Reactions of alkyl-iron(II) and -ruthenium(II) complexes with B(C 6F5)3 and its water adducts. X-ray structure of a cyclometallated-iron(II) carbene

Inorganica Chimica Acta

Volumn 353, Issue , 2003, Pages 245-252

  Bellachioma, Gianfranco ^a   Cardaci, Giuseppe ^a   Foresti, Elisabetta ^b   Macchioni, Alceo ^a   Sabatino, Piera ^b   Zuccaccia, Cristiano ^a  

^a UNIVERSITY OF PERUGIA   (Italy)

^b UNIVERSITY OF BOLOGNA   (Italy)

Author keywords

B(C6F5)3 activation; B(C6F5)3 H2O reactivity; Cyclometallated iron(II) carbene

Indexed keywords

IRON COMPOUNDS; ORGANIC COMPOUNDS;

CARBENES; COMPLEX 1; DECOMPOSITION PROCESS; REACTIVE SPECIES; RUTHENIUM COMPLEXES; WATER ADDUCTS; X-RAY DIFFRACTION STUDIES; X-RAY STRUCTURE;

RUTHENIUM COMPOUNDS;

CARBENE; FERROUS ION; IRON COMPLEX; METAL; RUTHENIUM COMPLEX; WATER;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; DECOMPOSITION; REACTION ANALYSIS; STRUCTURE ANALYSIS; X RAY DIFFRACTION;

EID: 0141740336     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0020-1693(03)00327-X     Document Type: Article

References (59)

