메뉴 건너뛰기




Volumn 146, Issue 1, 2000, Pages 132-139

Recoupling of Heteronuclear Dipolar Interactions with Rotational-Echo Double-Resonance at High Magic-Angle Spinning Frequencies

Author keywords

Finite pulse effects; Hetero nuclear dipolar recoupling; Magic angle spinning; Rotational echo double resonance; Solid state NMR

Indexed keywords

GLYCINE;

EID: 0034264324     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.2000.2128     Document Type: Article
Times cited : (95)

References (44)
  • 2
    • 0031000510 scopus 로고    scopus 로고
    • Direct measurement of angles between bond vectors in high-resolution NMR
    • B. Reif, M. Hennig, and C. Griesinger, Direct measurement of angles between bond vectors in high-resolution NMR, Science 276, 1230-1233 (1997).
    • (1997) Science , vol.276 , pp. 1230-1233
    • Reif, B.1    Hennig, M.2    Griesinger, C.3
  • 3
    • 0031450910 scopus 로고    scopus 로고
    • 13C′ (carbonyl) chemical shift anisotropy mechanisms
    • 13C′ (carbonyl) chemical shift anisotropy mechanisms, J. Am. Chem. Soc. 119, 11938-11940 (1997).
    • (1997) J. Am. Chem. Soc. , vol.119 , pp. 11938-11940
    • Yang, D.1    Konrat, R.2    Kay, L.E.3
  • 4
    • 0027772469 scopus 로고
    • Nuclear magnetic resonance methods for measuring dipolar couplings in rotating solids
    • J. M. Griffiths and R. G. Griffin, Nuclear magnetic resonance methods for measuring dipolar couplings in rotating solids, Anal. Chim. Acta 283, 1081-1101 (1993).
    • (1993) Anal. Chim. Acta , vol.283 , pp. 1081-1101
    • Griffiths, J.M.1    Griffin, R.G.2
  • 5
    • 0002960267 scopus 로고
    • Recoupling of homo- and heteronuclear dipolar interactions in rotating solids
    • (B. Blumich, Ed.), Springer-Verlag, Berlin
    • A. E. Bennett, R. G. Griffin, and S. Vega, Recoupling of homo- and heteronuclear dipolar interactions in rotating solids, in "Solid State NMR IV: Methods and Applications of Solid-State NMR" (B. Blumich, Ed.), pp. 1-77, Springer-Verlag, Berlin (1994).
    • (1994) Solid State NMR IV: Methods and Applications of Solid-State NMR , pp. 1-77
    • Bennett, A.E.1    Griffin, R.G.2    Vega, S.3
  • 7
    • 0031853671 scopus 로고    scopus 로고
    • Dipolar recoupling in MAS spectra of biological solids
    • R. G. Griffin, Dipolar recoupling in MAS spectra of biological solids, Nature Struct. Biol. 5, 508-512 (1998).
    • (1998) Nature Struct. Biol. , vol.5 , pp. 508-512
    • Griffin, R.G.1
  • 8
    • 0032986388 scopus 로고    scopus 로고
    • Solid-state nuclear magnetic resonance investigation of protein and polypeptide structure
    • R. Fu and T. A. Cross, Solid-state nuclear magnetic resonance investigation of protein and polypeptide structure. Annu. Rev. Biophys. Biomol. Struct. 28, 235-268 (1999).
    • (1999) Annu. Rev. Biophys. Biomol. Struct. , vol.28 , pp. 235-268
    • Fu, R.1    Cross, T.A.2
  • 9
    • 45149145322 scopus 로고
    • Rotational-echo double-resonance NMR
    • T. Gullion and J. Schaefer, Rotational-echo double-resonance NMR, J. Magn. Reson. 81, 196-200 (1989).
    • (1989) J. Magn. Reson. , vol.81 , pp. 196-200
    • Gullion, T.1    Schaefer, J.2
  • 10
    • 85011817347 scopus 로고
    • Detection of weak heteronuclear dipolar coupling by rotational-echo double-resonance nuclear magnetic resonance
