Szabo Z. Z. Naturforsch., Teil A 1977; 32: 1178.