The first (tripyrrinato)nickel(II) complexes, TrpyNiX with X = Cl, Br, I: Synthesis, structures and solvent coordination

Journal of the Chemical Society, Dalton Transactions

Volumn , Issue 22, 2002, Pages 4213-4218

  Bröring, Martin ^a   Prikhodovski, Serguei ^a   Brandt, Carsten D ^a  

^a UNIVERSITY OF WÜRZBURG   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

NICKEL COMPOUNDS; NUCLEAR MAGNETIC RESONANCE; PARAMAGNETIC MATERIALS; SOLVENTS; SPECTROSCOPIC ANALYSIS; SYNTHESIS (CHEMICAL); TITRATION;

LIGANDS;

ORGANOMETALLICS;

EID: 0036027129     PISSN: 1470479X     EISSN: None     Source Type: Journal    
DOI: 10.1039/b209212n     Document Type: Article

References (45)

1. J. F. Kirner, J. Garofalo Jr. and W. R. Scheidt, Inorg. Nucl. Chem. Lett., 1975, 11, 107-112; A. L. Balch, M. M. Olmstead and S. L. Phillips, Inorg. Chem., 1993, 32, 3931-3936; M. W. Renner, K. M. Barkigia, D. Melamed, K. M. Smith and J. Fajer, Inorg. Chem., 1996, 35, 5120-5121; K. Ozette, P. Leduc, M. Palacio, J.-F. Bartolic, K. M. Barkigia, J. Fajer, P. Battioni and D. Mansuy, J. Am. Chem. Soc., 1997, 119, 6442-6443; H. Duval, V. Bulach, J. Fisher and R. Weiss, Acta Crystallogr., Sect. C, 1997, 53, 1027-1029; S.-L. Jia, W. Jentzen, M. Shang, X.-Z. Song, J.-G. Ma, W. R. Scheidt and J. A. Shelnutt, Inorg. Chem., 1998, 37, 4402-4412.
2. J. F. Kirner, J. Garofalo Jr. and W. R. Scheidt, Inorg. Nucl. Chem. Lett., 1975, 11, 107-112; A. L. Balch, M. M. Olmstead and S. L. Phillips, Inorg. Chem., 1993, 32, 3931-3936; M. W. Renner, K. M. Barkigia, D. Melamed, K. M. Smith and J. Fajer, Inorg. Chem., 1996, 35, 5120-5121; K. Ozette, P. Leduc, M. Palacio, J.-F. Bartolic, K. M. Barkigia, J. Fajer, P. Battioni and D. Mansuy, J. Am. Chem. Soc., 1997, 119, 6442-6443; H. Duval, V. Bulach, J. Fisher and R. Weiss, Acta Crystallogr., Sect. C, 1997, 53, 1027-1029; S.-L. Jia, W. Jentzen, M. Shang, X.-Z. Song, J.-G. Ma, W. R. Scheidt and J. A. Shelnutt, Inorg. Chem., 1998, 37, 4402-4412.
3. J. F. Kirner, J. Garofalo Jr. and W. R. Scheidt, Inorg. Nucl. Chem. Lett., 1975, 11, 107-112; A. L. Balch, M. M. Olmstead and S. L. Phillips, Inorg. Chem., 1993, 32, 3931-3936; M. W. Renner, K. M. Barkigia, D. Melamed, K. M. Smith and J. Fajer, Inorg. Chem., 1996, 35, 5120-5121; K. Ozette, P. Leduc, M. Palacio, J.-F. Bartolic, K. M. Barkigia, J. Fajer, P. Battioni and D. Mansuy, J. Am. Chem. Soc., 1997, 119, 6442-6443; H. Duval, V. Bulach, J. Fisher and R. Weiss, Acta Crystallogr., Sect. C, 1997, 53, 1027-1029; S.-L. Jia, W. Jentzen, M. Shang, X.-Z. Song, J.-G. Ma, W. R. Scheidt and J. A. Shelnutt, Inorg. Chem., 1998, 37, 4402-4412.