    • T. Gullion and J. Schaefer, Detection of weak heteronuclear dipolar coupling by rotational-echo double-resonance nuclear magnetic resonance, Adv. Magn. Reson. 13, 57-83 (1989).
    • (1989) Adv. Magn. Reson. , vol.13 , pp. 57-83
    • Gullion, T.1    Schaefer, J.2
  • 11
    • 0000734747 scopus 로고
    • Elimination of resonance offset effects in rotational-echo, double-resonance NMR
    • T. Gullion and J. Schaefer, Elimination of resonance offset effects in rotational-echo, double-resonance NMR, J. Magn. Reson. 92, 439-442 (1991).
    • (1991) J. Magn. Reson. , vol.92 , pp. 439-442
    • Gullion, T.1    Schaefer, J.2
  • 12
    • 42649130559 scopus 로고
    • New, compensated Carr-Purcell sequences
    • T. Gullion, D. B. Baker, and M. S. Conradi, New, compensated Carr-Purcell sequences, J. Magn. Reson. 89, 479-484 (1990).
    • (1990) J. Magn. Reson. , vol.89 , pp. 479-484
    • Gullion, T.1    Baker, D.B.2    Conradi, M.S.3
  • 13
    • 0028008254 scopus 로고
    • Time-resolved solid-state REDOR NMR measurements on 5-enol-pyruvylshikimate-3-phosphate synthase
    • Y. Li, R. J. Appleyard, W. A. Shuttleworth, and J. N. S. Evans, Time-resolved solid-state REDOR NMR measurements on 5-enol-pyruvylshikimate-3-phosphate synthase, J. Am. Chem. Soc. 116, 10799-10800 (1994).
    • (1994) J. Am. Chem. Soc. , vol.116 , pp. 10799-10800
    • Li, Y.1    Appleyard, R.J.2    Shuttleworth, W.A.3    Evans, J.N.S.4
  • 14
    • 0029864204 scopus 로고    scopus 로고
    • Structural constraints on the ternary complex of 5-enol-pyruvylshikimate-3-phosphate synthase from rotational-echo double-resonance NMR
    • L. M. McDowell, A. Schmidt, E. R. Cohen, D. R. Studelska, and J. Schaefer, Structural constraints on the ternary complex of 5-enol-pyruvylshikimate-3-phosphate synthase from rotational-echo double-resonance NMR, J. Mol. Biol. 256, 160-171 (1996).
    • (1996) J. Mol. Biol. , vol.256 , pp. 160-171
    • McDowell, L.M.1    Schmidt, A.2    Cohen, E.R.3    Studelska, D.R.4    Schaefer, J.5
  • 16
    • 0032134545 scopus 로고    scopus 로고
    • Rotational-echo double-resonance in complex biopolymers: A study of Nephila clavipes dragline silk
    • C. A. Michal and L. W. Jelinski, Rotational-echo double-resonance in complex biopolymers: A study of Nephila clavipes dragline silk, J. Biomol. NMR 12, 231-241 (1998).
    • (1998) J. Biomol. NMR , vol.12 , pp. 231-241
    • Michal, C.A.1    Jelinski, L.W.2
  • 18
    • 0030810576 scopus 로고    scopus 로고
    • REDOR3D: Heteronuclear distance measurements in uniformly labeled and natural abundance solids
    • C. A. Michal and L. W. Jelinski, REDOR3D: Heteronuclear distance measurements in uniformly labeled and natural abundance solids, J. Am. Chem. Soc. 119, 9059-9060 (1997).
    • (1997) J. Am. Chem. Soc. , vol.119 , pp. 9059-9060
    • Michal, C.A.1    Jelinski, L.W.2
  • 19
    • 0032568767 scopus 로고    scopus 로고
    • θ-REDOR: An MAS NMR method to simplify multiple coupled heteronuclear spin systems
    • T. Gullion and C. H. Pennington, θ-REDOR: An MAS NMR method to simplify multiple coupled heteronuclear spin systems, Chem. Phys. Lett. 290, 88-93 (1998).
    • (1998) Chem. Phys. Lett. , vol.290 , pp. 88-93
    • Gullion, T.1    Pennington, C.H.2
  • 22
    • 0033208603 scopus 로고    scopus 로고
