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Volumn 4, Issue 15, 2002, Pages 2533-2536

Oligo(octithienylene-diethynylene)s as unprecedentedly long conjugated nanomolecules

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EID: 0041382880     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol026150r     Document Type: Article
Times cited : (21)

References (33)
  • 2
    • 0342517062 scopus 로고    scopus 로고
    • (b) Tour, J. M. Chem. Rev. 1996, 96, 537-553.
    • (1996) Chem. Rev. , vol.96 , pp. 537-553
    • Tour, J.M.1
  • 30
    • 0042593704 scopus 로고    scopus 로고
    • note
    • Preparative GPLC was performed on a Japan Analytical Industry (JAI) Recycling Preparative HPLC Model LC-918R with two columns connected in the series JAIGEL 4H and JAIGEL 3H using chloroform as an eluent (3.8 mL/min); the retention volumes were: 209.5 (1a), 199.5 (1b), 192.0 (1c), 186.0 (1d), 181.5 (1e), 177.5 (1f), 174.0 (1g), 171.0 (1h), 168.5 (1i), 165.5 (1j), and 164.5 (1k) mL.
  • 31
    • 0041591813 scopus 로고    scopus 로고
    • note
    • The yields of oligo(octithienylene-diethynylene)s 1 in Scheme 1 are given as overall yields from tetraoctyloctithiophene (8T), because the consecutive reactions were carried out without separation of the intermediates 4-9. In a separate experiment, however, the intermediates were isolated in the following yields: 4, 43%; 5, 33%; 6, 92%; 7, 95%; 8, 96%; 9, 91%.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.