Ruthenocenyl ruthenium bimetallic complexes: Electrospray mass spectrometric study of [RuX(η5-C5H5)(η2-dppr)] n+ (dppr=1,1′-bis(diphenylphosphino)ruthenocene) (X=Cl, n=0; X=CO, CH3CN, C=CHPh, n=1) and the X-ray crystal and molecular structure of [Ru(η5-C5H5)(CO)(η 2-dppr)]PF6

Journal of Organometallic Chemistry

Volumn 575, Issue 2, 1999, Pages 171-181

  Po Yeo, Siew ^a   Henderson, William ^b   Mak, Thomas C W ^c   Hor, T S Andy ^a  

^a NATIONAL UNIVERSITY OF SINGAPORE   (Singapore)

^b UNIVERSITY OF WAIKATO   (New Zealand)

^c CHINESE UNIVERSITY OF HONG KONG   (Hong Kong)

Author keywords

Crystal structure; Electrospray mass spectrometry; Metallocenyl phosphine; Ruthenium; Vinylidene

Indexed keywords

STAPHYLOCOCCUS PHAGE 3A;

EID: 0347660387     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(98)00990-5     Document Type: Article

References (60)

1. (a) L.S. Hegedus, in: M. Schlosser (Ed.), Organometallics in Synthesis - A Manual, Wiley, Chichester, 1994, p. 383.
2. (b) G.W. Parshall, S.D. Ittel, Homogeneous Catalysis: The Applications and Chemistry of Catalysis by Soluble Transition Metal Complexes, 2nd ed., Wiley, New York, 1992.
3. (a) J. Louie, M.S. Driver, B.C. Hamann, J.F. Hartwig, J. Org. Chem. 62 (1997) 1268.
4. (b) T. Ishiyama, M. Mori, A. Suzuki, N. Miyaura, J. Organomet. Chem. 525 (1996) 225.
5. Driver M.S., Hartwig J.F. J. Am. Chem. Soc. 118:1996;7217.
6. S. Li, B. Wei, P.M.N. Low, H.K. Lee, T.S.A. Hor, T.C.W. Mak, J. Chem. Soc. Dalton Trans. (1997) 1289.
7. Wei B., Li S., Lee H.K., Hor T.S.A. J. Organomet. Chem. 527:1997;133.
8. A.P. Snyder (Ed.), Biochemical and Biotechnological Applications of Electrospray Ionisation Mass Spectrometry, ACS, Washington DC, 1995.
9. For examples see: (a) W. Henderson, J.S. McIndoe, B.K. Nicholson, P.J. Dyson, Chem. Commun. 10 (1996) 1183. (b) M.B. Dinger, W. Henderson, B.K. Nicholson, A.L. Wilkins, J. Organomet. Chem. 526 (1996) 303. (c) R. Colton, A. D'Agostino, J.C. Traeger, Mass Spectrom. Rev. 14 (1995) 79. (d) R.T. Aplin, H. Doucet, M.W. Hooper, J.M. Brown, Chem. Commun. (1997) 2097. (e) H. Hori, F.P.A. Johnson, K. Koike, K. Takeuchi, T. Ibusuki, O. Ishitani, J. Chem. Soc. Dalton Trans. (1997) 1019.
10. For examples see: (a) W. Henderson, J.S. McIndoe, B.K. Nicholson, P.J. Dyson, Chem. Commun. 10 (1996) 1183. (b) M.B. Dinger, W. Henderson, B.K. Nicholson, A.L. Wilkins, J. Organomet. Chem. 526 (1996) 303. (c) R. Colton, A. D'Agostino, J.C. Traeger, Mass Spectrom. Rev. 14 (1995) 79. (d) R.T. Aplin, H. Doucet, M.W. Hooper, J.M. Brown, Chem. Commun. (1997) 2097. (e) H. Hori, F.P.A. Johnson, K. Koike, K. Takeuchi, T. Ibusuki, O. Ishitani, J. Chem. Soc. Dalton Trans. (1997) 1019.
