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It is noteworthy that there is a single datum that gives a precedent for a recoverable, solid organic catalyst for lactide polymerization in ref 11. In that work, DMAP immobilized on polystyrene was used as a catalyst and the solid was recovered by filtration. No discussion of residual catalyst in the polymer was presented for that sample.
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note
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Based on upon estimates of the amount of polymer adsorbed to the silica catalysts and the amount of polymer produced and recovered, the polymer loss with the catalyst amounts to 2% of the total polymer mass.
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