Complexation of uranium(VI) with protocatechuic acid-application of iterative transformation factor analysis to EXAFS spectroscopy

Analytical and Bioanalytical Chemistry

Volumn 376, Issue 5, 2003, Pages 631-638

  Rossberg A ^a   Reich, T ^b   Bernhard, G ^a  

^a INSTITUTE OF ION BEAM PHYSICS AND MATERIALS RESEARCH   (Germany)

^b JOHANNES GUTENBERG UNIVERSITY   (Germany)

Author keywords

Complexation; EXAFS spectroscopy; Factor analysis; Protocatechuic acid; Speciation; Uranium

Indexed keywords

ALGORITHMS; CARBOXYLIC ACIDS; CHELATION; COMPLEXATION; CONCENTRATION (PROCESS); ITERATIVE METHODS; PH; SOLUTIONS; X RAY ANALYSIS;

EXAFS SPECTROSCOPY; FACTOR ANALYSIS; PHOTOCATECHUIC ACID; SPECIATION;

URANIUM;

EID: 1442345758     PISSN: 16182642     EISSN: None     Source Type: Journal    
DOI: 10.1007/s00216-003-1963-5     Document Type: Article

References (38)

1. Ludwig C. H., Sarkanen K. V. Lignins - Occurence, formation, structure and reactions. (1971) Wiley, New York p. 773.
2. Cresser M., Killham K., Edwards T. (1993) Soil chemistry and its applications. In: Campbell P. G. C., Galloway J. N., Harrison R. M. (eds) Soil organic matter. Cambridge Environmental Chemistry Series, Cambridge University Press p. 34.
3. Fritsche W. (1985) Umwelt-Mikrobiologie. Akademie-Verlag, Berlin p. 52.
4. Ebert G. (1993) Biopolymere - Struktur und Eigenschaften. B. G. Teubner, Stuttgart p. 442.
5. Masselter S., Zemann A., Bobleter O.(1995) Analysis of lignin degradation products by capillary electrophoresis. Chromatographia 40 51.
6. Baraniak L., Schmidt M., Bernhard G., Nitsche H.(1997). Complex formation of hexavalent uranium with lignin degradation products. Annual Report 1996, Forschungszentrum Rossendorf, Institut für Radiochemie 180 28.
7. Böder W., Schuppan W. (1991) Schriftenreihe: Lagerstätten- forschung in Deutschland der Gesellschaft Deutscher Metallhütten- und Bergleute 64 203.
8. Roßberg A., Baraniak L., Reich T., Hennig C., Bernhard G., Nitsche H. (2000) EXAFS structural analysis of aqueous uranium(VI) complexes with lignin degradation products. Radiochim. Acta 88 593.
9. Matz W., Schell N., Bernhard G., Prokert F., Reich T., Claussner J., Oehme W., Schlenk R., Dienel S., Funke H., Eichhorn F., Betzel M., Proehl D., Strauch U., Hüttig G., Krug H., Neumann W., Brendler V., Reichel P., Denecke M. A., Nitsche H. (1999) ROBL - a CRC beamline for radiochemistry and materials research at the ESRF. J. Synchrotron Rad. 6 1076.
10. Bucher J.J., Allen P.G., Edelstein N.M., Shuh D.K., Madden N.W., Cork C., Luke P., Pehl D., Malone D. (1996) A multichannel monolithic Ge detector system for fluorescence x-ray absorption spectroscopy. Rev. Sci. Instrum. 67(9) 1.
11. Malinowski E. R. (1977) Determination of the number of factors and the experimental error in a datamatrix. Anal Chem 49 612.
12. George G. N., Pickering I. J. (1995) EXAFSPAK: A suite of computer programs for analysis of x-ray absorption spectra. Stanford Synchrotron Radiation Laboratory. Stanford, CA, USA.
13. Zabinsky S. I., Rehr J. J., Ankudinov A., Albers R. C., Eller M. J. (1995) Multiple-scattering calculations of x-ray-absorption spectra. Phys. Rev. B 52 2995.
14. Malinowski E. R. (1991) Factor analysis in chemistry. Wiley. New York.
15. Shrager R. I. (1986) Chemical transitions measured by spectra and resolved using singular value decomposition. Chemometrics and Intelligent Laboratory Systems 1 59.
