A monomeric samarium bis(iminophosphorano) chelate complex with a Sm=C bond [8]

Journal of the American Chemical Society

Volumn 122, Issue 4, 2000, Pages 726-727

  Aparna, Kasani ^a   Ferguson, Michael ^a   Cavell, Ronald G ^a  

^a UNIVERSITY OF ALBERTA   (Canada)

Author keywords

[No Author keywords available]

Indexed keywords

CHELATE; LANTHANIDE; SAMARIUM;

COMPLEX FORMATION; LETTER; PHOSPHORUS NUCLEAR MAGNETIC RESONANCE;

EID: 0033971257     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja9936114     Document Type: Letter

References (49)

1. (a) Gun'ko, Y. K.; Edelmann, F. T. Comments Inorg. Chem. 1997, 19, 153-184.
2. (b) Ephritikhine, M. Chem. Rev. 1997, 97, 2193-2242.
3. (c) Anwander, R.; Herrmann, W. A. Top. Curr. Chem. 1996, 179, 1-32.
4. (d) Edelmann, F. T. Top. Curr. Chem. 1996, 179, 247-276.
5. (e) Schumann, H.; Meese-Marktscheffel, J. A.; Esser, L. Chem. Rev. 1995, 95, 865-986.
6. (f) Edelmann, F. T. Angew. Chem., Int. Ed. Engl. 1995, 34, 2466-2488.
7. (g) Edelmann, F. T., Scandium, Yttrium, and the Lanthanide and Actinide elements. Excluding their Zero Oxidation State Complexes. In Comprehensive Organometallic Chemistry (II); Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon: Oxford, 1995; Vol. 4, Chapter 2, p 155.
8. (h) Schaverien, C. J. Adv. Organomet. Chem. 1994, 36, 283-363.
9. (a) Hultzsch, K. C.; Spaniol, T. P.; Okuda, J. Angew. Chem., Int. Ed. 1999, 38, 227-230.
10. (b) Shapiro, P. J.; Cotter, W. D.; Schaefer, W. P.; Labinger, J. A.; Bercaw, J. E. J. Am. Chem. Soc. 1994, 116, 4623-4640.
11. (c) Coughlin, E. B.; Bercaw, J. E. J. Am. Chem. Soc. 1992, 114, 7606-7607.
12. (d) Shapiro, P. J.; Bunel, E.; Schaefer, W. P.; Bercaw, J. E. Organometallics 1990, 9, 867-869.
13. (e) Yasuda, H.; Yamamoto, H.; Yokota, K.; Miyake, S.; Nakamura, A. J. Am. Chem. Soc. 1992, 114, 4908-4910.
14. (f) Schaverien, C. J. Organometallics 1994, 13, 69-82.
15. (g) Jeske, G.; Lauke, H.; Mauermann, H.; Swepston, P. N.; Schumann, H.; Marks, T. J. J. Am. Chem. Soc. 1985, 107, 8091-8103.
16. (h) Jeske, G.; Schock, L. E.; Swepston, P. N.; Schumann, H.; Marks, T. J. J. Am. Chem. Soc. 1985, 107, 8103-8110.
17. (i) Jeske, G.; Lauke, H.; Mauermann, H.; Schumann, H.; Marks, T. J. J. Am. Chem. Soc. 1985, 107, 8111-8118.
18. (j) Arredondo, V. M.; Tian, S.; McDonald, F. T.; Marks, T. J. J. Am. Chem. Soc. 1999, 121, 3633-3639.
19. (k) Arredondo, V. M.; McDonald, F. T.; Marks, T. J. Organometallics 1999, 18, 1949-1960.
20. Herrmann, W. A.; Munck, F. C.; Artus, G. R. J.; Runte, O.; Anwander, R. Organometallics 1997, 16, 682-688.
21. Schumann, H.; Glanz, M.; Winterfeld, J.; Hemling, H.; Kuhn, N.; Kratz, T. Angew. Chem., Int. Ed. Engl. 1994, 33, 1733-1734.