11. For examples see: (a) W. Henderson, J.S. McIndoe, B.K. Nicholson, P.J. Dyson, Chem. Commun. 10 (1996) 1183. (b) M.B. Dinger, W. Henderson, B.K. Nicholson, A.L. Wilkins, J. Organomet. Chem. 526 (1996) 303. (c) R. Colton, A. D'Agostino, J.C. Traeger, Mass Spectrom. Rev. 14 (1995) 79. (d) R.T. Aplin, H. Doucet, M.W. Hooper, J.M. Brown, Chem. Commun. (1997) 2097. (e) H. Hori, F.P.A. Johnson, K. Koike, K. Takeuchi, T. Ibusuki, O. Ishitani, J. Chem. Soc. Dalton Trans. (1997) 1019.
12. For examples see: (a) W. Henderson, J.S. McIndoe, B.K. Nicholson, P.J. Dyson, Chem. Commun. 10 (1996) 1183. (b) M.B. Dinger, W. Henderson, B.K. Nicholson, A.L. Wilkins, J. Organomet. Chem. 526 (1996) 303. (c) R. Colton, A. D'Agostino, J.C. Traeger, Mass Spectrom. Rev. 14 (1995) 79. (d) R.T. Aplin, H. Doucet, M.W. Hooper, J.M. Brown, Chem. Commun. (1997) 2097. (e) H. Hori, F.P.A. Johnson, K. Koike, K. Takeuchi, T. Ibusuki, O. Ishitani, J. Chem. Soc. Dalton Trans. (1997) 1019.
13. For examples see: (a) W. Henderson, J.S. McIndoe, B.K. Nicholson, P.J. Dyson, Chem. Commun. 10 (1996) 1183. (b) M.B. Dinger, W. Henderson, B.K. Nicholson, A.L. Wilkins, J. Organomet. Chem. 526 (1996) 303. (c) R. Colton, A. D'Agostino, J.C. Traeger, Mass Spectrom. Rev. 14 (1995) 79. (d) R.T. Aplin, H. Doucet, M.W. Hooper, J.M. Brown, Chem. Commun. (1997) 2097. (e) H. Hori, F.P.A. Johnson, K. Koike, K. Takeuchi, T. Ibusuki, O. Ishitani, J. Chem. Soc. Dalton Trans. (1997) 1019.
14. (a) T. Lover, G.A. Bowmaker, W. Henderson, R.P. Cooney, Chem. Commun. 5 (1996) 683.
15. (b) K.J. Fisher, W. Henderson, I.G . Dance, G.D. Willett, J. Chem. Soc. Dalton Trans. (1996) 4109.
16. (a) G.S. Ashby, M.I. Bruce, I.B. Tomkins, R.C. Wallis, Aust. J. Chem. 32 (1979) 1003.
17. (b) M.I. Bruce, I.R. Butler, W.R. Cullen, G.A. Koutsantonis, M.R. Snow, E.T. Tiekink, Aust. J. Chem. 41 (1988) 963.
18. (a) G. Consiglio, F. Morandini, Chem. Rev. 87 (1987) 761.
19. (b) G. Consiglio, F. Morandini, G.F. Ciani, A. Sironi, Organometallics 5 (1986) 1976.
20. (a) C. Masters, Homogeneous Transition-metal Catalysis: A Gentle Art, Chapman and Hall, London, 1981, p. 52.
21. (b) B.R. James, L.D. Markham, D.K. Wang, J. Chem. Soc. Chem. Commun. (1974) 439.
22. (c) J. Tsuji, H. Suzuki, Chem. Lett. (1977) 1083.
23. (a) R. Noyori, H. Takaya, Acc. Chem. Res. 23 (1990) 345.
24. (b) H. Takaya, T. Ohta, R. Noyori, K. Mashima, Pure Appl. Chem. 62 (1990) 1135.
25. (c) K. Mashima, Y. Matsumura, K. Kusano, H. Kumobayashi, N. Sayo, Y. Hori, T. Ishizaki, S. Akutagawa, H. Takaya, J. Chem. Soc. Chem. Commun. (1991) 609.
26. (d) Monsanto, World Patent WO9,015,790A, 1991.
27. Brown J.M., Guiry P.J. Inorg. Chim. Acta. 220:1994;249.
28. T. Blackmore, M.I. Bruce, F.G.A. Stone, J. Chem. Soc. (A) (1971) 2376.
29. M.I. Bruce, F.S. Wong, B.W. Skelton, A.H. White, J. Chem. Soc. Dalton Trans. (1981) 1398.
30. Onaka S., Moriya T., Takagi S., Mizuno A., Furuta H. Bull. Chem. Soc. Jpn. 65:1992;1415.
31. (a) M.I. Bruce, R.C. Wallis, Aust. J. Chem. 32 (1979) 1471.
32. (b) M. Sato, M. Sekino, J. Organomet. Chem. 444 (1996) 185.
33. Czech P.T., Xe X.G., Fenske R.F. Organometallics. 9:1990;2016.