    • 13C multiple-quantum correlation in solids under ultrafast MAS
    • 13C multiple-quantum correlation in solids under ultrafast MAS, J. Magn. Reson. 140, 471-476 (1999).
    • (1999) J. Magn. Reson. , vol.140 , pp. 471-476
    • Saalwächter, K.1    Graf, R.2    Spiess, H.W.3
  • 23
    • 33748501698 scopus 로고    scopus 로고
    • 13C REDOR, X-ray diffraction, and molecular dynamics simulation
    • 13C REDOR, X-ray diffraction, and molecular dynamics simulation, J. Phys. Chem. 100, 14995-15004 (1996); A. Naito, S. Tuzi, and H. Saito, Dipolar interactions and interatomic distances, in "Solid State NMR of Polymers" (I. Ando and T. Asakura, Eds.), pp. 23-49, Elsevier, Amsterdam (1998).
    • (1996) J. Phys. Chem. , vol.100 , pp. 14995-15004
    • Naito, A.1    Nishimura, K.2    Kimura, S.3    Tuzi, S.4    Aida, M.5    Yasuoka, N.6    Saito, H.7
  • 24
    • 77957046272 scopus 로고    scopus 로고
    • Dipolar interactions and interatomic distances
    • (I. Ando and T. Asakura, Eds.), Elsevier, Amsterdam
    • 13C REDOR, X-ray diffraction, and molecular dynamics simulation, J. Phys. Chem. 100, 14995-15004 (1996); A. Naito, S. Tuzi, and H. Saito, Dipolar interactions and interatomic distances, in "Solid State NMR of Polymers" (I. Ando and T. Asakura, Eds.), pp. 23-49, Elsevier, Amsterdam (1998).
    • (1998) Solid State NMR of Polymers , pp. 23-49
    • Naito, A.1    Tuzi, S.2    Saito, H.3
  • 25
    • 0031552562 scopus 로고    scopus 로고
    • Recoupling of heteronuclear dipolar interactions in solid-state magic-angle spinning NMR by simultaneous frequency and amplitude modulation
    • R. Fu, S. A. Smith, and G. Bodenhausen, Recoupling of heteronuclear dipolar interactions in solid-state magic-angle spinning NMR by simultaneous frequency and amplitude modulation, Chem. Phys. Lett. 272, 361-369 (1997).
    • (1997) Chem. Phys. Lett. , vol.272 , pp. 361-369
    • Fu, R.1    Smith, S.A.2    Bodenhausen, G.3
  • 26
    • 85005675278 scopus 로고
    • The transition amplitudes of centerband and sidebands in NMR spectra of rotating solids
    • A. Schmidt and S. Vega, The transition amplitudes of centerband and sidebands in NMR spectra of rotating solids, Isr. J. Chem. 32, 215-230 (1992).
    • (1992) Isr. J. Chem. , vol.32 , pp. 215-230
    • Schmidt, A.1    Vega, S.2
  • 27
    • 0346475450 scopus 로고
    • Floquet density matrices and effective Hamiltonians in magic-angle-spinning NMR spectroscopy
    • O. Weintraub and S. Vega, Floquet density matrices and effective Hamiltonians in magic-angle-spinning NMR spectroscopy, J. Magn. Reson. A 105, 245-267 (1993).
    • (1993) J. Magn. Reson. A , vol.105 , pp. 245-267
    • Weintraub, O.1    Vega, S.2
  • 28
    • 36049055838 scopus 로고
    • Coherent averaging effects in magnetic resonance
    • U. Haeberlen and J. S. Waugh, Coherent averaging effects in magnetic resonance, Phys. Rev. 175, 453-467 (1968).
    • (1968) Phys. Rev. , vol.175 , pp. 453-467
    • Haeberlen, U.1    Waugh, J.S.2
  • 30
    • 0000785903 scopus 로고
    • Rotary resonance recoupling of dipolar interactions in solid-state nuclear magnetic resonance spectroscopy
    • T. G. Oas, R. G. Griffin, and M. H. Levitt, Rotary resonance recoupling of dipolar interactions in solid-state nuclear magnetic resonance spectroscopy, J. Chem. Phys. 89, 692-695 (1988).