16. Press W. H., Flannery B. P., Teukolsky S. A., Vetterling W. T. (1986) Numerical recipes: The art of scientific computing. Cambridge University Press, New York.
17. Köckler N. (1994) Numerical methods and scientific computing. Oxford University Press, New York.
18. Jonsthon R. L. (1982) Numerical methods - A software approach. Wiley, New York.
19. Wold H. (1966) In: Krishnaiah P. R. (ed) Multivariate analysis. Academic Press, Orlando FL.
20. Gourlay A. R., Watson G. A. (1973) Computational methods for matrix eigenproblems. Wiley, New York.
21. Fernandez-Garcia M., Marquez Alvarez C., Haller G. L. (1995) XANES-TPR study of Cu-Pd bimetallic catalysts: Application of factor analysis. J. Phys. Chem. 99 12565.
22. Roßberg A. (2002) Anwendung der Faktorenanalyse auf die Röntgenabsorptionsspektroskopie zur Bestimmung der Speziation von Uran in Lösungen. Doctoral Thesis, Technical University Dresden, Dresden.
23. Brayden T. H., Poropatic P. A., Watanabe J. L. (1988) Iterative target testing for calculation of missing data points. Anal. Chem. 60 1154.
24. Kaiser H. F. (1958) The VARIMAX criterion for analytic rotation in factor analysis. Psychometrika 23 187.
25. Teo B. K. (1986) EXAFS: Basic principles and data analysis. Springer, Berlin Heidelberg New York.
26. Templeton, D. H., Zalkin A., Ruben H., Templeton L. K. (1985) Redetermination and absolute configuration of sodium uranyl(VI) triacetate. Act. Cryst. C41 1439.
27. Reich T., Hudson E. A., Denecke M. A., Allen P. G., Nitsche H. (1997) Structural analysis of uranium(VI) complexes by X-ray absorption spectroscopy. Poverkhnost 4-5 149.
28. Hudson E. A., Allen P. G., Terminello L. J., Denecke M. A., Reich T. (1996) Polarized X-ray-absorption spectroscopy of the uranyl ion: Comparison of experiment and theory. Phys. Rev. B 54 156.
29. Denecke M. A., Reich T., Pompe S., Bubner M., Heise K. H., Nitsche H., Allen P. G., Bucher J. J., Edelstein N. M., Shuh D. K. (1997) Differentiating between monodentate and bidentate carboxylate ligands coordinated to uranyl ions using EXAFS. J. Phys. IV France 7, C2-637.
30. Thompson H. A., Brown Jr. G. E., Parks G. A. (1997) XAFS spectroscopic study of uranyl coordination in solids and aqueous solution. Am. Mineralogist 82 483.
31. 3+ by X-ray absorption fine structure spectroscopy. Inorg. Chem. 36 4676.
32. Roßberg A., Acker M., Reich T., Bernhard G. (2003) (in preparation)
33. 2 thin films prepared by ion beam induced CVD: Preparation and characterization by X-ray absorption spectroscopy. Thin Solid Films 353 113.
34. 2 nanoparticles by factor analysis of XAS and FT-IR spectra. Solid State Ionics 116 117.
35. Wasserman S. R., Winans R. E., McBeth R. (1996) Iron species in Argonne premium coal samples: An investigation using X-ray absorption spectroscopy. Energy & Fuels 10 392.
36. Wasserman S. R. (1997) The analysis of mixtures: Application of principal component analysis to XAS spectra. J. Phys. IV France 7 C2-203.
37. Wasserman S. R., Allen P. G., Shun D. K., Bucher J. J., Edelstein N. M. (1999) EXAFS and principal component analysis: A new shell game. J. Synchrotron Rad. 6 284.
38. Fay M. J., Proctor A., Hoffman D. P., Houalla M., Hercules D. M. (1992) Determination of the Mo surface environment of Mo/TiO2 catalysts by EXAFS, XANES and PCA. Mikrochim. Acta 109, 281.