34. R.M. Bullock, J. Chem. Soc. Chem. Commun. (1989) 165.
35. Sato M., Asa M. J. Organomet. Chem. 508:1996;121.
36. (a) M.I. Bruce, Chem. Rev. 91 (1991) 197.
37. (b) M.I. Bruce, Pure Appl. Chem. 62 (1990) 1021.
38. (c) I. de los Ríos, M.J. Tenorio, M.C. Puerta, P. Valerga, J. Am. Chem. Soc. 119 (1997) 6529.
39. (d) R. Le Lagadec, E. Roman, L. Toupet, U. Müller, P.H. Dixneuf, Organometallics 13 (1994) 5030.
40. (e) S.G. Davies, J.P. McNally, A.J. Smallridge, Adv. Organomet. Chem. 30 (1990) 1.
41. (f) J. Silvestre, R. Hoffmann, Helv. Chim. Acta 68 (1985) 1461.
42. (a) F.J.G. Alonson, A. Höhn, J. Wolf, H. Otto, H. Werner, Angew. Chem. Int. Ed. Engl. 24 (1985) 406.
43. (b) K.R. Birdwhistell, T.L. Tonker, J.L. Templeton, J. Am. Chem. Soc. 107 (1985) 4474.
44. Bianchini C., Peruzzini M., Vacca A., Zanobini F. Organometallics. 10:1991;3697.
45. Wakatsuki Y., Koga N., Werner H., Morokuma K. J. Am. Chem. Soc. 119:1997;360.
46. (a) B.M. Trost, R.J. Kulawiec, J. Am. Chem. Soc. 114 (1992) 5579.
47. (b) Y. Nishibayashi, I. Takei, M. Hidai, Organometallics 16 (1997) 3091.
48. Henderson W., Olsen G.M. Polyhedron. 17:1998;577.
49. Henderson W., Sabat M. Polyhedron. 16:1997;1663.
50. M.I. Bruce, M. Ke, P.J. Low, Chem. Commun. (1996) 2405.
51. W. Henderson, B.M. Nicholson, J. Chem. Soc. Chem. Commun. (1995) 2531.
52. (a) M. Oliván, O. Eisenstein, K.G. Caulton, Organometallics 16 (1997) 2227.
53. (b) M. Oliván, E. Clot, O. Eisenstein, K.G. Caulton, Organometallics 17 (1998) 3091.
54. (a) D.F. Shriver, M.A. Drezdzon, The Manipulation of Air-Sensitive Compounds, 2nd ed., Wiley-Interscience, New York, 1986. (b) J.P. McNally, V.S. Leong, N.J. Cooper, in: A.L. Wayda, M.Y. Darensbourg (Eds.), Experimental Organometallic Chemistry - A Practicum in Synthesis and Characterisation, ACS Symposium Series 357, ACS, Washington DC, 1987.
55. (b) J.P. McNally, V.S. Leong, N.J. Cooper, in: A.L. Wayda, M.Y. Darensbourg (Eds.), Experimental Organometallic Chemistry - A Practicum in Synthesis and Characterisation, ACS Symposium Series 357, ACS, Washington DC, 1987.
56. Gordon A.J., Ford R.A. The Chemist's Companion: A Handbook of Practical Data, Techniques and References. 1972;Wiley-Interscience, New York.
57. Arnold L.J. J. Chem. Educ. 69:1992;811.
58. (a) SHELXTL Version 5 Reference Manual, Siemens Energy&Automation, Madison, WI, 1996. (b) G.M. Sheldrick, in: H.D. Flack, L. Párkányi, K. Simon (Eds.), Crystallographic Computing 6: A Window in Modern Crystallography, Oxford University Press, New York, 1993, pp. 100-122.
59. (b) G.M. Sheldrick, in: H.D. Flack, L. Párkányi, K. Simon (Eds.), Crystallographic Computing 6: A Window in Modern Crystallography, Oxford University Press, New York, 1993, pp. 100-122.
60. (b) G.M. Sheldrick, in: H.D. Flack, L. Párkányi, K. Simon (Eds.), Crystallographic Computing 6: A Window in Modern Crystallography, Oxford University Press, New York, 1993, pp. 100-122.