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Volumn 6, Issue 22, 2000, Pages 4203-4210

Development of an easy-to-use mass spectrometric technique to monitor solid-phase reactions on polystyrene supports

Author keywords

IR spectroscopy; Kinetics; Mass spectrometry; Polystyrene; Solid phase synthesis

Indexed keywords

POLYSTYRENE; RESIN;

EID: 0034680538     PISSN: 09476539     EISSN: None     Source Type: Journal    
DOI: 10.1002/1521-3765(20001117)6:22<4203::AID-CHEM4203>3.0.CO;2-Q     Document Type: Article
Times cited : (29)

References (55)
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    • All MS methods reported so far for the analysis of solid-phase reactions involve a cleavage step prior to MS analysis: a) B. J. Egner, G. J. Langley, M. Bradley, J. Org. Chem. 1995, 60, 2652-2653;
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    • note
    • The time for drying of resins (usually 24-48 h) can be reduced for fast MS reaction control to about 15-30 min under reduced pressure as the adsorbed solvent is then removed in the MS spectrometer at temperatures below 200°C, so that solvent molecules do not interfere with the resin measurement at T>400°C.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.