4. J. F. Kirner, J. Garofalo Jr. and W. R. Scheidt, Inorg. Nucl. Chem. Lett., 1975, 11, 107-112; A. L. Balch, M. M. Olmstead and S. L. Phillips, Inorg. Chem., 1993, 32, 3931-3936; M. W. Renner, K. M. Barkigia, D. Melamed, K. M. Smith and J. Fajer, Inorg. Chem., 1996, 35, 5120-5121; K. Ozette, P. Leduc, M. Palacio, J.-F. Bartolic, K. M. Barkigia, J. Fajer, P. Battioni and D. Mansuy, J. Am. Chem. Soc., 1997, 119, 6442-6443; H. Duval, V. Bulach, J. Fisher and R. Weiss, Acta Crystallogr., Sect. C, 1997, 53, 1027-1029; S.-L. Jia, W. Jentzen, M. Shang, X.-Z. Song, J.-G. Ma, W. R. Scheidt and J. A. Shelnutt, Inorg. Chem., 1998, 37, 4402-4412.
5. J. F. Kirner, J. Garofalo Jr. and W. R. Scheidt, Inorg. Nucl. Chem. Lett., 1975, 11, 107-112; A. L. Balch, M. M. Olmstead and S. L. Phillips, Inorg. Chem., 1993, 32, 3931-3936; M. W. Renner, K. M. Barkigia, D. Melamed, K. M. Smith and J. Fajer, Inorg. Chem., 1996, 35, 5120-5121; K. Ozette, P. Leduc, M. Palacio, J.-F. Bartolic, K. M. Barkigia, J. Fajer, P. Battioni and D. Mansuy, J. Am. Chem. Soc., 1997, 119, 6442-6443; H. Duval, V. Bulach, J. Fisher and R. Weiss, Acta Crystallogr., Sect. C, 1997, 53, 1027-1029; S.-L. Jia, W. Jentzen, M. Shang, X.-Z. Song, J.-G. Ma, W. R. Scheidt and J. A. Shelnutt, Inorg. Chem., 1998, 37, 4402-4412.
6. J. F. Kirner, J. Garofalo Jr. and W. R. Scheidt, Inorg. Nucl. Chem. Lett., 1975, 11, 107-112; A. L. Balch, M. M. Olmstead and S. L. Phillips, Inorg. Chem., 1993, 32, 3931-3936; M. W. Renner, K. M. Barkigia, D. Melamed, K. M. Smith and J. Fajer, Inorg. Chem., 1996, 35, 5120-5121; K. Ozette, P. Leduc, M. Palacio, J.-F. Bartolic, K. M. Barkigia, J. Fajer, P. Battioni and D. Mansuy, J. Am. Chem. Soc., 1997, 119, 6442-6443; H. Duval, V. Bulach, J. Fisher and R. Weiss, Acta Crystallogr., Sect. C, 1997, 53, 1027-1029; S.-L. Jia, W. Jentzen, M. Shang, X.-Z. Song, J.-G. Ma, W. R. Scheidt and J. A. Shelnutt, Inorg. Chem., 1998, 37, 4402-4412.
7. P. J. Chmielewski, L. Latos-Grazyński and T. Glowiak, J. Am. Chem. Soc., 1996, 118, 5690-5701.
8. P. J. Chmielewski, L. Latos-Grazyński, M. M. Olmstead and A. L. Balch, Chem. Eur. J., 1997, 3, 268-278.
9. B. Sridevi, S. J. Narayanan, A. Srinivasan, T. K. Chandrashekar and J. Subramanian, J. Chem. Soc., Dalton Trans., 1998, 1979-1984; E. Pacholska, P. J. Chmielewski and L. Latos-Grazyński, Inorg. Chim. Acta, 1998, 273, 184-190.
