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85037800480
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Deletion studies have determined that R is the important residue for PHSRN function, suggesting that this sequence could be further truncated to SRN, yet still retain its synergistic activity (see ref 5). Therefore, for simplicity, small peptides were chosen. However the polymers can be synthesized using the same approach with larger pendent peptides such as GRGDS and PHSRN.
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15
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85037784863
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note
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Poly(15) and poly(16) have been synthesized by Baigini, et al. (ref 11a,b) using molybdenum catalysts; since ruthenium initiators were used in our study, the synthesis and characterization of these polymers using 1 as the initiator is included here.
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85037785019
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This is thought to be due to unfavorable steric interactions between the monomer and initiating species; see ref 11b.
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12944251622
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Brandrup, J., Immergut, E. H., Grulke, E. A., Eds.; Wiley-Interscience: New York
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85037797525
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note
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Catalyst 1 is markedly less active than 2 and 3 at higher temperatures and is less stable at higher temperatures (see ref 21). For this reason, polymerizations with 1 were conducted at room temperature, while those with 2 and 3 were conducted at 55°C.
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33
-
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85037786947
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-
note
-
This method could not be used with the other protected polymers due to the insolubility of these polymers in solvents suitable for centrifugation through the membrane.
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