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2O (10:1) was used for the exchange of dodecanethiol with the OPV molecules. Samples were immersed in 1 mL OPV solution and flushed with Ar for 20 min. Ethylenediamine (10 μL) was added to deprotect the acetyl thiols. The mixture was kept under Ar and allowed to react for 20 min. The samples were washed in acetonitrile and water to remove unreacted material.
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