10. B. Sridevi, S. J. Narayanan, A. Srinivasan, T. K. Chandrashekar and J. Subramanian, J. Chem. Soc., Dalton Trans., 1998, 1979-1984; E. Pacholska, P. J. Chmielewski and L. Latos-Grazyński, Inorg. Chim. Acta, 1998, 273, 184-190.
11. L. Latos-Grazyński, J. Lisowski, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 1183-1188; P. J. Chmielewski, M. Grzeszczuk, L. Latos-Grazyński and J. Lisowski, Inorg. Chem., 1989, 28, 3546-3552; L. Latos-Grazyński, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 4065-4066; J. Lisowski, L. Latos-Grazyński and L. Szterenberg, Inorg. Chem., 1992, 31, 1933-1940; R. J. Chmielewski and L. Latos-Grazyński, Inorg. Chem., 1992, 31, 5231-5235; R. P. Pandian and T. K. Chandrashekar, J. Chem. Soc., Dalton Trans., 1993, 119-125; R. P. Pandian and T. K. Chandrashekar, Inorg. Chem., 1994, 33, 3317-3324; P. Chmielewski, L. Latos-Grazyński and E. Pacholska, Inorg. Chem., 1994, 33, 1992-1999.
12. L. Latos-Grazyński, J. Lisowski, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 1183-1188; P. J. Chmielewski, M. Grzeszczuk, L. Latos-Grazyński and J. Lisowski, Inorg. Chem., 1989, 28, 3546-3552; L. Latos-Grazyński, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 4065-4066; J. Lisowski, L. Latos-Grazyński and L. Szterenberg, Inorg. Chem., 1992, 31, 1933-1940; R. J. Chmielewski and L. Latos-Grazyński, Inorg. Chem., 1992, 31, 5231-5235; R. P. Pandian and T. K. Chandrashekar, J. Chem. Soc., Dalton Trans., 1993, 119-125; R. P. Pandian and T. K. Chandrashekar, Inorg. Chem., 1994, 33, 3317-3324; P. Chmielewski, L. Latos-Grazyński and E. Pacholska, Inorg. Chem., 1994, 33, 1992-1999.
13. L. Latos-Grazyński, J. Lisowski, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 1183-1188; P. J. Chmielewski, M. Grzeszczuk, L. Latos-Grazyński and J. Lisowski, Inorg. Chem., 1989, 28, 3546-3552; L. Latos-Grazyński, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 4065-4066; J. Lisowski, L. Latos-Grazyński and L. Szterenberg, Inorg. Chem., 1992, 31, 1933-1940; R. J. Chmielewski and L. Latos-Grazyński, Inorg. Chem., 1992, 31, 5231-5235; R. P. Pandian and T. K. Chandrashekar, J. Chem. Soc., Dalton Trans., 1993, 119-125; R. P. Pandian and T. K. Chandrashekar, Inorg. Chem., 1994, 33, 3317-3324; P. Chmielewski, L. Latos-Grazyński and E. Pacholska, Inorg. Chem., 1994, 33, 1992-1999.
14. L. Latos-Grazyński, J. Lisowski, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 1183-1188; P. J. Chmielewski, M. Grzeszczuk, L. Latos-Grazyński and J. Lisowski, Inorg. Chem., 1989, 28, 3546-3552; L. Latos-Grazyński, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 4065-4066; J. Lisowski, L. Latos-Grazyński and L. Szterenberg, Inorg. Chem., 1992, 31, 1933-1940; R. J. Chmielewski and L. Latos-Grazyński, Inorg. Chem., 1992, 31, 5231-5235; R. P. Pandian and T. K. Chandrashekar, J. Chem. Soc., Dalton Trans., 1993, 119-125; R. P. Pandian and T. K. Chandrashekar, Inorg. Chem., 1994, 33, 3317-3324; P. Chmielewski, L. Latos-Grazyński and E. Pacholska, Inorg. Chem., 1994, 33, 1992-1999.
