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85037511769
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note
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The mono- and dichlorides described in this report were prepared in situ at 0°C, concentrated in vacuo in the presence of toluene and used without further purification.
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Ethylammonium phosphite, prepared as in Hammond, P. R. J. Chem. Soc. 1962, 2521-2522, was converted to ethylphenyl phosphite by treatment with benzyl alcohol and pivaloyl chloride, similarly to Hill, J. M.; Lowe, G. J. Chem. Soc., Perkin Trans. 1 1995, 2001-2007.
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Ethylammonium phosphite, prepared as in Hammond, P. R. J. Chem. Soc. 1962, 2521-2522, was converted to ethylphenyl phosphite by treatment with benzyl alcohol and pivaloyl chloride, similarly to Hill, J. M.; Lowe, G. J. Chem. Soc., Perkin Trans. 1 1995, 2001-2007.
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we have only observed formation of 5-iodo-2-nitrobenzoic acid, and no 3-iodo-2-nitrobenzoic acid
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