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4Cl and extraction with dichloromethane. The alcohols were isolated by conventional column chromatography on silica gel. In the case of reactions with preformed catalyst, 5 was replaced by 20 mol% of 6; otherwise the procedure was identical.
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4Cl and extraction with dichloromethane. The alcohols were isolated by conventional column chromatography on silica gel. In the case of reactions with preformed catalyst, 5 was replaced by 20 mol% of 6; otherwise the procedure was identical.
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0036959837
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