15. L. Latos-Grazyński, J. Lisowski, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 1183-1188; P. J. Chmielewski, M. Grzeszczuk, L. Latos-Grazyński and J. Lisowski, Inorg. Chem., 1989, 28, 3546-3552; L. Latos-Grazyński, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 4065-4066; J. Lisowski, L. Latos-Grazyński and L. Szterenberg, Inorg. Chem., 1992, 31, 1933-1940; R. J. Chmielewski and L. Latos-Grazyński, Inorg. Chem., 1992, 31, 5231-5235; R. P. Pandian and T. K. Chandrashekar, J. Chem. Soc., Dalton Trans., 1993, 119-125; R. P. Pandian and T. K. Chandrashekar, Inorg. Chem., 1994, 33, 3317-3324; P. Chmielewski, L. Latos-Grazyński and E. Pacholska, Inorg. Chem., 1994, 33, 1992-1999.
16. L. Latos-Grazyński, J. Lisowski, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 1183-1188; P. J. Chmielewski, M. Grzeszczuk, L. Latos-Grazyński and J. Lisowski, Inorg. Chem., 1989, 28, 3546-3552; L. Latos-Grazyński, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 4065-4066; J. Lisowski, L. Latos-Grazyński and L. Szterenberg, Inorg. Chem., 1992, 31, 1933-1940; R. J. Chmielewski and L. Latos-Grazyński, Inorg. Chem., 1992, 31, 5231-5235; R. P. Pandian and T. K. Chandrashekar, J. Chem. Soc., Dalton Trans., 1993, 119-125; R. P. Pandian and T. K. Chandrashekar, Inorg. Chem., 1994, 33, 3317-3324; P. Chmielewski, L. Latos-Grazyński and E. Pacholska, Inorg. Chem., 1994, 33, 1992-1999.
17. L. Latos-Grazyński, J. Lisowski, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 1183-1188; P. J. Chmielewski, M. Grzeszczuk, L. Latos-Grazyński and J. Lisowski, Inorg. Chem., 1989, 28, 3546-3552; L. Latos-Grazyński, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 4065-4066; J. Lisowski, L. Latos-Grazyński and L. Szterenberg, Inorg. Chem., 1992, 31, 1933-1940; R. J. Chmielewski and L. Latos-Grazyński, Inorg. Chem., 1992, 31, 5231-5235; R. P. Pandian and T. K. Chandrashekar, J. Chem. Soc., Dalton Trans., 1993, 119-125; R. P. Pandian and T. K. Chandrashekar, Inorg. Chem., 1994, 33, 3317-3324; P. Chmielewski, L. Latos-Grazyński and E. Pacholska, Inorg. Chem., 1994, 33, 1992-1999.
18. L. Latos-Grazyński, J. Lisowski, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 1183-1188; P. J. Chmielewski, M. Grzeszczuk, L. Latos-Grazyński and J. Lisowski, Inorg. Chem., 1989, 28, 3546-3552; L. Latos-Grazyński, M. M. Olmstead and A. L. Balch, Inorg. Chem., 1989, 28, 4065-4066; J. Lisowski, L. Latos-Grazyński and L. Szterenberg, Inorg. Chem., 1992, 31, 1933-1940; R. J. Chmielewski and L. Latos-Grazyński, Inorg. Chem., 1992, 31, 5231-5235; R. P. Pandian and T. K. Chandrashekar, J. Chem. Soc., Dalton Trans., 1993, 119-125; R. P. Pandian and T. K. Chandrashekar, Inorg. Chem., 1994, 33, 3317-3324; P. Chmielewski, L. Latos-Grazyński and E. Pacholska, Inorg. Chem., 1994, 33, 1992-1999.
19. S. Will, J. Lex, E. Vogel, H. Schmickler, J.-P. Gisselbrecht, C. Haubtmann, M. Bernard and M. Gross, Angew. Chem., Int. Ed. Engl., 1997, 36, 357-361; A. Ghosh, T. Wondimagegn and A. B. J. Parusel, J. Am. Chem. Soc., 2000, 122, 5100-5104.