22. Arduengo, A. J., III; Tamm, M.; McLain, S. J.; Calabrese, J. C.; Davidson, F.; Marshall, W. J. J. Am. Chem. Soc. 1994, 116, 7927-7928.
23. See for example: (a) Collman, J. P.; Hegedus, L. S.; Norton, J. R.; Finke, R. G. Principles and Applications of Organotransition Metal Chemistry; University Science Books: Mill Valley, CA, 1987; pp 475
24. (b) Doyle, M. P.; Forbes, D. C. Chem. Rev. 1998, 98, 911-935.
25. (c) Vyboishchikov, S. F.; Frenking, G. Chem. Eur. J. 1998, 4, 1428-1438.
26. (d) Brothers, P. J.; Roper, W. R. Chem. Rev. 1988, 88, 1293-1326.
27. (e) Erker, G. Angew. Chem., Int. Ed. Engl. 1989, 28, 397-412.
28. (f) Feldman, J.; Schrock, R. R. Prog. Inorg. Chem. 1991, 39, 1-74.
29. (g) Wulff, W. D. Organometallics 1998, 17, 3116-3134.
30. (h) Brookhart, M.; Studabaker, W. B. Chem. Rev. 1987, 87, 411-432.
31. Cavell, R. G.; Kamalesh Babu, R. P.; Kasani, A.; McDonald, R. J. Am. Chem. Soc. 1999, 121, 5805-5806.
32. Kamalesh Babu, R. P.; McDonald, R.; Decker, S. A.; Klobukowski, M.; Cavell, R. G. Organometallics 1999, 18, 4226-4229.
33. Kasani, A.; McDonald, R.; Cavell, R. G. Organometallics 1999, 18, 3775-3777.
34. Kasani, A.; Kamalesh Babu, R. P.; McDonald, R.; Cavell, R. G. Angew. Chem., Int. Ed. Engl. 1999, 38, 1483-1484.
35. Aparna, K.; Ferguson, M.; McDonald, R.; Cavell, R. G. Organometallics 1999, 18, 4241-4243.
36. Kasani, A.; McDonald, R.; Cavell, R. G. J. Chem. Soc., Chem. Commun. 1999, 1993-1994.
37. Appel, R.; Ruppert, I. Z. Anorg. Allg. Chem. 1974, 406, 131-144.
38. Minhas, R. K.; Ma, Y.; Song, J.-I.; Gambarolla, S. Inorg. Chem. 1996, 35, 1866-1873.
39. 2Sm.: C, 58.83; H, 7.14; N, 4.38. Found: C, 59.39; H. 7.25; N, 4.40.
40. Al-Resayes, S. I.; Hitchcock, P. B.; Nixon, J. F. J. Chem. Soc., Chem. Commun. 1986, 1710-1711.
41. Browning, J.; Dixon, K. R.; Hilts, R. W. Organometallics 1989, 8, 552-554.
42. Robinson, G. H.; Lee, B.; Pennington, W. T.; Sangokoya, S. A. J. Am. Chem. Soc. 1988, 110, 6260-6261.
43. Lee, B.; Sangokoya, S. A.; Pennington, W. T.; Robinson, G. H. J. Coord. Chem. 1990, 21, 99-105.
44. Robinson, G. H.; Self, M. F.; Pennington, W. T.; Sangokoya, S. A. Organometallics 1988, 7, 2424-2426.
45. 2).
46. Johnson, C. K.; ORTEP, Report ORNL No. 5138, Oak Ridge National Labs, Oak Ridge, TN, 1976.
47. Allen, F. H.; Davies, J. E.; Galloy, J. J.; Johnson, O.; Kennard, O.; Macrae, C. F.; Mitchell, E. M.; Mitchell, G. F.; Smith, J. M.; Watson, D. G. J. Chem. Inf. Comput. Sci. 1991, 31, 187-204. The values were calculated from the data retrieved from the Cambridge Crystallographic Data Base.
48. Avis, M. W.; Elsevier: C. J.; Veldman, N.; Kooijman, H.; Spek, A. L. Inorg. Chem. 1996, 35, 1518-1528.
49. 2:: Kamalesh Babu, R. P.; Cavell, R. G.; McDonald, R., University of Alberta Structure Determination Laboratory, Report RGC 9802.