    • (1988) J. Chem. Phys. , vol.89 , pp. 692-695
    • Oas, T.G.1    Griffin, R.G.2    Levitt, M.H.3
  • 36
    • 0000539530 scopus 로고
    • NMR in rotating solids
    • M. M. Maricq and J. S. Waugh, NMR in rotating solids, J. Chem. Phys. 70, 3300-3316 (1979).
    • (1979) J. Chem. Phys. , vol.70 , pp. 3300-3316
    • Maricq, M.M.1    Waugh, J.S.2
  • 37
    • 0042432202 scopus 로고
    • 13C NMR studies of ferrocene as a function of magic angle sample spinning frequency
    • 13C NMR studies of ferrocene as a function of magic angle sample spinning frequency, Chem. Phys. Lett. 196, 588-594 (1992).
    • (1992) Chem. Phys. Lett. , vol.196 , pp. 588-594
    • Shannon, I.J.1    Harris, K.D.M.2    Arumugam, S.3
  • 38
    • 0000059834 scopus 로고
    • 13C MAS NMR linewidths. Phase-modulated irradiation for efficient heteronuclear decoupling in rapidly rotating solids
    • 13C MAS NMR linewidths. Phase-modulated irradiation for efficient heteronuclear decoupling in rapidly rotating solids, J. Magn. Reson. A 107, 129-133 (1994).
    • (1994) J. Magn. Reson. A , vol.107 , pp. 129-133
    • Tekely, P.1    Palmas, P.2    Canet, D.3
  • 39
    • 0000013523 scopus 로고    scopus 로고
    • Second-order recoupling of chemical-shielding and dipolar-coupling tensors under spin decoupling in solid-state NMR
    • M. Ernst, S. Bush, A. C. Kolbert, and A. Pines, Second-order recoupling of chemical-shielding and dipolar-coupling tensors under spin decoupling in solid-state NMR, J. Chem. Phys. 105, 3387-3397 (1996).
    • (1996) J. Chem. Phys. , vol.105 , pp. 3387-3397
    • Ernst, M.1    Bush, S.2    Kolbert, A.C.3    Pines, A.4
  • 40
    • 0000353122 scopus 로고    scopus 로고
    • A simple model for heteronuclear spin decoupling in solid-state NMR
    • M. Ernst, H. Zimmermann, and B. H. Meier, A simple model for heteronuclear spin decoupling in solid-state NMR, Chem. Phys. Lett. 317, 581-588 (2000).
    • (2000) Chem. Phys. Lett. , vol.317 , pp. 581-588
    • Ernst, M.1    Zimmermann, H.2    Meier, B.H.3
  • 41
    • 0000432697 scopus 로고    scopus 로고
    • Fivefold symmetric homonuclear dipolar recoupling in rotating solids: Application to double quantum spectroscopy
    • M. Hohwy, C. M. Rienstra, C. P. Jaroniec, and R. G. Griffin, Fivefold symmetric homonuclear dipolar recoupling in rotating solids: Application to double quantum spectroscopy, J. Chem. Phys. 110, 7983-7992 (1999).
    • (1999) J. Chem. Phys. , vol.110 , pp. 7983-7992
    • Hohwy, M.1    Rienstra, C.M.2    Jaroniec, C.P.3    Griffin, R.G.4
  • 43
    • 33750405141 scopus 로고
    • Sideband intensities in NMR spectra of samples spinning at the magic angle
    • J. Herzfeld and A. E. Berger, Sideband intensities in NMR spectra of samples spinning at the magic angle, J. Chem. Phys. 73, 6021-6030 (1980).
    • (1980) J. Chem. Phys. , vol.73 , pp. 6021-6030
    • Herzfeld, J.1    Berger, A.E.2
  • 44
    • 43949161069 scopus 로고
    • Ramped-amplitude cross-polarization in magic-angle-spinning NMR
    • G. Metz, X. Wu, and S. O. Smith, Ramped-amplitude cross-polarization in magic-angle-spinning NMR, J. Magn. Reson. A 110, 219-227 (1994).
    • (1994) J. Magn. Reson. A , vol.110 , pp. 219-227
    • Metz, G.1    Wu, X.2    Smith, S.O.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.