20. S. Will, J. Lex, E. Vogel, H. Schmickler, J.-P. Gisselbrecht, C. Haubtmann, M. Bernard and M. Gross, Angew. Chem., Int. Ed. Engl., 1997, 36, 357-361; A. Ghosh, T. Wondimagegn and A. B. J. Parusel, J. Am. Chem. Soc., 2000, 122, 5100-5104.
21. J. V. Bonfiglio, R. Bonnett, M. B. Hursthouse and K. M. Abdul Malik, J. Chem. Soc., Chem. Commun., 1977, 83-84; J. V. Bonfiglio, R. Bonnett, D. G. Buckley, D. Hamzetash, M. B. Hursthouse, K. M. Abdul Malik, A. F. McDonagh and J. Trotter, Tetrahedron, 1983, 39, 1865-1874; P. A. Lord, M. M. Olmstead and A. L. Balch, Inorg. Chem., 2000, 39, 1128-1134.
22. J. V. Bonfiglio, R. Bonnett, M. B. Hursthouse and K. M. Abdul Malik, J. Chem. Soc., Chem. Commun., 1977, 83-84; J. V. Bonfiglio, R. Bonnett, D. G. Buckley, D. Hamzetash, M. B. Hursthouse, K. M. Abdul Malik, A. F. McDonagh and J. Trotter, Tetrahedron, 1983, 39, 1865-1874; P. A. Lord, M. M. Olmstead and A. L. Balch, Inorg. Chem., 2000, 39, 1128-1134.
23. J. V. Bonfiglio, R. Bonnett, M. B. Hursthouse and K. M. Abdul Malik, J. Chem. Soc., Chem. Commun., 1977, 83-84; J. V. Bonfiglio, R. Bonnett, D. G. Buckley, D. Hamzetash, M. B. Hursthouse, K. M. Abdul Malik, A. F. McDonagh and J. Trotter, Tetrahedron, 1983, 39, 1865-1874; P. A. Lord, M. M. Olmstead and A. L. Balch, Inorg. Chem., 2000, 39, 1128-1134.
24. M. Bröring and C. D. Brandt, Chem. Commun., 2001, 499-500; M. Bröring and C. D. Brandt, J. Chem. Soc., Dalton Trans., 2002, 1391-1395.
25. M. Bröring and C. D. Brandt, Chem. Commun., 2001, 499-500; M. Bröring and C. D. Brandt, J. Chem. Soc., Dalton Trans., 2002, 1391-1395.
26. F. A. Cotton, B. G. DeBoer and J. R. Pipal, Inorg. Chem., 1970, 9, 783-788; compare also R. J. Butcher, C. J. O'Connor and E. Sinn, Inorg. Chem., 1979, 18, 492-497.
27. F. A. Cotton, B. G. DeBoer and J. R. Pipal, Inorg. Chem., 1970, 9, 783-788; compare also R. J. Butcher, C. J. O'Connor and E. Sinn, Inorg. Chem., 1979, 18, 492-497.
28. R. J. Letcher, W. Zhang, C. Bensimon and R. J. Crutchley, Inorg. Chim. Acta, 1993, 210, 183-191; aggregates have also been observed, see T. I. Benzer, L. Dann, C. R. Schwitzgebel, M. D. Tamburro and E. P. Dudek, Inorg. Chem., 1971, 10, 2204-2209.
29. R. J. Letcher, W. Zhang, C. Bensimon and R. J. Crutchley, Inorg. Chim. Acta, 1993, 210, 183-191; aggregates have also been observed, see T. I. Benzer, L. Dann, C. R. Schwitzgebel, M. D. Tamburro and E. P. Dudek, Inorg. Chem., 1971, 10, 2204-2209.
