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Before AFM measurement, 1 mg of shortened SWNTs were dispersed in 1 mL of DMF solvent by ultrasonication for 30 min to form a black transparent suspension. A drop of 1 μL suspension was added on mica. After the solvent had evaporated, TM-AFM was performed on nanoscope IIIa (Digital Instrument).
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note
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Renishaw System 1000 Raman imaging System (Renishaw plc, UK), equipped with a 632.8 nm, 25mW He-Ne laser (Spectra Physics, USA) and a BH-2 microscope (Olympus, Japan). The incident light was introduced to the sample through a 50° × objective as a spot less than 2um in diameter, with the power no more than 5 mW. The backscattered light from the sample was collected through the same objective. The spectrum was the sum of a least 10 spectra at different spots.
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