1. Chen E.Y.-X., Marks T.J. Chem. Rev. 100:2000;1391. and references therein.
2. Ittel S.D., Johnson L.K., Brookhart M. Chem. Rev. 100:2000;1169. and references therein.
3. Crabtree R.H. Chem. Rev. 85:1985;245.
4. Shilov R.E. Activation of Saturated Hydrocarbon by Transition Metal Complexes. 1984;D. Reidel, Dordrecht.
5. Piers W.E., Chiver T. Chem. Soc. Rev. 26:1997;345.
6. Jacobsen H., Berke H., Doring S., Kehr G., Erker G., Frohlich R., Meyer O. Organometallics. 18:1999;1724.
7. Yang X., Stern C.L., Marks T.J. J. Am. Chem. Soc. 119:1991;3623.
8. Jia L., Yang X., Stern C.L., Marks T.J. Organometallics. 16:1997;842.
9. Giardello M.A., Disen M.S., Stern C.L., Marks T.J. J. Am. Chem. Soc. 117:1995;12114.
10. Snofield M.J., Ewast S.W., Tremblay T.L., Baird M.C. J. Chem. Soc., Dalton Trans. 1997;3097.
11. Le Grognec E., Poli R., Richard P., Llusar R., Uriel S. J. Organomet. Chem. 640:2001;113.
12. Bazan G.C., Rogers J.S., Fang C.C. Organometallics. 20:2001;2059.
13. Lee B.Y., Bazan G.C., Vela J., Komon Z.J.A., Bu X. J. Am. Chem. Soc. 123:2001;5352.
14. Hill G.S., Rendina L.M., Puddephatt R.J. J. Chem. Soc., Dalton Trans. 1996;1809.
15. Chen Y.-X., Stern C.L., Marks T.J. J. Am. Chem. Soc. 119:1997;2582.
16. Chen Y.-X., Stern C.L., Marks T.J. J. Am. Chem. Soc. 118:1996;12451.
17. Tritto I., Bonetti R., Sacchi M.C., Locatelli P., Zannoni G. Macromolecules. 32:1999;264.
18. Tritto I., Bonetti R., Sacchi M.C., Locatelli P., Zannoni G. Macromolecules. 30:1997;1247.
19. Danopoulos A.A., Galsworthy J.R., Green M.L.H., Gafferkey S., Doerrer L.H., Hursthouse M.B. J. Chem. Soc., Dalton Trans. 1998;2529.
20. Doerrer L.H., Green M.L.H. J. Chem. Soc., Dalton Trans. 1999;4325.
21. Beringhelli T., Maggioni D., D'Alfonso G. Organometallics. 20:2001;4927.
22. Reichenbach G., Cardaci G., Bellachioma G. J. Chem. Soc., Dalton Trans. 1982;847.
23. Pankoski M., Bigorgne M. J. Organomet. Chem. 30:1971;227.
24. Cardaci G. J. Organomet. Chem. 323:1987;C10.
25. Pankowski M., Samuel E., Bigorgne M. J. Organomet. Chem. 97:1975;105.
26. Bellachioma G., Cardaci G., Macchioni A., Zuccaccia C. J. Organomet. Chem. 628:2001;255.
27. Weissberger A., Proskauer E.S. second ed Technique of Organic Chemistry: Organic Solvents. VII:1955;Interscience, New York.
28. Bellachioma G., Cardaci G., Reichenbach G. J. Chem. Soc., Dalton Trans. 1983;2593.
29. Cardaci G., Reichenbach G., Bellachioma G., Wassink B., Baird M.C. Organometallics. 7:1988;2475.
30. Bellachioma G., Cardaci G., Macchioni A., Madami A. Inorg. Chem. 32:1993;554.
31. Siemens "SHELXTLPLUS Version 5.1 (Windows NT Version) Structure Determination Package", Siemens Analytical X-ray Instruments Inc., Madison, WI, 1998.
32. Farrugia L.J. J. Appl. Crystallogr. 1997;565.
33. Brackemeyer T., Erker G., Frohlich R. Organometallics. 16:1997;531.
34. Yang X., Stern C.L., Marks T.J. J. Am. Chem. Soc. 116:1994;10015.
35. Bochmann M., Lancaster S.J., Hursthouse M.B., Malik K.M.A. Organometallics. 13:1994;2235.
36. Desjardins S.Y., Way A.A., Murray M.C., Adirim D., Baird M.C. Organometallics. 17:1998;2382.
37. Bellachioma G., Cardaci G., Jablonski C., Macchioni A., Reichenbach G. Inorg. Chem. 32:1993;2404.
38. Green M.L.H., Haggitt J., Mehnert C.P. J. Chem. Soc., Chem. Commun. 2:1995;1853.
39. Chernega A.N., Graham A.J., Green M.L.H., Haggitt J., Lloyd J., Mehnert C.P., Metzler N., Souter J. J. Chem. Soc., Dalton Trans. 1997;2293.
40. Jameson C.J. Mason J. Multinuclear NMR. 1987;Plenum Press, New York. Chapter 16.
41. Harris R.K. Can. J. Chem. 39:1961;216.
42. Kalamarides H.A., Iyer S., Lipian J., Rhodes L.F., Day C. Organometallics. 19:2000;3983.
43. Hill G.S., Manojlovic-Muir L., Muir K.W., Puddephatt R.J. Organometallics. 16:1997;525.
44. Bellachioma G., Cardaci G., Macchioni A., Reichenbach G., Terenzi S. Organometallics. 15:1996;4349.
45. Macchioni A., Bellachioma G., Cardaci G., Gramlich V., Rüegger H., Terenzi S., Venanzi L.M. Organometallics. 16:1997;2139.
46. Macchioni A., Bellachioma G., Cardaci G., Cruciani G., Foresti E., Sabatino P., Zuccaccia C. Organometallics. 17:1998;5549.
47. Bellachioma G., Cardaci G., Gramlich V., Macchioni A., Valentini M., Zuccaccia C. Organometallics. 17:1998;5025.
48. Zuccaccia C., Bellachioma G., Cardaci G., Macchioni A. Organometallics. 18:1999;1.
49. Zuccaccia C., Bellachioma G., Cardaci G., Macchioni A. J. Am. Chem. Soc. 123:2001;11020.
50. Cambridge Structural Data Base, Version 5.22, October 2001.
51. Bellachioma G., Cardaci G., Macchioni A., Reichenbach G., Foresti E., Sabatino P. J. Organomet. Chem. 531:1997;227.
52. Kandler H., Bidell W., Janicke M., Knickmeier M., Veghini D., Berke H. Organometallics. 17:1998;960.
53. Ferré K., Poignant G., Toupet L., Guerchais V. J. Organomet. Chem. 629:2001;19.
54. Mann B.E. Mason J. Multinuclear NMR. 1987;Plenum Press, New York. Chapter 10.
55. 13C NMR of Transition Metal Phosphine Complexes. 1979;Springer, Berlin.
56. 13C NMR Data for Organometallic Compounds. 1981;Academic Press, London.
57. Butts S.B., Strauss S.H., Holt E.M., Stimson R.E., Alcock N.W., Shriver D.F. J. Am. Chem. Soc. 102:1980;5093.
58. Richmond T.G., Basolo F., Shriver D.F. Inorg. Chem. 21:1982;1272.
59. Barlow G.K., Boyle J.D., Cooley N.A., Ghaffar T., Wass D.F. Organometallics. 19:2000;1470.