30. J. L. Sessler, A. Gebauer, V. Král and V. Lynch, Inorg. Chem., 1996, 35, 6636; R. G. Khoury, M. O. Senge, J. E. Colchester and K. M. Smith, J. Chem. Soc., Dalton Trans., 1996, 3937-3950.
31. J. L. Sessler, A. Gebauer, V. Král and V. Lynch, Inorg. Chem., 1996, 35, 6636; R. G. Khoury, M. O. Senge, J. E. Colchester and K. M. Smith, J. Chem. Soc., Dalton Trans., 1996, 3937-3950.
32. D. F. Evans, J. Chem. Soc., 1955, 2003-2005; D. F. Evans and T. A. James, J. Chem. Soc., Dalton Trans., 1979, 723-726.
33. D. F. Evans, J. Chem. Soc., 1955, 2003-2005; D. F. Evans and T. A. James, J. Chem. Soc., Dalton Trans., 1979, 723-726.
34. W. R. Scheidt, in The Porphyrin Handbook, eds. K. M. Kadish, K. M. Smith and R. Guilard, Academic, San Diego, CA, 2000, vol. 3, ch. 16, p. 67, and references given therein.
35. Solvent coordination is frequently observed for tetracoordinate Ni(II) complexes with N ligands. For examples, see: R. H. Holm and K. Swaminathan, Inorg. Chem., 1962, 1, 599-607; L. Rusnak and R. B. Jordan, Inorg. Chem., 1971, 10, 2199-2204; A. Anichini, L. Fabbrizzi and P. Paoletti, Inorg. Chim. Acta, 1977,24, L21-L23; N. Herron and P. Moore, Inorg. Chim. Acta, 1979, 36, 89-96; L. Sabatini and L. Fabbrizzi, Inorg. Chem., 1979, 18, 438-444; E. H. Curzon, N. Herron and P. Moore, J. Chem. Soc., Dalton Trans., 1980, 574-578; L. Helm, P. Meier, A. E. Merbach and P. A. Tregloan, Inorg. Chim. Acta, 1983, 73, 1-9; P. Moore, J. Sachinidis and G. R. Willey, J. Chem. Soc., Chem. Commun., 1983, 522-523; P. Moore, J. Sachinidis and R. Willey, J. Chem. Soc., Dalton Trans., 1984, 1323-1327.
36. Solvent coordination is frequently observed for tetracoordinate Ni(II) complexes with N ligands. For examples, see: R. H. Holm and K. Swaminathan, Inorg. Chem., 1962, 1, 599-607; L. Rusnak and R. B. Jordan, Inorg. Chem., 1971, 10, 2199-2204; A. Anichini, L. Fabbrizzi and P. Paoletti, Inorg. Chim. Acta, 1977, 24, L21-L23; N. Herron and P. Moore, Inorg. Chim. Acta, 1979, 36, 89-96; L. Sabatini and L. Fabbrizzi, Inorg. Chem., 1979, 18, 438-444; E. H. Curzon, N. Herron and P. Moore, J. Chem. Soc., Dalton Trans., 1980, 574-578; L. Helm, P. Meier, A. E. Merbach and P. A. Tregloan, Inorg. Chim. Acta, 1983, 73, 1-9; P. Moore, J. Sachinidis and G. R. Willey, J. Chem. Soc., Chem. Commun., 1983, 522-523; P. Moore, J. Sachinidis and R. Willey, J. Chem. Soc., Dalton Trans., 1984, 1323-1327.
37. Solvent coordination is frequently observed for tetracoordinate Ni(II) complexes with N ligands. For examples, see: R. H. Holm and K. Swaminathan, Inorg. Chem., 1962, 1, 599-607; L. Rusnak and R. B. Jordan, Inorg. Chem., 1971, 10, 2199-2204; A. Anichini, L. Fabbrizzi and P. Paoletti, Inorg. Chim. Acta, 1977, 24, L21-L23; N. Herron and P. Moore, Inorg. Chim. Acta, 1979, 36, 89-96; L. Sabatini and L. Fabbrizzi, Inorg. Chem., 1979, 18, 438-444; E. H. Curzon, N. Herron and P. Moore, J. Chem. Soc., Dalton Trans., 1980, 574-578; L. Helm, P. Meier, A. E. Merbach and P. A. Tregloan, Inorg. Chim. Acta, 1983, 73, 1-9; P. Moore, J. Sachinidis and G. R. Willey, J. Chem. Soc., Chem. Commun., 1983, 522-523; P. Moore, J. Sachinidis and R. Willey, J. Chem. Soc., Dalton Trans., 1984, 1323-1327.
38. Solvent coordination is frequently observed for tetracoordinate Ni(II) complexes with N ligands. For examples, see: R. H. Holm and K. Swaminathan, Inorg. Chem., 1962, 1, 599-607; L. Rusnak and R. B. Jordan, Inorg. Chem., 1971, 10, 2199-2204; A. Anichini, L. Fabbrizzi and P. Paoletti, Inorg. Chim. Acta, 1977, 24, L21-L23; N. Herron and P. Moore, Inorg. Chim. Acta, 1979, 36, 89-96; L. Sabatini and L. Fabbrizzi, Inorg. Chem., 1979, 18, 438-444; E. H. Curzon, N. Herron and P. Moore, J. Chem. Soc., Dalton Trans., 1980, 574-578; L. Helm, P. Meier, A. E. Merbach and P. A. Tregloan, Inorg. Chim. Acta, 1983, 73, 1-9; P. Moore, J. Sachinidis and G. R. Willey, J. Chem. Soc., Chem. Commun., 1983, 522-523; P. Moore, J. Sachinidis and R. Willey, J. Chem. Soc., Dalton Trans., 1984, 1323-1327.
39. Solvent coordination is frequently observed for tetracoordinate Ni(II) complexes with N ligands. For examples, see: R. H. Holm and K. Swaminathan, Inorg. Chem., 1962, 1, 599-607; L. Rusnak and R. B. Jordan, Inorg. Chem., 1971, 10, 2199-2204; A. Anichini, L. Fabbrizzi and P. Paoletti, Inorg. Chim. Acta, 1977, 24, L21-L23; N. Herron and P. Moore, Inorg. Chim. Acta, 1979, 36, 89-96; L. Sabatini and L. Fabbrizzi, Inorg. Chem., 1979, 18, 438-444; E. H. Curzon, N. Herron and P. Moore, J. Chem. Soc., Dalton Trans., 1980, 574-578; L. Helm, P. Meier, A. E. Merbach and P. A. Tregloan, Inorg. Chim. Acta, 1983, 73, 1-9; P. Moore, J. Sachinidis and G. R. Willey, J. Chem. Soc., Chem. Commun., 1983, 522-523; P. Moore, J. Sachinidis and R. Willey, J. Chem. Soc., Dalton Trans., 1984, 1323-1327.
40. Solvent coordination is frequently observed for tetracoordinate Ni(II) complexes with N ligands. For examples, see: R. H. Holm and K. Swaminathan, Inorg. Chem., 1962, 1, 599-607; L. Rusnak and R. B. Jordan, Inorg. Chem., 1971, 10, 2199-2204; A. Anichini, L. Fabbrizzi and P. Paoletti, Inorg. Chim. Acta, 1977, 24, L21-L23; N. Herron and P. Moore, Inorg. Chim. Acta, 1979, 36, 89-96; L. Sabatini and L. Fabbrizzi, Inorg. Chem., 1979, 18, 438-444; E. H. Curzon, N. Herron and P. Moore, J. Chem. Soc., Dalton Trans., 1980, 574-578; L. Helm, P. Meier, A. E. Merbach and P. A. Tregloan, Inorg. Chim. Acta, 1983, 73, 1-9; P. Moore, J. Sachinidis and G. R. Willey, J. Chem. Soc., Chem. Commun., 1983, 522-523; P. Moore, J. Sachinidis and R. Willey, J. Chem. Soc., Dalton Trans., 1984, 1323-1327.
41. Solvent coordination is frequently observed for tetracoordinate Ni(II) complexes with N ligands. For examples, see: R. H. Holm and K. Swaminathan, Inorg. Chem., 1962, 1, 599-607; L. Rusnak and R. B. Jordan, Inorg. Chem., 1971, 10, 2199-2204; A. Anichini, L. Fabbrizzi and P. Paoletti, Inorg. Chim. Acta, 1977, 24, L21-L23; N. Herron and P. Moore, Inorg. Chim. Acta, 1979, 36, 89-96; L. Sabatini and L. Fabbrizzi, Inorg. Chem., 1979, 18, 438-444; E. H. Curzon, N. Herron and P. Moore, J. Chem. Soc., Dalton Trans., 1980, 574-578; L. Helm, P. Meier, A. E. Merbach and P. A. Tregloan, Inorg. Chim. Acta, 1983, 73, 1-9; P. Moore, J. Sachinidis and G. R. Willey, J. Chem. Soc., Chem. Commun., 1983, 522-523; P. Moore, J. Sachinidis and R. Willey, J. Chem. Soc., Dalton Trans., 1984, 1323-1327.
42. Solvent coordination is frequently observed for tetracoordinate Ni(II) complexes with N ligands. For examples, see: R. H. Holm and K. Swaminathan, Inorg. Chem., 1962, 1, 599-607; L. Rusnak and R. B. Jordan, Inorg. Chem., 1971, 10, 2199-2204; A. Anichini, L. Fabbrizzi and P. Paoletti, Inorg. Chim. Acta, 1977, 24, L21-L23; N. Herron and P. Moore, Inorg. Chim. Acta, 1979, 36, 89-96; L. Sabatini and L. Fabbrizzi, Inorg. Chem., 1979, 18, 438-444; E. H. Curzon, N. Herron and P. Moore, J. Chem. Soc., Dalton Trans., 1980, 574-578; L. Helm, P. Meier, A. E. Merbach and P. A. Tregloan, Inorg. Chim. Acta, 1983, 73, 1-9; P. Moore, J. Sachinidis and G. R. Willey, J. Chem. Soc., Chem. Commun., 1983, 522-523; P. Moore, J. Sachinidis and R. Willey, J. Chem. Soc., Dalton Trans., 1984, 1323-1327.
43. Solvent coordination is frequently observed for tetracoordinate Ni(II) complexes with N ligands. For examples, see: R. H. Holm and K. Swaminathan, Inorg. Chem., 1962, 1, 599-607; L. Rusnak and R. B. Jordan, Inorg. Chem., 1971, 10, 2199-2204; A. Anichini, L. Fabbrizzi and P. Paoletti, Inorg. Chim. Acta, 1977, 24, L21-L23; N. Herron and P. Moore, Inorg. Chim. Acta, 1979, 36, 89-96; L. Sabatini and L. Fabbrizzi, Inorg. Chem., 1979, 18, 438-444; E. H. Curzon, N. Herron and P. Moore, J. Chem. Soc., Dalton Trans., 1980, 574-578; L. Helm, P. Meier, A. E. Merbach and P. A. Tregloan, Inorg. Chim. Acta, 1983, 73, 1-9; P. Moore, J. Sachinidis and G. R. Willey, J. Chem. Soc., Chem. Commun., 1983, 522-523; P. Moore, J. Sachinidis and R. Willey, J. Chem. Soc., Dalton Trans., 1984, 1323-1327.
44. S. Hannah, V. Lynch, D. M. Guldi, N. Gerasimchuk, C. L. B. MacDonald, D. Magda and J. L. Sessler, J. Am. Chem. Soc., 2002, 124, 8416-8427.
45. M. N. Burnett and C. K. Johnson, ORTEP, Report ORNL-6895, Oak Ridge National Laboratory, Oak Ridge, TN, 1996.